嘌呤衍生物在葫芦[6]脲单轮烷键合固定相上的色谱行为

在反相和正相色谱模式下,研究了几种嘌呤衍生物在葫芦[6]脲单轮烷键合硅胶固定相上的高效液相色谱行为,并在反相模式下与OD S固定相进行了比较,考察了流动相中甲醇含量、流动相pH值和离子强度对嘌呤化合物保留的影响。研究结果表明:在反相模式下,嘌呤化合物与葫芦[6]脲单轮烷键合相之间存在多种相互作用,除疏水作用外,分离过程中还存在与OD S不同的色谱分离机制。在正相条件下,多作用力的色谱分离机制同样存在。葫芦[6]脲单轮烷键合相与溶质之间存在疏水、氢键、π-π和偶极-偶极等多种作用力,协同作用提高了固定相对嘌呤化合物的分离选择性。

复杂地质条件储气库“极限动用”理论与实践

针对复杂地质条件储气库,基于20余年的运行实践,结合储气库系列攻关成果,揭示了储气地质体承压动力学机制,发现了“多轮相渗滞后”和“分区差异动用”气水互驱渗流规律,提出了以“储气库储气最多、井注入产出能力最大、空间利用效率最高”为目标的复杂地质条件储气库“极限动用”理论,形成了储气地质体极限承压、井极限产能、储气空间极限调峰能力三位一体的评价方法。实现了储气地质体在上限压力条件下获得最大储气空间(库容)、充分发挥地层-井筒气体流动协调的井极限产能以及满足有限时率不稳定渗流条件的最佳井网密度,获得下限压力条件下的最大调峰能力,达到安全和能力的双重极限效果。新疆呼图壁、西南相国寺、辽河双6等地下储气库的运行实践证明,“极限动用”理论有力推动了中国储气库业务高质量发展。

怎样拆装汽车轮胎

拆卸轮胎前,首先将气放尽,严禁带气拆卸。拆卸时通常用一根直头、一根弯头的两根专用撬棒,先将挡圈的切口从轮辋槽内撬出,取出挡圈后,随后拆下轮胎。拆轮胎时,不能用大铁锤猛击轮辋,以免挡圈和轮辋产生永久变形。轮辋除锈要彻底,涂漆要均匀,如有严重变形应更换;检查外胎有无严重老化、裂纹、起包、脱层,检查内胎有无擦伤、漏气等现象,如有应及时修复或更换。

PYRAMIDAL MULTIPHASE LEVEL SET FRAMEWORK FOR BRAIN TUMOR DETECTION USING GENERALIZED TECHNIQUE OF PAINTING BACKGROUND

The pyramidal multiphase level set framework （PMLSF） based on the technique of painting background （TPBG） and the Chan-Vese model can detect multiple objects on a given image. However, the boundaries of the sub-object obtained by PMLSF-TPBG are not variable since a specialcolor parameter is used in TPBG. To solve the problem, a new technique utilizing a varying parameter is proposed to ensure that PMLSF is effective for the detection of the desired boundaries of the sub-object. The interval of the variable color parameter is proved and the effects of the parameter are also discussed. Experimental results for the brain tumor detection show that different boundaries of the brain tumors can be detected with different color parameters. It is especially useful for clinical diagnoses.

Error-CompensatingFive-SamplePhase-Shifting Algorithm Based on Phase-Shift Error Estimation

A new error compensating five sample phase shifting algorithm which is insensitive to phase shift error is proposed to retrieve the phase distribution of a fringe pattern. It includes two steps. First, the linear phase shift error is estimated using four sample images. Then, the phase distribution is calculated with error corrected by using the phase shift error estimated in the first step. As the equations of error estimation and phase calculation are simple, this new algorithm is practical as well as effective. Computer simulations were carried out to verify the effectiveness of the algorithm. Results of two other well known error compensating algorithms are also presented, which show the new algorithm is the least sensitive to phase shift error.

“哈铁职工赛”

九五年度哈尔滨铁路局棋牌赛在齐齐哈尔市举行,牡丹江分局的张晓刚在九轮棋比赛中六胜三和积十五分获个人冠军,牡分局也获得团体冠军。海拉尔分局唐振东是一员经验丰富的老将,棋风沉稳厚重,中残局功力颇佳,且看两人最后一轮相遇之战:

Wheel slip-sinkage and its prediction model of lunar rover

In order to investigate wheel slip-sinkage problem, which is important for the design, control and simulation of lunar rovers, experiments were carried out with a wheel-soil interaction test system to measure the sinkage of three types of wheels in dimension with wheel lugs of different heights and numbers under a series of slip ratios (0-0.6). The curves of wheel sinkage versus slip ratio were obtained and it was found that the sinkage with slip ratio of 0.6 is 3-7 times of the static sinkage. Based on the experimental results, the slip-sinkage principle of lunar's rover lugged wheels (including the sinkage caused by longitudinal flow and side flow of soil, and soil digging of wheel lugs) was analyzed, and corresponding calculation equations were derived. All the factors that can cause slip sinkage were considered to improve the conventional wheel-soil interaction model, and a formula of changing the sinkage exponent with the slip ratio was established. Mathematical model for calculating the sinkage of wheel according to vertical load and slip ratio was developed. Calculation results show that this model can predict the slip-sinkage of wheel with high precision, making up the deficiency of Wong-Reece model that mainly reflects longitudinal slip-sinkage.

Profilometry with Grating Projection Based on One-step Phase Shift

An optical technique for 3 D shape measurement is presented. This technique, based on a deformed projected grating pattern which carries 3 D information of the measured object, can automatically and accurately obtain the phase map of a measured object by using one step phase shift algorithm.In comparison with traditional phase shift technique, the technique is much faster, with the equivalent accuracy. Only one frame image is sufficient for measuring. Experimental result of typical object is presented.

Dynamic performance of heavy-haul combined train applying emergency braking on straight line

A heavy-haul train-track coupled model is developed. Taking the emergency braking of the 2×104 t combined train as example, the train longitudinal impulse, the coupler dynamic behaviors and wheel-rail interactions of vehicles distributing in the different positions are analyzed. The results indicate that under the coupler compressing forces, the couplers of middle locomotives may tilt to the free swing limits, which induces the unidirectional tilt of their connected wagon couplers. Consequently, the coupler longitudinal forces produce the lateral components, and then affect the wheel-rail dynamic interaction. The performance of the middle locomotive and their neighboring freight wagons deteriorate significantly, becoming the most dangerous parts in the combined train. The wagons disconnecting with the locomotives can basically keep their couplers to stabilize in the centering positions, even though the maximum coupler longitudinal force acts on it. And its corresponding running safety also has little changes.

Flooding Characteristics of Hydrofoil Impeller in a Two- and Three-phase Stirred Tank

The flooding characteristics of hydrofoil impeller were systematically investigated in a two-and three-phase 383 mm i.d. stirred tank operated on air, water and spherical glass beads. The volumetric solid concen-tration Cs was varied from 0 to 25%. And the superficial gas velocity Ug was at the range of 0-0.096 m·s-1. A fast and objective method for identifying flooding point NF is developed based on the statistical analysis of the pressure fluctuation signals. It is found, the effect of solid concentration on the flooding point NF depends on the gas velocity. At the lower gas velocity (Ug = 0.010 m·s-1), the solid concentration has only a minor effect. However, it displays a very significant effect on the flooding point NF at the medium and high gas velocity. The flooding point NF linearly increases with the gas velocity Ug, at lower solid concentration (Cs = 0, 10%). When Cs = 20%, the behavior of NF versus Ug becomes more complex. The correlations of the flooding characteristics in the slurry stirred tank are proposed by considering the solid concentration effect.

Effect of wind fluctuating on self-starting aerodynamics characteristics of VAWT

The present work deals with an investigation of the self-starting aerodynamic characteristics of VAWT under fluctuating wind. In contrast to the previous studies, the rotational speed of the turbine is not fixed, the rotation of the turbine is determined by the dynamic interaction between the fluctuating wind and turbine. A weak coupling method is developed to simulate the dynamic interaction between the fluctuating wind and passive rotation turbine, and the results show that if the fluctuating wind with appropriate fluctuation amplitude and frequency, the self-starting aerodynamic characteristics of VAWT will be enhanced. It is also found that compared with the fluctuation amplitude, the fluctuation frequency of the variation in wind velocity is shown to have a minor effect on the performance of the turbine. The analysis will provide straightforward physical insight into the self-starting aerodynamic characteristics of VAWT under fluctuating wind.

Modeling and Simulation of aCounter-Rotating Turbine System for Underwater Vehicles

The structure of a counter-rotating turbine of an underwater vehicle is designed by adding the counter-rotating second-stage turbine disk to the conventional single-stage turbine. The available kinetic energy and the absorption power of the auxiliary system are calculated at different working conditions, and the results show that the power of the main engine and auxiliary system at the counter-rotating turbine system matches well with each other. The technology scheme of the counter-rotating turbine system is proposed, then the experimental simulation of the lubricating oil loop, fuel loop, and seawater loop is completed. The simulation results indicate that the hydraulic transmission system can satisfy the requirements for an underwater vehicle running at a steady sailing or variable working conditions.

Numerical simulation of tire/soil interaction using a verified 3D finite element model

The compaction and stress generation on terrain were always investigated based on empirical approaches or testing methods for tire/soil interaction.However,the analysis should be performed for various tires and at different soil strengths.With the increasing capacity of numerical computers and simulation software,finite element modeling of tire/terrain interaction seems a good approach for predicting the effect of change on the parameters.In this work,an elaborated 3D model fully complianning with the geometry of radial tire 115/60R13 was established,using commercial code Solidwork Simulation.The hyper-elastic and incompressible rubber as tire main material was analyzed by Moony-Rivlin model.The Drucker-Prager yield criterion was used to model the soil compaction.Results show that the model realistically predicts the laboratory tests outputs of the modeled tire on the soft soil.

Void Fraction Distributions in Cold-gassed and Hot-sparged Three Phase Stirred Tanks with Multi-impeller

Vertical distributions of void fraction in gas-liquid and gas-liquid-solid stirred tanks have been measured in a fully baffled dished base vessel of 0.48 m diameter, using a conductivity probe. The impeller configuration （a hollow half elliptical blade dispersing turbine below two up-pumping wide blade hydrofoils, identified as HEDT＋2WHu） recommended in previous work has been used in this work. The operating temperatures were 24℃ and 81℃, identified as cold and hot respectively. The effects of superficial gas velocity, agitator speed and the corresponding power input on the local void fraction in two-phase systems are .investigated and discussed. Results show thatth-e increasing of agitator speed or gas flow rate leads to an increase in local-void fraction at the majority of measurement points in both cold and hot systems. However, the unifo,rmity of gas dispersion does not always in crease as the raising of agitator speed and power input. In either cold or hot sparged conditions, the two- and three-phase systems.have similar vertical profiles for void fraction, with maxima in similar locations; however, the void fractions are significantly lower in hot sparging than with cold. In cold operation the presence of particles leads to a lower void fraction at most points, although the local void fractions increase a little with the addition of solid particles at high temperature, in good agreement with the global gas holdup results, and the possible reasons are discussed in this paper. This work can give a better understanding of the differences between cold-gassed and hot-sparged three phase＇stirred tanks.

Study on Model of Correlation Between Chemical Ele－ment Contents in Tree Rings and Soils near Tree Roots

The chemical element contents in tree rings are correlated with those in the soils near the tree roots. Theresults in the present study showed that the correlation between them could be described using the followinglogarithmic linear correlation model:lgC'(Z) = α(Z) + b(Z)lgC(Z).Therefore, by determining the chrono-sequence C(Z, t), where Z is the atomic number and t the year ofelemental contents in the annual growth rings of trees, we could get the chrono-sequence C'(Z, t) of elementalcontents in the soil, thus inferring the dynamic variations of relevant elemental contents in the soil.

Ultimate Strength Assessment of a Tanker Hull Based on Experimentally Developed Master Curves

A geometrically similar scaling was made from small-scale specimen to full-scale stiffened panels and then their collapse behaviour is investigated. It is considered that the stiffened panel compressive ultimate strength test was designed according to geometrical scaling laws so that the output of the test could be used as representative of the stiffened panels of the compressive zone of a tanker hull subjected to vertical bending moment. The ultimate strength of a tanker hull is analysed by a FE analysis using the experimentally developed master stress-strain curves which are obtained by the beam tension test and the compressive test of the stiffened panel, and are then compared with the result achieved by the progressive collapse method.

Alterable-element Method for Vehicle-bridge Interaction Considering the Transient Jump of Wheel

The so called "alterable-element method" (AEM) was introduced to deal with the coupling interac-tion of vehicle and sub-structure considering the actual transient jump of wheel, while the classical "contact all along" assumption based on which wheels and lower structure are always contact was abandoned. The alterable element used in this method is a conceptional element, which is used to calculate the coupling interaction of upper and lower structures and has some typical characteristics: firstly it flows along with the moving of contact point; secondly whether it is used for calculation depends on the contact state; thirdly its sizes could change according to specific problems and so on. VISUAL FORTRAN program was coded, and different moving vehicle models were presented taking into consideration the effects of random corrugation in the numerical study. The numerical solutions are favored comparing with the results obtained by alternative methods when there is no jump phenomenon existed. With abrupt irregularity, the transient jump of wheel was studied using the present method.

A method of dealing polygon’s self-intersection contour in SLA

The contour of the slices of SLA parts is composed of a great deal of small lines. When offsetting the contour to compensate for the radius of laser spot, many self-intersection contours come into being, which decrease the precision of formed parts. A new lemma to judge the local self-intersection contour and the global self-intersection contour separately is put forward, according to which self-intersection contour can be removed reliably. Meanwhile, a new beam offsetting algorithm for SLA parts is described, which brings about good resuits in the practical manufacturing process.

Advances in LES of Two-phase Combustion(Ⅱ) LES of Complex Gas-Particle Flows and Coal Combustion

Large-eddy simulation(LES) is under its rapid development and is recognized as a possible second generation of CFD methods used in engineering.Large-eddy simulation of two-phase flows and combustion is particularly important for engineering applications.Some investigators,including the present authors,give their review on LES of spray combustion in gas-turbine combustors and internal combustion engines.However,up to now only a few papers are related to the state-of-the-art on LES of gas-particle flows and combustion.In this paper a review of the advances in LES of complex gas-particle flows and coal combustion is presented.Different sub-grid scale(SGS) stress models and combustion models are described,some of the main results are summarized,and some research needs are discussed.

Effect of Corrosion on the Ship Hull of a Double Hull Very Large Crude Oil Carrier

This study aims to examine and analyze the effect of corrosion wastage on the ship hull of a double hull very large crude oil carrier. To calculate the ultimate bending moment capacity, along with the neutral axis position at the limit state, section modulus, and moment of inertia, the incremental-iterative method is employed. This paper also considered the residual strength checking criteria of ship hull and the ultimate stress behaviors of the representative structural elements. Then, Paik's probabilistic corrosion, which employs two levels of corrosion rate and three different assumptions of coating life time, is applied to assess the corrosion effects. The calculation results obtained through relevant analyses are also presented.