Three extraction methods, ultrasonic assisted extraction (USE), microwave assisted extraction (MSE), and conventional single extraction (CSE), in conjunction with the modified three-stage BCR sequential extraction pro...Three extraction methods, ultrasonic assisted extraction (USE), microwave assisted extraction (MSE), and conventional single extraction (CSE), in conjunction with the modified three-stage BCR sequential extraction procedure (SEP) were applied to examine the contents of Cd, Cu, Cr, Ni, Pb and Zn from lake sediment samples, to know whether these techniques can reduce extraction time and improve reproducibility. The SEP and developed alternative single extrac- tion methods were validated by the analysis of certified reference material BCR 601. By the use of optimized sonication and microwave conditions, steps 1, 2 and 3 of the BCR sequential extraction methods (excluding the hydrogen peroxide digestion in step 3, which was not performed with sonication and microwave) could be completed in 15-30 min and 60- 150 s, respectively. The recoveries of total extractable metal contents in BCR 601, obtained by three single extractions ranged from 93.3%-102%, 88.9%-104% and 81.2%-96.2% for CSE, USE and MSE, respectively. The precision of the single extraction methods was found in the range of 3.7%-9.4% for all metals (n = 6).展开更多
A compressive design and analysis of a turbofan engine is presented in this paper. The components of jet engine have been analyzed based on mechanical design concept. An attempt has been to select materials based on s...A compressive design and analysis of a turbofan engine is presented in this paper. The components of jet engine have been analyzed based on mechanical design concept. An attempt has been to select materials based on sustainability and green design considerations. The energy content (e) of the materials has been one of the parameters for material selection. The choice of material has a substantial impact on cost, manuthcturing process, and the life cycle efficiency. All components nose cone, fan blade, inlet shaft, including compressor has been solid modeled using Siemens NX 11.0 CAD software. The finite element analysis of every component was performed and found safe. A tolerance analysis was performed before assembly of the turbofan engine. A numerical analysis was completed on blade and inlet geometries to determine a more efficient turbofan engine. Thermal analysis was executed oi1 the cone and suitable corrections were made. Finally, the cost and the total energy were estimated to show how much energy is needed to manufacture a turbofan jet engine.展开更多
基金Project supported by the Higher Education Commission of Pakistan (No.Ac-I/GS/963)
文摘Three extraction methods, ultrasonic assisted extraction (USE), microwave assisted extraction (MSE), and conventional single extraction (CSE), in conjunction with the modified three-stage BCR sequential extraction procedure (SEP) were applied to examine the contents of Cd, Cu, Cr, Ni, Pb and Zn from lake sediment samples, to know whether these techniques can reduce extraction time and improve reproducibility. The SEP and developed alternative single extrac- tion methods were validated by the analysis of certified reference material BCR 601. By the use of optimized sonication and microwave conditions, steps 1, 2 and 3 of the BCR sequential extraction methods (excluding the hydrogen peroxide digestion in step 3, which was not performed with sonication and microwave) could be completed in 15-30 min and 60- 150 s, respectively. The recoveries of total extractable metal contents in BCR 601, obtained by three single extractions ranged from 93.3%-102%, 88.9%-104% and 81.2%-96.2% for CSE, USE and MSE, respectively. The precision of the single extraction methods was found in the range of 3.7%-9.4% for all metals (n = 6).
文摘A compressive design and analysis of a turbofan engine is presented in this paper. The components of jet engine have been analyzed based on mechanical design concept. An attempt has been to select materials based on sustainability and green design considerations. The energy content (e) of the materials has been one of the parameters for material selection. The choice of material has a substantial impact on cost, manuthcturing process, and the life cycle efficiency. All components nose cone, fan blade, inlet shaft, including compressor has been solid modeled using Siemens NX 11.0 CAD software. The finite element analysis of every component was performed and found safe. A tolerance analysis was performed before assembly of the turbofan engine. A numerical analysis was completed on blade and inlet geometries to determine a more efficient turbofan engine. Thermal analysis was executed oi1 the cone and suitable corrections were made. Finally, the cost and the total energy were estimated to show how much energy is needed to manufacture a turbofan jet engine.