A comparative study was conducted by using solution combustion synthesis with three different doping routes(liquid-liquid(WL10), liquid-solid(WLNO) and solid-solid(WLO)) to produce nanoscale powders and further fabric...A comparative study was conducted by using solution combustion synthesis with three different doping routes(liquid-liquid(WL10), liquid-solid(WLNO) and solid-solid(WLO)) to produce nanoscale powders and further fabricate the ultrafine-grained W-1.0 wt.%La2O3 alloys by pressureless sintering. Compared with pure tungsten, W-1.0 wt.%La2O3 alloys exhibit ultrafine grains and excellent mechanical properties. After sintering, the average grain size of the WLO sample is larger than that of WL10 and WLNO samples;the microhardness values of WL10 and WLNO samples are similar but larger than the value of WLO sample. The optimized La2O3 particles are obtained in the WL10 sample after sintering at 1500 ℃ with the minimum mean size by comparing with WLNO and WLO samples, which are uniformly distributed either at grain boundaries or in the grain interior with the sizes of(57±29.7) and(27±13.1) nm, respectively. This study exhibits ultrafine microstructure and outperforming mechanical properties of the W-1.0 wt.%La2O3 alloy via the liquid-liquid doping route, as compared with conventionally-manufactured tungsten materials.展开更多
The broad applicability of super-resolution microscopy has been widely demonstrated in various areas and disciplines. The optimization and improvement of algorithms used in super-resolution microscopy are of great imp...The broad applicability of super-resolution microscopy has been widely demonstrated in various areas and disciplines. The optimization and improvement of algorithms used in super-resolution microscopy are of great importance for achieving optimal quality of super-resolution imaging. In this review, we comprehensively discuss the computational methods in different types of super-resolution microscopy, including deconvolution microscopy, polarization-based super-resolution microscopy, structured illumination microscopy, image scanning microscopy, super-resolution optical fluctuation imaging microscopy, single-molecule localization microscopy, Bayesian super-resolution microscopy, stimulated emission depletion microscopy, and translation microscopy. The development of novel computational methods would greatly benefit super-resolution microscopy and lead to better resolution, improved accuracy, and faster image processing.展开更多
A sol-gel synthetic approach combined with an ultrasonic method was utilized to prepare Al/B/Fe2O3 nanothermites.The structure and properties of the prepared nanothermites were characterized by thermogravimetric analy...A sol-gel synthetic approach combined with an ultrasonic method was utilized to prepare Al/B/Fe2O3 nanothermites.The structure and properties of the prepared nanothermites were characterized by thermogravimetric analysis,differential scanning calorimetry,scanning electron microscopy,X-ray diffraction,and an impact sensitivity test.The results verified that the nano-aluminum and the micro-boron were uniformly dispersed in the pores of the iron oxide gel.The heat of the prepared Al/B/Fe2O3 nanothermites was 1.3 times that of the simple physically mixed sample.In addition,the heat of the combustion test showed that these materials were indeed energetic.Small-scale safe experiments also showed that the prepared materials through sol-gel were relatively insensitive to standard impact.展开更多
基金Projects(2017YFB0306000,2017YFB0305600)supported by the National Key Research and Development Program of ChinaProjects(51774035,51604025,51574031,51574030,51574029,51604240)supported by the National Natural Science Foundation of China+2 种基金Project(2019JZZY010327)supported by the Shandong Key Research and Development Plan Project,ChinaProjects(2174079,2162027)supported by the Natural Science Foundation Program of Beijing,ChinaProjects(FRF-IDRY-19-025,FRF-TP-17-034A2,FRF-TP-19-015A3,FRF-IDRY-19-003C2)supported by the Fundamental Research Funds for the Central Universities of China。
文摘A comparative study was conducted by using solution combustion synthesis with three different doping routes(liquid-liquid(WL10), liquid-solid(WLNO) and solid-solid(WLO)) to produce nanoscale powders and further fabricate the ultrafine-grained W-1.0 wt.%La2O3 alloys by pressureless sintering. Compared with pure tungsten, W-1.0 wt.%La2O3 alloys exhibit ultrafine grains and excellent mechanical properties. After sintering, the average grain size of the WLO sample is larger than that of WL10 and WLNO samples;the microhardness values of WL10 and WLNO samples are similar but larger than the value of WLO sample. The optimized La2O3 particles are obtained in the WL10 sample after sintering at 1500 ℃ with the minimum mean size by comparing with WLNO and WLO samples, which are uniformly distributed either at grain boundaries or in the grain interior with the sizes of(57±29.7) and(27±13.1) nm, respectively. This study exhibits ultrafine microstructure and outperforming mechanical properties of the W-1.0 wt.%La2O3 alloy via the liquid-liquid doping route, as compared with conventionally-manufactured tungsten materials.
基金Project supported by the National Key Foundation for Exploring Scientific Instrument （No. 2013YQ03065102）, the National Basic Research Program （973） of China （No. 2012CB316503）, and the National Natural Science Foundation of China （Nos. 31327901, 61475010, 31361163004, and 61428501）
文摘The broad applicability of super-resolution microscopy has been widely demonstrated in various areas and disciplines. The optimization and improvement of algorithms used in super-resolution microscopy are of great importance for achieving optimal quality of super-resolution imaging. In this review, we comprehensively discuss the computational methods in different types of super-resolution microscopy, including deconvolution microscopy, polarization-based super-resolution microscopy, structured illumination microscopy, image scanning microscopy, super-resolution optical fluctuation imaging microscopy, single-molecule localization microscopy, Bayesian super-resolution microscopy, stimulated emission depletion microscopy, and translation microscopy. The development of novel computational methods would greatly benefit super-resolution microscopy and lead to better resolution, improved accuracy, and faster image processing.
文摘A sol-gel synthetic approach combined with an ultrasonic method was utilized to prepare Al/B/Fe2O3 nanothermites.The structure and properties of the prepared nanothermites were characterized by thermogravimetric analysis,differential scanning calorimetry,scanning electron microscopy,X-ray diffraction,and an impact sensitivity test.The results verified that the nano-aluminum and the micro-boron were uniformly dispersed in the pores of the iron oxide gel.The heat of the prepared Al/B/Fe2O3 nanothermites was 1.3 times that of the simple physically mixed sample.In addition,the heat of the combustion test showed that these materials were indeed energetic.Small-scale safe experiments also showed that the prepared materials through sol-gel were relatively insensitive to standard impact.
