Active volatile components in drug pair(DP)Herba Ephedrae-Ramulus Cinnamomi(HE-RC),single drug HE and RC were analyzed by gas chromatography/mass spectrometry(GC/MS),chemometric resolution method(CRM)and overall volum...Active volatile components in drug pair(DP)Herba Ephedrae-Ramulus Cinnamomi(HE-RC),single drug HE and RC were analyzed by gas chromatography/mass spectrometry(GC/MS),chemometric resolution method(CRM)and overall volume integration.By means of CRM,the two-dimensional data obtained from GC-MS instruments were resolved into a pure chromatogram and a mass spectrum of each chemical compound.In total,97,62,and 78 volatile chemical components in volatile oil of HE,RC,and DP HE-RC,were respectively determined qualitatively and quantitatively,accounting for 90.08%,91.62%,and 89.76% total contents of volatile oil of HE,RC,and DP HE-RC respectively.It is further demonstrated that the numbers of volatile components of DP HE-RC are almost the sum of those of two single drugs,but some relative contents of them are changed.Some new components,such as 1,6-dimethylhepta-1,3,5-triene,tetracyclo[4.2.1.1(2,5).0(9,10)]deca-3,7-diene,globulol and(E,E)-6,10,14-trimethyl-5,9,13-pentadecatrien-2-one are found in DP HE-RC because of chemical reactions and physical changes during decoction.展开更多
Statistical studies were conducted on the southwest vortex(SWV) during the summers of 2000–13 using high-resolution reanalysis data with a horizontal resolution of 0.5°× 0.5°. A total of 578 SWVs were ...Statistical studies were conducted on the southwest vortex(SWV) during the summers of 2000–13 using high-resolution reanalysis data with a horizontal resolution of 0.5°× 0.5°. A total of 578 SWVs were detected, with a maximum interannual frequency of 55. The variation of the interannual frequency featured a period of around six years. The most active period of SWVs was early July and the maximum occurrence of SWVs appeared in early morning(0200–0800 Beijing Standard Time(BST)). Most of the SWVs were short-lived, with only 66 cases(11.4%) lasting for more than 24 h. In addition, the moving tracks and three-dimensional shape of long-lived(≥ 36 h) SWVs are also presented. For those SWVs that lasted for more than 12 h, four types of SWVs(Types I–IV) were identified using a new method, and the results indicated that the dynamical and thermodynamical conditions before the formation of SWVs are effective indicators of the subsequent evolution of the vortex and associated severe weathers. Moreover, a further level of classification was also constructed for Type II SWVs, which accounted for the largest proportion out of Types I–IV, and the results indicated that the lifespan, radius and maximum 6-h precipitation were all closely related to the intensity of precipitation before the formation of SWVs.展开更多
基金Project (01962502) supported by the Natural Science Foundation of Hunan Province, China
文摘Active volatile components in drug pair(DP)Herba Ephedrae-Ramulus Cinnamomi(HE-RC),single drug HE and RC were analyzed by gas chromatography/mass spectrometry(GC/MS),chemometric resolution method(CRM)and overall volume integration.By means of CRM,the two-dimensional data obtained from GC-MS instruments were resolved into a pure chromatogram and a mass spectrum of each chemical compound.In total,97,62,and 78 volatile chemical components in volatile oil of HE,RC,and DP HE-RC,were respectively determined qualitatively and quantitatively,accounting for 90.08%,91.62%,and 89.76% total contents of volatile oil of HE,RC,and DP HE-RC respectively.It is further demonstrated that the numbers of volatile components of DP HE-RC are almost the sum of those of two single drugs,but some relative contents of them are changed.Some new components,such as 1,6-dimethylhepta-1,3,5-triene,tetracyclo[4.2.1.1(2,5).0(9,10)]deca-3,7-diene,globulol and(E,E)-6,10,14-trimethyl-5,9,13-pentadecatrien-2-one are found in DP HE-RC because of chemical reactions and physical changes during decoction.
基金supported by a project of the Chengdu Institute of Plateau Meteorology, CMA (Grant No. LPM2011006)the State Grid Science & Technology Project (GC71-13-007)the National Natural Science Foundation of China (Grant Nos. 41205027, 41375053, and 41375058)
文摘Statistical studies were conducted on the southwest vortex(SWV) during the summers of 2000–13 using high-resolution reanalysis data with a horizontal resolution of 0.5°× 0.5°. A total of 578 SWVs were detected, with a maximum interannual frequency of 55. The variation of the interannual frequency featured a period of around six years. The most active period of SWVs was early July and the maximum occurrence of SWVs appeared in early morning(0200–0800 Beijing Standard Time(BST)). Most of the SWVs were short-lived, with only 66 cases(11.4%) lasting for more than 24 h. In addition, the moving tracks and three-dimensional shape of long-lived(≥ 36 h) SWVs are also presented. For those SWVs that lasted for more than 12 h, four types of SWVs(Types I–IV) were identified using a new method, and the results indicated that the dynamical and thermodynamical conditions before the formation of SWVs are effective indicators of the subsequent evolution of the vortex and associated severe weathers. Moreover, a further level of classification was also constructed for Type II SWVs, which accounted for the largest proportion out of Types I–IV, and the results indicated that the lifespan, radius and maximum 6-h precipitation were all closely related to the intensity of precipitation before the formation of SWVs.
