1420铝锂合金回归再回火析出δ′相行为

采用小角 X射线散射技术研究了回归再回火处理 1 42 0铝锂合金 δ′相的形成和粗化 .结果表明 ,再回火 5h析出的 δ′相与基体之间存在过渡区 ,该过渡区经再回火 48h处理后消失 ;之后

Diffusion bonding of Al 7075 and Mg AZ31 alloys:Process parameters, microstructural analysis and mechanical properties

Al 7075 and Mg AZ31 alloys were joined by diffusion bonding method. Joining process was performed in pressure range of 10-35 MPa at temperatures of 430-450 ℃ for 60 min under a vacuum of 13.3 MPa. The microstructure evaluation, phase analysis and distribution of elements at the interface were done using scanning electron microscopy （SEM）, energy-dispersive X-ray spectroscopy （EDS） and X-ray diffraction （XRD）. The pressure of 25 MPa was determined as the optimum pressure in which the minimum amount of plastic deformation takes place at the joint. Different reaction layers containing intermetallic compounds, such as Al12Mg17, Al3Mg2 andα（Al） solid solution, were observed, in interfacial transition zone （ITZ）. Thickness of layers was increased with increasing the operating temperature. According to the results, diffusion of aluminum atoms into magnesium alloy was more and the interface movement towards the Al alloy was observed. The maximum bond strength of 38 MPa was achieved at the temperature of 440 ℃ and pressure of 25 MPa. Fractography studies indicated that the brittle fracture originated from Al3Mg2 phase.

Experimental study on the shear behavior of grout-infilled specimens and micromechanical properties of grout-rock interface

The grout-rock interfacial property is one of the key factors associated with the strength of grouted rock masses.In this study,direct shear tests and nanoindentation tests were adopted to investigate the mechanical properties of the grout-rock interface at both the macroscale and microscale.The cohesion of the cement specimens was higher than that of the grout-infilled joint specimens,while their internal friction angle was lower than that of the grout-infilled joint specimens.A“separation method”for identifying the different phases according to the qualitative and quantitative estimations was introduced,and the irregular interfacial transition zone(ITZ)thickness and elastic modulus were estimated.The ITZ thickness of the grout-infilled sandstone specimen ranged from 0 to 30μm,whereas it was within the range of 10-40μm for the grout-infilled mudstone specimen.The average elastic modulus of the ITZ in grout-infilled sandstone and mudstone specimens was approximately 58.2%and 54.1%lower than that of the bulk grout,respectively.Regarding the incidence of the rock type,the interlacing between the grout and sandstone was better developed.The ITZ with a higher porosity and lower modulus had a significant effect on the mechanical properties of the grout-infilled specimens.

Improving performance of recycled aggregate concrete with superfine pozzolanic powders

Phosphorous slag （PHS）, ground granulated blast-furnace slag （GGBS） and fly ash （FA） were used as replacements of Portland cement to modify the microstruc^xe of recycled aggregate concrete （RAC）. A new manufacturing method named ＂W3T4＂ was proposed to improve the performances of interracial transition zone （ITZ） between recycled aggregate and mortar. The mechanical properties and the durability of RAC were tested, which show that this new manufacturing method improves the properties of RAC, and the GGBS with finest size makes a great contribution to the performance of RAC due to its better filling effect and much earlier pozzolanic reaction. Combined with GGBS, the effects of PHS on the retardation of setting time can be alleviated and the synergistic effect helps to make a more compact RAC. For the RAC with 25% of the recycled aggregate （RA） replacement and 10% PHS ＋ 10% GGBS additives, the compressive strength increases by 25.4%, but the permeability decreases by 64.3% with respect to the reference concrete made with nature aggregates. The micro-mechanisms of these improvements were investigated by the scanning electron microscope （SEM）. The SEM images show that the new manufacturing method, adding superfine pozzolanic powders and super-plasticizer benefits, makes a much denser ITZ in RAC.

Bonding between Aggregates and Cement Pastes in Concrete

This investigation was carried out to study the effect of aggregate roughness on ITZ （interfacial transition zone） at same water/cement ratio and the influence of silica fume on the bond strength. On the experimental side, two types of aggregates （limestone and granite） were used, which were prepared with broken surface. Cement （Type I） was used with same w/c ratio for all batches. In order to study the effect of silica fume on the bond, the same mixes were produced with 8% silica fume. Three different tests were performed： ＂pull a part＂, Brazilian test and compressive strength test. The specimens for Brazilian and compressive strength were tested after 28 days, while the ＂pull a part＂ specimens were tested after 29 days. The result showed that the bond strength is influenced by the surface roughness of aggregate. For the same mix, limestone recorded higher bond strength than granite. Moreover, the bond strength is increased by adding the silica fume.

Numerical calculation and influencing factors of the volume fraction of interfacial transition zone in concrete

The determination of volume fraction of interracial transition zone （ITZ） is very important for investigating the quantitative relationship between the microstructure and macroscopical property of concrete. In this paper, based on Lu and Torquato＇s most nearest surface distribution function, a calculating process of volume fraction of ITZ is given in detail according to the actual sieve curve in concrete. Then, quantitative formulas are put forward to measure the influencing factors on the ｜TZ vol- ume fraction. In order to validate the given model, the volume fractions of ITZ obtained by numerical calculation are compared with those by computer simulation. The results show that the two are in good agreement. The order of the factors influencing the ITZ volume fraction is the ITZ thickness, the volume fraction of aggregate and the maximum aggregate diameter for Fuller gradation in turn. The 1TZ volume fraction obtained from the equal volume fraction （EVF） gradation is always larger than that from the Fuller gradation for a given volume fraction of aggregate.