The determination method of 10-hydroxycamptothecin in Camptotheca acuminata fruits by high-performance liquid chromatogram (HPLC) was studied. The HPLC analysis was performed on a HIQ sil C18(4.6×250 mm) column w...The determination method of 10-hydroxycamptothecin in Camptotheca acuminata fruits by high-performance liquid chromatogram (HPLC) was studied. The HPLC analysis was performed on a HIQ sil C18(4.6×250 mm) column with mobile phase of acetonitrilewater (3:7, V:V), flow rate 1 mLmin-1 and UV detective wavelength 266 nm. Extracting 10-hydroxycamptothecin by ultrasonic method from fruits of C. acuminata to prepare samples for analysis was systematically discussed. The optimal extraction condition was carried out by 60% alcohol solution at 60℃ for 50 minutes.展开更多
Aim To develop a high speed and high resolution dynamic rangefinding device for the measurement of large distances.Methods The device was comprised of an ultrasonic transmitter and a receiver,and a receiver , and a co...Aim To develop a high speed and high resolution dynamic rangefinding device for the measurement of large distances.Methods The device was comprised of an ultrasonic transmitter and a receiver,and a receiver , and a continuous ultrasonic wave amplitude-modulated by a low- frequency acoustic signal was used. The rangefinding was achieved by detecting the phase difference between the transmitted and received ultrasonic signals. The design principle. hard- ware implementation , experimental results and performance analysis of the device are included. Results and Conclusion Experiments show that the accuracy of the device are included. within 1.5m while its dynamic data update rate can be up to 40kHz.展开更多
In order to meet the high precision requirement of wide steel strip in industry field, a novel online measurement of roller profile based on sonic circulation and pulse-echo technology was introduced. All kinds of the...In order to meet the high precision requirement of wide steel strip in industry field, a novel online measurement of roller profile based on sonic circulation and pulse-echo technology was introduced. All kinds of the factors influencing the accuracy of roller profile online measurement were analyzed in detail and error compensation analysis of system was accordingly presented. In order to reduce count error, field program gate array(FPGA) was introduced and a highprecision data acquisition system was designed based on digital phase-shift technology. Experiments indicate that the standard deviation of measure data was 7.27 μm, which showed the feasibility and validity of the proposed method, and realized the roll profile measurement with high precision.展开更多
NIOSH ground control safety research program at Spokane,Washington,is exploring applications of photogrammetry to rock mass and support monitoring. This paper describes two ways photogrammetric techniques are being us...NIOSH ground control safety research program at Spokane,Washington,is exploring applications of photogrammetry to rock mass and support monitoring. This paper describes two ways photogrammetric techniques are being used. First,photogrammetric data of laboratory testing is being used to correlate energy input and support deformation. This information can be used to infer remaining support toughness after ground deformation events. This technique is also demonstrated in a field application.Second,field photogrammetric data is compared to crackmeter data from a deep underground mine.Accuracies were found to average 8 mm,but have produced results within 0.2 mm of true displacement,as measured by crackmeters. Application of these techniques consists of monitoring overall fault activity by monitoring multiple points around the crackmeter. A case study is provided in which a crackmeter is clearly shown to have provided insufficient information regarding overall fault ground deformation.Photogrammetry is proving to be a useful ground monitoring tool due to its unobtrusiveness and ease of use.展开更多
AIM: To study the prolonged colonic motility under normal conditions with a novel capsule-style microsystem and to assess its clinical significance. METHODS: A single use telemetry capsule (10 mm in diameter, 20 mm...AIM: To study the prolonged colonic motility under normal conditions with a novel capsule-style microsystem and to assess its clinical significance. METHODS: A single use telemetry capsule (10 mm in diameter, 20 mm in length) embedded with a pressure sensor was ingested by the subjects. The sensor is capable of transmitting colonic pressure wirelessly for more than 130 h. The time of capsule entering the segmental colon was detected by ultrasound. The ultrasonic electrodes were mounted on the surface of the ileocecum and navel and at the junction of the left and rectosigmoid colon of the subjects in sequence, which were identified by abdominal X-rays with radiopaque markers. To verify the accuracy and reliability of ultrasonic detection of telemetry capsules at key points of colon, the segmental colonic transit time was simultaneously recorded by using radiopaque markers. RESULTS: The signal lamp showed that all recorders could receive the radio signal transmitted by the telemetry capsule. The X-rays showed that all telemetry capsules were detected successfully when they were passing through the key points of colon. There was a significant correlation between the transit results obtained by ultrasonic detection or by radiopaque markers. Colorectal recording was obtained from 20 healthy subjects during 613 h (411 h during waking, 202 h during sleep). Compared to waking, the number of pressure contractions and the area under pressure contractions were significantly (P 〈 0.05) decreased during sleep (21 ± 5 h^-vs 15 ± 4 h1, 463 ± 54 mmHg·/min vs 342 ± 45 mmHg·/min). The colonic motility exhibited significant regional variations both in the circadian behavior and in response to waking and meal. CONCLUSION: The capsule-style micro-system is reliable and noninvasive, and may represent a useful tool for the study of physiology and pathology of colonic motor disorders.展开更多
This review gives a short introduction into the principles of ultrasonic measurement techniques for liquids, using cavity resonators. Guidelines for the resonator design in broad-band ultrasonic stxctroscopy as well a...This review gives a short introduction into the principles of ultrasonic measurement techniques for liquids, using cavity resonators. Guidelines for the resonator design in broad-band ultrasonic stxctroscopy as well as in high-resolution single-frequncy or narrowband applications are presented. Deviations of the field configuration in real cells frtxn that in an ideal resonator are discussed and relations for the mode spectrum of cavity fields are given. Recent resonator measurement procedures and methods of data evaluation are mentioned briefly. Some examples of measurements show the extended usability of ultrasonic resonator techniques in basic science and in a wide range of applications for rrkaterials characterization, in manufacturing processes, as well as in control routines.展开更多
Concrete setting and hardening processes are the most critical phases during construction works, influencing properties of a concrete structure. The initial set is important as it provides an estimate when concrete ha...Concrete setting and hardening processes are the most critical phases during construction works, influencing properties of a concrete structure. The initial set is important as it provides an estimate when concrete has reached a point that it can no longer he vibrated without damaging concrete. The point at which final set occurs is important since it provides an estimate when the development of concrete strength and stiffness starts. In this study, experimental work is performed under laboratory conditions to indentify the setting time of cement paste using ultrasonic waves. Correlation between the ultrasonic wave parameters (speed, amplitude and energy) passing through the fresh cement paste and setting time determined using the Vicat test method is analyzed. A method of acoustic emission is also used and acoustic signals recorded in cement paste during hydration are presented.展开更多
Ultrasonic aided slurry sampling hydride generation atomic fluorescence spectrometry (USS-HG-AFS) was developed for the determination of Hg in soil samples from a sewage-irrigated farm. 500 mg grounded soil was susp...Ultrasonic aided slurry sampling hydride generation atomic fluorescence spectrometry (USS-HG-AFS) was developed for the determination of Hg in soil samples from a sewage-irrigated farm. 500 mg grounded soil was suspended in agar solution by an ultrasound water bath before the HG-AFS determination. The results for the reference material of soil (serial number GBW-07411) agreed satisfactorily with the certified values. Results obtained by the developed procedure compared well with those after traditional acid digestion of samples. The detection limit are 6.7ngL-1 for Hg respectively, with average relative standard deviation values of 6.4% for analysis of a series of soil samples of different origin. The recoveries of the anatytes varied in the range from 95 to 107%. This observation has stimulated interest in fast, accurate and sensitive analytical methods for determination of metals in soil.展开更多
The ultrasonic echo in liquid density measurement often suffers noise,which makes it difficult to obtain the useful echo waveform,resulting in low accuracy of density measurement.A denoising method based on improved v...The ultrasonic echo in liquid density measurement often suffers noise,which makes it difficult to obtain the useful echo waveform,resulting in low accuracy of density measurement.A denoising method based on improved variational mode decomposition(VMD)for noise echo signals is proposed.The number of decomposition layers of the traditional VMD is hard to determine,therefore,the center frequency similarity factor is firstly constructed and used as the judgment criterion to select the number of VMD decomposition layers adaptively;Secondly,VMD algorithm is used to decompose the echo signal into several modal components with a single modal component,and the useful echo components are extracted based on the features of the ultrasonic emission signal;Finally,the liquid density is calculated by extracting the amplitude and time of the echo from the modal components.The simulation results show that using the improved VMD to decompose the echo signal not only can improve the signal-to-noise ratio of the echo signal to 20.64 dB,but also can accurately obtain the echo information such as time and amplitude.Compared with the ensemble empirical mode decomposition(EEMD),this method effectively suppresses the modal aliasing,keeps the details of the signal to the maximum extent while suppressing noise,and improves the accuracy of the liquid density measurement.The density measurement accuracy can reach 0.21%of full scale.展开更多
Broadband ultrasound signals will produce distortion in viscoacoustic medium, which may influence the accuracy of time-of-flight (TOF) measurement. Under the condition of single-frequency acoustic source, the wave pro...Broadband ultrasound signals will produce distortion in viscoacoustic medium, which may influence the accuracy of time-of-flight (TOF) measurement. Under the condition of single-frequency acoustic source, the wave propagation process in viscoacoustic medium was analyzed and an approximate solution of the wave propagation was given. Instances of broadband ultrasound were analyzed and simulated based on the single-frequency results. A single-frequency matching pursuits (SFMP) algorithm was then introduced to solve the waveform distortion problem. Time-frequency decomposition was applied to extracting the single-frequency compositions from broadband ultrasound signals, and then these compositions were sent to the matching pursuits (MP) algorithm for calculating the TOF parameters. Compared with the broadband signals, the shapes of extracted single-frequency signals change more slightly as distance and attenuation coefficient increase. The residuals of SFMP were far less than those of MP algorithm. Experimental results show that the SFMP algorithm is able to eliminate waveform distortion of broadband ultrasound in viscoacoustic medium, which helps improve the accuracy of TOF measurement.展开更多
Ultrasonic wave testing was applied to investigate the quality and weathering status of rock specimens obtained in two borings situated in the Xishan Buddha rock slope in Taiyuan, China. This paper pays special attent...Ultrasonic wave testing was applied to investigate the quality and weathering status of rock specimens obtained in two borings situated in the Xishan Buddha rock slope in Taiyuan, China. This paper pays special attention to the distribution of bulk density, dynamic parameters and static parameters of rock specimens as well as the relationship between static and dynamic parameters. The results illustrate that the distribution of both parameters is identical along the depth of two drilled holes in the rock slope. When the hole depth increases, the density of rock mass, saturated compression strength and static elastic modulus, dynamic elastic modulus and wave velocity also show increase tendency. The weathering degree in the rock mass ranging from the surface of cliff to the depth of 2.5 m is the highest while the rock mass is unsalted and more rigid when the depth is larger than 3.0 m. The relationship between dynamic elastic modulus, sonic wave velocity and horizontal depth indicates that dynamic elastic modulus is more sensitive than sonic wave velocity. Conversely, by comparing quantity relationship between static elastic modulus and sonic wave velocity, it is found that the composition of rock has a great influence on the relationship between static and dynamic parameters, that is, inequality of rock composition will lead to dispersion and abnormality of the distribution of static and dynamic parameters.展开更多
基金This paper was supported by National Natural Science Foundation of China (No. 30070086).
文摘The determination method of 10-hydroxycamptothecin in Camptotheca acuminata fruits by high-performance liquid chromatogram (HPLC) was studied. The HPLC analysis was performed on a HIQ sil C18(4.6×250 mm) column with mobile phase of acetonitrilewater (3:7, V:V), flow rate 1 mLmin-1 and UV detective wavelength 266 nm. Extracting 10-hydroxycamptothecin by ultrasonic method from fruits of C. acuminata to prepare samples for analysis was systematically discussed. The optimal extraction condition was carried out by 60% alcohol solution at 60℃ for 50 minutes.
文摘Aim To develop a high speed and high resolution dynamic rangefinding device for the measurement of large distances.Methods The device was comprised of an ultrasonic transmitter and a receiver,and a receiver , and a continuous ultrasonic wave amplitude-modulated by a low- frequency acoustic signal was used. The rangefinding was achieved by detecting the phase difference between the transmitted and received ultrasonic signals. The design principle. hard- ware implementation , experimental results and performance analysis of the device are included. Results and Conclusion Experiments show that the accuracy of the device are included. within 1.5m while its dynamic data update rate can be up to 40kHz.
文摘In order to meet the high precision requirement of wide steel strip in industry field, a novel online measurement of roller profile based on sonic circulation and pulse-echo technology was introduced. All kinds of the factors influencing the accuracy of roller profile online measurement were analyzed in detail and error compensation analysis of system was accordingly presented. In order to reduce count error, field program gate array(FPGA) was introduced and a highprecision data acquisition system was designed based on digital phase-shift technology. Experiments indicate that the standard deviation of measure data was 7.27 μm, which showed the feasibility and validity of the proposed method, and realized the roll profile measurement with high precision.
文摘NIOSH ground control safety research program at Spokane,Washington,is exploring applications of photogrammetry to rock mass and support monitoring. This paper describes two ways photogrammetric techniques are being used. First,photogrammetric data of laboratory testing is being used to correlate energy input and support deformation. This information can be used to infer remaining support toughness after ground deformation events. This technique is also demonstrated in a field application.Second,field photogrammetric data is compared to crackmeter data from a deep underground mine.Accuracies were found to average 8 mm,but have produced results within 0.2 mm of true displacement,as measured by crackmeters. Application of these techniques consists of monitoring overall fault activity by monitoring multiple points around the crackmeter. A case study is provided in which a crackmeter is clearly shown to have provided insufficient information regarding overall fault ground deformation.Photogrammetry is proving to be a useful ground monitoring tool due to its unobtrusiveness and ease of use.
基金Supported by the High Technology Research and Development Program of China, No. 2004AA404013
文摘AIM: To study the prolonged colonic motility under normal conditions with a novel capsule-style microsystem and to assess its clinical significance. METHODS: A single use telemetry capsule (10 mm in diameter, 20 mm in length) embedded with a pressure sensor was ingested by the subjects. The sensor is capable of transmitting colonic pressure wirelessly for more than 130 h. The time of capsule entering the segmental colon was detected by ultrasound. The ultrasonic electrodes were mounted on the surface of the ileocecum and navel and at the junction of the left and rectosigmoid colon of the subjects in sequence, which were identified by abdominal X-rays with radiopaque markers. To verify the accuracy and reliability of ultrasonic detection of telemetry capsules at key points of colon, the segmental colonic transit time was simultaneously recorded by using radiopaque markers. RESULTS: The signal lamp showed that all recorders could receive the radio signal transmitted by the telemetry capsule. The X-rays showed that all telemetry capsules were detected successfully when they were passing through the key points of colon. There was a significant correlation between the transit results obtained by ultrasonic detection or by radiopaque markers. Colorectal recording was obtained from 20 healthy subjects during 613 h (411 h during waking, 202 h during sleep). Compared to waking, the number of pressure contractions and the area under pressure contractions were significantly (P 〈 0.05) decreased during sleep (21 ± 5 h^-vs 15 ± 4 h1, 463 ± 54 mmHg·/min vs 342 ± 45 mmHg·/min). The colonic motility exhibited significant regional variations both in the circadian behavior and in response to waking and meal. CONCLUSION: The capsule-style micro-system is reliable and noninvasive, and may represent a useful tool for the study of physiology and pathology of colonic motor disorders.
文摘This review gives a short introduction into the principles of ultrasonic measurement techniques for liquids, using cavity resonators. Guidelines for the resonator design in broad-band ultrasonic stxctroscopy as well as in high-resolution single-frequncy or narrowband applications are presented. Deviations of the field configuration in real cells frtxn that in an ideal resonator are discussed and relations for the mode spectrum of cavity fields are given. Recent resonator measurement procedures and methods of data evaluation are mentioned briefly. Some examples of measurements show the extended usability of ultrasonic resonator techniques in basic science and in a wide range of applications for rrkaterials characterization, in manufacturing processes, as well as in control routines.
文摘Concrete setting and hardening processes are the most critical phases during construction works, influencing properties of a concrete structure. The initial set is important as it provides an estimate when concrete has reached a point that it can no longer he vibrated without damaging concrete. The point at which final set occurs is important since it provides an estimate when the development of concrete strength and stiffness starts. In this study, experimental work is performed under laboratory conditions to indentify the setting time of cement paste using ultrasonic waves. Correlation between the ultrasonic wave parameters (speed, amplitude and energy) passing through the fresh cement paste and setting time determined using the Vicat test method is analyzed. A method of acoustic emission is also used and acoustic signals recorded in cement paste during hydration are presented.
文摘Ultrasonic aided slurry sampling hydride generation atomic fluorescence spectrometry (USS-HG-AFS) was developed for the determination of Hg in soil samples from a sewage-irrigated farm. 500 mg grounded soil was suspended in agar solution by an ultrasound water bath before the HG-AFS determination. The results for the reference material of soil (serial number GBW-07411) agreed satisfactorily with the certified values. Results obtained by the developed procedure compared well with those after traditional acid digestion of samples. The detection limit are 6.7ngL-1 for Hg respectively, with average relative standard deviation values of 6.4% for analysis of a series of soil samples of different origin. The recoveries of the anatytes varied in the range from 95 to 107%. This observation has stimulated interest in fast, accurate and sensitive analytical methods for determination of metals in soil.
文摘The ultrasonic echo in liquid density measurement often suffers noise,which makes it difficult to obtain the useful echo waveform,resulting in low accuracy of density measurement.A denoising method based on improved variational mode decomposition(VMD)for noise echo signals is proposed.The number of decomposition layers of the traditional VMD is hard to determine,therefore,the center frequency similarity factor is firstly constructed and used as the judgment criterion to select the number of VMD decomposition layers adaptively;Secondly,VMD algorithm is used to decompose the echo signal into several modal components with a single modal component,and the useful echo components are extracted based on the features of the ultrasonic emission signal;Finally,the liquid density is calculated by extracting the amplitude and time of the echo from the modal components.The simulation results show that using the improved VMD to decompose the echo signal not only can improve the signal-to-noise ratio of the echo signal to 20.64 dB,but also can accurately obtain the echo information such as time and amplitude.Compared with the ensemble empirical mode decomposition(EEMD),this method effectively suppresses the modal aliasing,keeps the details of the signal to the maximum extent while suppressing noise,and improves the accuracy of the liquid density measurement.The density measurement accuracy can reach 0.21%of full scale.
基金Supported by National Natural Science Foundation of China (No.30800240 and No.60901043)
文摘Broadband ultrasound signals will produce distortion in viscoacoustic medium, which may influence the accuracy of time-of-flight (TOF) measurement. Under the condition of single-frequency acoustic source, the wave propagation process in viscoacoustic medium was analyzed and an approximate solution of the wave propagation was given. Instances of broadband ultrasound were analyzed and simulated based on the single-frequency results. A single-frequency matching pursuits (SFMP) algorithm was then introduced to solve the waveform distortion problem. Time-frequency decomposition was applied to extracting the single-frequency compositions from broadband ultrasound signals, and then these compositions were sent to the matching pursuits (MP) algorithm for calculating the TOF parameters. Compared with the broadband signals, the shapes of extracted single-frequency signals change more slightly as distance and attenuation coefficient increase. The residuals of SFMP were far less than those of MP algorithm. Experimental results show that the SFMP algorithm is able to eliminate waveform distortion of broadband ultrasound in viscoacoustic medium, which helps improve the accuracy of TOF measurement.
文摘Ultrasonic wave testing was applied to investigate the quality and weathering status of rock specimens obtained in two borings situated in the Xishan Buddha rock slope in Taiyuan, China. This paper pays special attention to the distribution of bulk density, dynamic parameters and static parameters of rock specimens as well as the relationship between static and dynamic parameters. The results illustrate that the distribution of both parameters is identical along the depth of two drilled holes in the rock slope. When the hole depth increases, the density of rock mass, saturated compression strength and static elastic modulus, dynamic elastic modulus and wave velocity also show increase tendency. The weathering degree in the rock mass ranging from the surface of cliff to the depth of 2.5 m is the highest while the rock mass is unsalted and more rigid when the depth is larger than 3.0 m. The relationship between dynamic elastic modulus, sonic wave velocity and horizontal depth indicates that dynamic elastic modulus is more sensitive than sonic wave velocity. Conversely, by comparing quantity relationship between static elastic modulus and sonic wave velocity, it is found that the composition of rock has a great influence on the relationship between static and dynamic parameters, that is, inequality of rock composition will lead to dispersion and abnormality of the distribution of static and dynamic parameters.