The segregation of Sn and discontinuous precipitation at grain boundaries are detrimental to the strength,ductility,and machinability of the Cu−Ni−Sn alloy.A strategy to solve the above problems is multi-component com...The segregation of Sn and discontinuous precipitation at grain boundaries are detrimental to the strength,ductility,and machinability of the Cu−Ni−Sn alloy.A strategy to solve the above problems is multi-component composition design by introducing strong enthalpic interaction element.In this work,a series of Cu_(80)Ni_(15)Sn_(5−x)Ti_(x)(at.%)alloys were designed by cluster-plus-glue-atom model,and the effects of Ti content on the microstructure and properties of the alloys were systematically investigated using TEM and other analysis methods.The results demonstrate that Ti can effectively inhibit the segregation and discontinuous precipitation while promoting continuous precipitation to improve the high-temperature stability of the alloys.As the Ti content increases,the distribution of Ti changes from uniform distribution to predominant precipitation.The hardness and conductivity of the alloy exceed those of the C72900(Cu−15Ni−8Sn(wt.%))commercial alloy and the Cu_(80)Ni_(15)Sn_(5)(at.%)reference alloy when Ti is in the solution state.展开更多
Ni-based alloy was transient liquid phase bonded using a BNi-2 interlayer. The effect of bonding parameters on the microstructures and mechanical properties of the joints was investigated. With the increase of bonding...Ni-based alloy was transient liquid phase bonded using a BNi-2 interlayer. The effect of bonding parameters on the microstructures and mechanical properties of the joints was investigated. With the increase of bonding temperature or time, the number of Ni-rich and Cr-rich borides and the grain size of precipitation zone decrease. Higher bonding temperature or longer bonding time is beneficial to the diffusion of melting point depressant elements (B and Si) from the PZ to the base metal and atomic interdiffusion between the base metal and the joint. The chemical composition and microstructure of the joints bonded at 1170 ℃ for 24 h are comparable to the base metal. The shear test results show that both the room and elevated temperature shear-strengths of the joints increase with increasing bonding time. However, the effect of bonding time on elevated temperature tensile-shear strength is greater than on room temperature tensile-shear strength.展开更多
This paper introduces a novel digital transceiver for the cordless telephone zero (CT0) standard,which uses a digital modulation and demodulation technique to handle the signal instead of the traditional analog meth...This paper introduces a novel digital transceiver for the cordless telephone zero (CT0) standard,which uses a digital modulation and demodulation technique to handle the signal instead of the traditional analog meth-od. In the transmitter,a fractional-N phase locked loop (PLL) is utilized to realize the continuous phase frequency shift key (CPFSK) modulation,and a 2 Ts raised cosine (2RC) shaping technique is used to reduce the occupied bandwidth. In the receiver,a novel digital method is proposed to demodulate the 2RC CPFSK signal. This chip is fabricated using an SMIC 0.35μm mixed signal CMOS process with a die size of 2mm × 2mm. With an external low noise amplifier (LNA),the sensitivity of the chip is better than -103dBm.展开更多
A model of continuous-time insider trading in which a risk-neutral in-sider possesses two imperfect correlated signals of a risky asset is studied.By conditional expectation theory and filtering theory,we first establ...A model of continuous-time insider trading in which a risk-neutral in-sider possesses two imperfect correlated signals of a risky asset is studied.By conditional expectation theory and filtering theory,we first establish three lemmas:normal corre-lation,equivalent pricing and equivalent profit,which can guarantee to turn our model into a model with insider knowing full information.Then we investigate the impact of the two correlated signals on the market equilibrium consisting of optimal insider trading strategy and semi-strong pricing rule.It shows that in the equilibrium,(1)the market depth is constant over time;(2)if the two noisy signals are not linerly correlated,then all private information of the insider is incorporated into prices in the end while the whole information on the asset value can not incorporated into prices in the end;(3)if the two noisy signals are linear correlated such that the insider can infer the whole information of the asset value,then our model turns into a model with insider knowing full information;(4)if the two noisy signals are the same then the total ex ant profit of the insider is increasing with the noise decreasing,while down to O as the noise going up to infinity;(5)if the two noisy signals are not linear correlated then with one noisy signal fixed,the total ex ante profit of the insider is single-peaked with a unique minimum with respect to the other noisy signal value,and furthermore as the noisy value going to O it gets its maximum,the profit in the case that the real value is observed.展开更多
Cu-4.7%Sn (mass fraction) alloy plate was prepared by the self-developed two-phase zone continuous casting (TZCC) process. The relationship between process parameters of TZCC and surface quality of the alloy plate...Cu-4.7%Sn (mass fraction) alloy plate was prepared by the self-developed two-phase zone continuous casting (TZCC) process. The relationship between process parameters of TZCC and surface quality of the alloy plate was investigated. The microstructure and mechanical properties of the TZCC alloy plate were analyzed. The results show that Cu-4.7%Sn alloy plate with smooth surface can be obtained by means of reasonable matching the entrance temperature of two-phase zone mold and the continuous casting speed. The microstructure of the TZCC alloy is composed of grains-covered grains, small grains with self-closed grain boundaries, columnar grains and equiaxed grains. Compared with cold mold continuous casting Cu-4.7%Sn alloy plate, the room temperature tensile strength and ductility of the TZCC alloy plate are greatly improved.展开更多
In this paper, direct sequence spread spectrum multiple access (DS/SSMA) communication system employing serially concatenated trellis coded modulation (TCM) and continuous phase modulation (CPM) over flat Rayleigh fa...In this paper, direct sequence spread spectrum multiple access (DS/SSMA) communication system employing serially concatenated trellis coded modulation (TCM) and continuous phase modulation (CPM) over flat Rayleigh fading channel are presented. The performance of this concatenated TCM/CPM DS/SSMA system is exploited by the theoretical analysis and numerical simulations. The results demonstrate that significant improvements in error probability of this DS/SSMA system over the system with single TCM or CPM of different modulation indices can be achieved under the same conditions.展开更多
To determine the feasibility and practicability of interrupt continuous wave (CW) approach proposed for real time simulating radar intermediate frequency(IF) video signal, theoretical analysis and computer simulation...To determine the feasibility and practicability of interrupt continuous wave (CW) approach proposed for real time simulating radar intermediate frequency(IF) video signal, theoretical analysis and computer simulation were used. Phases at two linked points between the end and beginning of adjoined frames are always consistent; the bias Doppler frequency for the time delay of A/D sampling start responds to that for target acceleration. No digital phase compensation is required at continuous points, and the interrupt CW approach has apparently practical values.展开更多
Aim To develop a high speed and high resolution dynamic rangefinding device for the measurement of large distances.Methods The device was comprised of an ultrasonic transmitter and a receiver,and a receiver , and a co...Aim To develop a high speed and high resolution dynamic rangefinding device for the measurement of large distances.Methods The device was comprised of an ultrasonic transmitter and a receiver,and a receiver , and a continuous ultrasonic wave amplitude-modulated by a low- frequency acoustic signal was used. The rangefinding was achieved by detecting the phase difference between the transmitted and received ultrasonic signals. The design principle. hard- ware implementation , experimental results and performance analysis of the device are included. Results and Conclusion Experiments show that the accuracy of the device are included. within 1.5m while its dynamic data update rate can be up to 40kHz.展开更多
To study actions of the genes associated with tight junction, adherent junction, focal adhesion, and gap junction during liver regeneration (LR), these genes were obtained by collecting data from databases and thesi...To study actions of the genes associated with tight junction, adherent junction, focal adhesion, and gap junction during liver regeneration (LR), these genes were obtained by collecting data from databases and thesis, and their expression profiles in rat regenerating liver were detected employing Rat Genome 230 2.0 array. Next the LR-associated genes were identified by comparing the difference between sham operation (SO) and partial hepatectomy (PH) groups. 79, 53, 109, 53 genes involved in the above four junctions were found to be LR-associated. The initial and total expression numbers of these genes occurring in the initial phase of LR, G0/G1, cell proliferation, cell differentiation, and structure-functional rebuilding were 124, 43, 122, 10, and 249, 145, 957, 306, respectively, illustrating that genes were initi^ly expressed mainly in the initiation stage, and functioned in different phases. Up-regulation-and down-regulation to a total of 972 and 540 times, as well as, 41 types of expression patterns showed that the physiological and biochemical activities were diverse and complicated in LR. According to the data, there was an increase in the forepart and prophase, but a decrease in late-metaphase and anaphase for gap junction assembly. Focal adhesion formation displayed an enhancement in forepart, prophase, and anaphase; and formation of tight junctions and adherent junctions last throughout the LR.展开更多
Microstructure and creep properties of AZ61 alloy containing 1 and 3 wt.% Ca were investigated. The creep properties were examined using impression method under different stresses between 200 and 500 MPa at the temper...Microstructure and creep properties of AZ61 alloy containing 1 and 3 wt.% Ca were investigated. The creep properties were examined using impression method under different stresses between 200 and 500 MPa at the temperature ranging from 423 to 491 K. The microstructure of AZ61 alloy contains α(Mg) matrix and Mg17 Al12 intermetallic phases. It is shown that adding Ca to AZ61 alloy reduces the amount of Mg17 Al12 phase via forming(Mg,Al)2 Ca phase;furthermore, increasing the Ca content to 3 wt.% leads to the formation of(Mg,Al)2 Ca phase, as well as the elimination of the Mg17 Al12 phase. Creep properties of AZ61 alloy are improved with the Ca addition. The improvement in creep properties is attributed to the reduction in the amount of Mg17 Al12 phase and the formation of(Mg,Al)2 Ca phase with high thermal stability. According to the obtained creep data, it is concluded that the pipe diffusion-climb controlled dislocation creep is the dominant creep mechanism and Ca addition has no influence on this mechanism. The effect of pre-deformation on the creep properties of AZ61+3%Ca alloy reveals that the creep resistance of the alloy depends on the continuity of(Mg,Al)2 Ca phase. It is decreased by reducing the phase continuity.展开更多
The hydrothermal reaction of ZnO, H3PO4(85%), (H2NCH2CH2)2NH and H2pydc results in the formation of a discrete mononuclear zinc(II) complex Zn(Hpydc)2(H2O). It crystallizes in monoclinic space group C2/c with a = 17.9...The hydrothermal reaction of ZnO, H3PO4(85%), (H2NCH2CH2)2NH and H2pydc results in the formation of a discrete mononuclear zinc(II) complex Zn(Hpydc)2(H2O). It crystallizes in monoclinic space group C2/c with a = 17.9947(8), b = 7.1875(3), c = 12.5895(4) , b = 110.802(2), V = 1522.14(10) 3, Z = 4, Mr = 415.61, (C14H10N2O9Zn), Dc = 1.814g/cm3, = 16.71cm-1, F(000) = 840, R = 0.0505, wR = 0.1144. Each zinc(II) is coordinated to two nitrogen and three oxygen atoms of which two nitrogen and two oxygen atoms are from two pydc ligands, and one oxygen atom from the coordinated water molecule to form an irregular polyhedral geometry. The complex is linked further into a three-dimensional structure through the weak interactions of hydrogen bonds between the two oxygen atoms. IR spectrum of the complex is also discussed.展开更多
In order to investigate the microstructure evolution and gain complete isothermal solidification time, transient liquid phase (TLP) bonding of IN-738LC superalloy was carried out using powdered AMS 4777 as the fille...In order to investigate the microstructure evolution and gain complete isothermal solidification time, transient liquid phase (TLP) bonding of IN-738LC superalloy was carried out using powdered AMS 4777 as the filler metal. The influence of gap size and bonding time on the joints was investigated. For example, complete isothermal solidification time for 40μm gap size was obtained as 45 min. In the case of lack of completion of isothermal solidification step, the remained molten interlayer cooled in the bonding zone under non-equilibrium condition andγ–γ′ eutectic phase formed in that area. The relationship between gap size and holding time was not linear. With the increase in gap size, eutectic phase width became thicker. In the diffusion affected zone, a much larger amount of alloying elements were observed reaching a peak. These peaks might be due to the formation of boride or silicide intermetallic. With the increase in gap size, the time required for bonding will increase, so the alloying elements have more time for diffusion and distribution in farther areas. As a result, concentrations of alloying elements decreased slightly with the increase in the gap size. The present bi-phasic model did not properly predict the complete isothermal solidification time for IN-738LC-AMS 4777-IN-738LC TLP bonding system.展开更多
A reduced state Soft Input Soft Output (SISO) a posteriori probability algorithm for Seri-ally Concatenated Continuous Phase Modulation (SCCPM) is proposed in this paper. Based on the Reduced State Sequence Detection ...A reduced state Soft Input Soft Output (SISO) a posteriori probability algorithm for Seri-ally Concatenated Continuous Phase Modulation (SCCPM) is proposed in this paper. Based on the Reduced State Sequence Detection (RSSD),it has more general form compared with other reduced state SISO algorithms. The proposed algorithm can greatly reduce the state number,thus leads to the computation complexity reduction. It also minimizes the degradation in Euclidean distance with decision feedback in the reduced state trellis. Analysis and simulation results show that the perform-ance degradation is little with proper reduction scheme.展开更多
Fatigue properties of Al7075-T6 alloy joined by temperature gradient transient liquid phase(TGTLP) diffusion bonding using liquid gallium interlayer was investigated. The fatigue specimen was jointed at 460 °C un...Fatigue properties of Al7075-T6 alloy joined by temperature gradient transient liquid phase(TGTLP) diffusion bonding using liquid gallium interlayer was investigated. The fatigue specimen was jointed at 460 °C under 10 MPa pressure for 10 min. The TLP bonded samples were homogenized at 465 °C for 2 h and then T6-heat treated. The fatigue life of Al7075-T6 alloy was determined as 107 cycles under 90 MPa while the fatigue life of TLP bonded sample under this stress amplitude was 1.2×106 cycles, which is about 10% of the total Al7075 alloy fatigue life. The fatigue fracture surfaces of Al7075 sample and TGTLP bonded sample were studied using scanning electron microscope to characterize the nucleation sites and crack growth stages in both samples.展开更多
Transient liquid phase bonding of two dissimilar alloys Al 2024 and Ti?6Al?4V using Cu?22%Zn interlayer was carried out at 510 °C under vacuum of 0.01 Pa for various bonding time. In order to characterize the mic...Transient liquid phase bonding of two dissimilar alloys Al 2024 and Ti?6Al?4V using Cu?22%Zn interlayer was carried out at 510 °C under vacuum of 0.01 Pa for various bonding time. In order to characterize the microstructure evolution in the joint zone, scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) and X-ray diffraction (XRD) were applied. The results show that joint formation is attributed to the solid-state diffusion of Cu and Zn into Ti?6Al?4V and Al 2024 alloys followed by eutectic formation and isothermal solidification along the Cu?Zn/Al 2024 interface. The hardness of the joints at the interface increases with an increase in bonding time which can be attributed to formation of intermetallic compounds such as Al2Cu, TiCu3, Al4.2Cu3.2Zn0.7, Al0.71Zn0.29, Ti2Cu, TiAl3 and TiZn16 in the joint zone. Moreover, shear strength of the joint reaches the highest value of 37 MPa at bonding time of 60 min.展开更多
Isothermal solidification process of a dissimilar transient liquid phase (TLP) bonding of FSX-414/MBF80/IN738 system was simulated by finite difference method. The TLP joint model was divided into two parts and a mo...Isothermal solidification process of a dissimilar transient liquid phase (TLP) bonding of FSX-414/MBF80/IN738 system was simulated by finite difference method. The TLP joint model was divided into two parts and a moving liquid /solid interface model was used for the parts. Diffusion equations were solved for each half of the joints simultaneously up to the end of isothermal solidification. The completion time of isothermal solidification, concentration profiles and position of the solid/liquid interface for each half were calculated. The intersection of the solid/liquid interfaces of two halves was considered the end of isothermal solidification. To obtain some required diffusion data, TLP bonding of FSX-414/MBF80/IN738 was performed at different temperature and time under vacuum atmosphere. The calculated results show good agreement with the experimental results.展开更多
For the modified demodulation arithmetic of 3×3 coupler, the processing software built on the basis of Labview is able to demodulate asymmetric 3×3 coupler signal and do further spectrum analysis. It shows t...For the modified demodulation arithmetic of 3×3 coupler, the processing software built on the basis of Labview is able to demodulate asymmetric 3×3 coupler signal and do further spectrum analysis. It shows that the measured frequency ranges from 10 Hz to 1 000 Hz and phase range is covered by -10 rad^10 rad. The phase sensitivity is 0.5 V/rad. This system is proved to show high resolution and wide dynamic range.展开更多
基金support from the National Natural Science Foundation of China(No.52071052).
文摘The segregation of Sn and discontinuous precipitation at grain boundaries are detrimental to the strength,ductility,and machinability of the Cu−Ni−Sn alloy.A strategy to solve the above problems is multi-component composition design by introducing strong enthalpic interaction element.In this work,a series of Cu_(80)Ni_(15)Sn_(5−x)Ti_(x)(at.%)alloys were designed by cluster-plus-glue-atom model,and the effects of Ti content on the microstructure and properties of the alloys were systematically investigated using TEM and other analysis methods.The results demonstrate that Ti can effectively inhibit the segregation and discontinuous precipitation while promoting continuous precipitation to improve the high-temperature stability of the alloys.As the Ti content increases,the distribution of Ti changes from uniform distribution to predominant precipitation.The hardness and conductivity of the alloy exceed those of the C72900(Cu−15Ni−8Sn(wt.%))commercial alloy and the Cu_(80)Ni_(15)Sn_(5)(at.%)reference alloy when Ti is in the solution state.
基金Projects (50975062, 51105107, 51275135, 51021002) supported by the National Natural Science Foundation of ChinaProject (QC2011C044) supported by the Natural Science Foundation of Heilongjiang Province, China+1 种基金Project (20112302130005) supported by Specialized Research Fund for the Doctoral Program of Higher Education, ChinaProject (20100471027) supported by the Postdoctoral Science Foundation of China
文摘Ni-based alloy was transient liquid phase bonded using a BNi-2 interlayer. The effect of bonding parameters on the microstructures and mechanical properties of the joints was investigated. With the increase of bonding temperature or time, the number of Ni-rich and Cr-rich borides and the grain size of precipitation zone decrease. Higher bonding temperature or longer bonding time is beneficial to the diffusion of melting point depressant elements (B and Si) from the PZ to the base metal and atomic interdiffusion between the base metal and the joint. The chemical composition and microstructure of the joints bonded at 1170 ℃ for 24 h are comparable to the base metal. The shear test results show that both the room and elevated temperature shear-strengths of the joints increase with increasing bonding time. However, the effect of bonding time on elevated temperature tensile-shear strength is greater than on room temperature tensile-shear strength.
文摘This paper introduces a novel digital transceiver for the cordless telephone zero (CT0) standard,which uses a digital modulation and demodulation technique to handle the signal instead of the traditional analog meth-od. In the transmitter,a fractional-N phase locked loop (PLL) is utilized to realize the continuous phase frequency shift key (CPFSK) modulation,and a 2 Ts raised cosine (2RC) shaping technique is used to reduce the occupied bandwidth. In the receiver,a novel digital method is proposed to demodulate the 2RC CPFSK signal. This chip is fabricated using an SMIC 0.35μm mixed signal CMOS process with a die size of 2mm × 2mm. With an external low noise amplifier (LNA),the sensitivity of the chip is better than -103dBm.
文摘A model of continuous-time insider trading in which a risk-neutral in-sider possesses two imperfect correlated signals of a risky asset is studied.By conditional expectation theory and filtering theory,we first establish three lemmas:normal corre-lation,equivalent pricing and equivalent profit,which can guarantee to turn our model into a model with insider knowing full information.Then we investigate the impact of the two correlated signals on the market equilibrium consisting of optimal insider trading strategy and semi-strong pricing rule.It shows that in the equilibrium,(1)the market depth is constant over time;(2)if the two noisy signals are not linerly correlated,then all private information of the insider is incorporated into prices in the end while the whole information on the asset value can not incorporated into prices in the end;(3)if the two noisy signals are linear correlated such that the insider can infer the whole information of the asset value,then our model turns into a model with insider knowing full information;(4)if the two noisy signals are the same then the total ex ant profit of the insider is increasing with the noise decreasing,while down to O as the noise going up to infinity;(5)if the two noisy signals are not linear correlated then with one noisy signal fixed,the total ex ante profit of the insider is single-peaked with a unique minimum with respect to the other noisy signal value,and furthermore as the noisy value going to O it gets its maximum,the profit in the case that the real value is observed.
基金Project(51374025) supported by the National Natural Science Foundation of ChinaProject(2014Z-05) supported by the State Key Laboratory for Advanced Metals and Materials,University of Science and Technology Beijing,ChinaProject(2152020) supported by the Beijing Natural Science Foundation,China
文摘Cu-4.7%Sn (mass fraction) alloy plate was prepared by the self-developed two-phase zone continuous casting (TZCC) process. The relationship between process parameters of TZCC and surface quality of the alloy plate was investigated. The microstructure and mechanical properties of the TZCC alloy plate were analyzed. The results show that Cu-4.7%Sn alloy plate with smooth surface can be obtained by means of reasonable matching the entrance temperature of two-phase zone mold and the continuous casting speed. The microstructure of the TZCC alloy is composed of grains-covered grains, small grains with self-closed grain boundaries, columnar grains and equiaxed grains. Compared with cold mold continuous casting Cu-4.7%Sn alloy plate, the room temperature tensile strength and ductility of the TZCC alloy plate are greatly improved.
文摘In this paper, direct sequence spread spectrum multiple access (DS/SSMA) communication system employing serially concatenated trellis coded modulation (TCM) and continuous phase modulation (CPM) over flat Rayleigh fading channel are presented. The performance of this concatenated TCM/CPM DS/SSMA system is exploited by the theoretical analysis and numerical simulations. The results demonstrate that significant improvements in error probability of this DS/SSMA system over the system with single TCM or CPM of different modulation indices can be achieved under the same conditions.
文摘To determine the feasibility and practicability of interrupt continuous wave (CW) approach proposed for real time simulating radar intermediate frequency(IF) video signal, theoretical analysis and computer simulation were used. Phases at two linked points between the end and beginning of adjoined frames are always consistent; the bias Doppler frequency for the time delay of A/D sampling start responds to that for target acceleration. No digital phase compensation is required at continuous points, and the interrupt CW approach has apparently practical values.
文摘Aim To develop a high speed and high resolution dynamic rangefinding device for the measurement of large distances.Methods The device was comprised of an ultrasonic transmitter and a receiver,and a receiver , and a continuous ultrasonic wave amplitude-modulated by a low- frequency acoustic signal was used. The rangefinding was achieved by detecting the phase difference between the transmitted and received ultrasonic signals. The design principle. hard- ware implementation , experimental results and performance analysis of the device are included. Results and Conclusion Experiments show that the accuracy of the device are included. within 1.5m while its dynamic data update rate can be up to 40kHz.
基金the National Basic Research 973 Pre-research Program of China (No. 2006CB708506).
文摘To study actions of the genes associated with tight junction, adherent junction, focal adhesion, and gap junction during liver regeneration (LR), these genes were obtained by collecting data from databases and thesis, and their expression profiles in rat regenerating liver were detected employing Rat Genome 230 2.0 array. Next the LR-associated genes were identified by comparing the difference between sham operation (SO) and partial hepatectomy (PH) groups. 79, 53, 109, 53 genes involved in the above four junctions were found to be LR-associated. The initial and total expression numbers of these genes occurring in the initial phase of LR, G0/G1, cell proliferation, cell differentiation, and structure-functional rebuilding were 124, 43, 122, 10, and 249, 145, 957, 306, respectively, illustrating that genes were initi^ly expressed mainly in the initiation stage, and functioned in different phases. Up-regulation-and down-regulation to a total of 972 and 540 times, as well as, 41 types of expression patterns showed that the physiological and biochemical activities were diverse and complicated in LR. According to the data, there was an increase in the forepart and prophase, but a decrease in late-metaphase and anaphase for gap junction assembly. Focal adhesion formation displayed an enhancement in forepart, prophase, and anaphase; and formation of tight junctions and adherent junctions last throughout the LR.
文摘Microstructure and creep properties of AZ61 alloy containing 1 and 3 wt.% Ca were investigated. The creep properties were examined using impression method under different stresses between 200 and 500 MPa at the temperature ranging from 423 to 491 K. The microstructure of AZ61 alloy contains α(Mg) matrix and Mg17 Al12 intermetallic phases. It is shown that adding Ca to AZ61 alloy reduces the amount of Mg17 Al12 phase via forming(Mg,Al)2 Ca phase;furthermore, increasing the Ca content to 3 wt.% leads to the formation of(Mg,Al)2 Ca phase, as well as the elimination of the Mg17 Al12 phase. Creep properties of AZ61 alloy are improved with the Ca addition. The improvement in creep properties is attributed to the reduction in the amount of Mg17 Al12 phase and the formation of(Mg,Al)2 Ca phase with high thermal stability. According to the obtained creep data, it is concluded that the pipe diffusion-climb controlled dislocation creep is the dominant creep mechanism and Ca addition has no influence on this mechanism. The effect of pre-deformation on the creep properties of AZ61+3%Ca alloy reveals that the creep resistance of the alloy depends on the continuity of(Mg,Al)2 Ca phase. It is decreased by reducing the phase continuity.
基金the National Natural Science Foundation of China the Natural Science Foundation of Fujian Provincea key project from the Chinese Academic of Sciences.
文摘The hydrothermal reaction of ZnO, H3PO4(85%), (H2NCH2CH2)2NH and H2pydc results in the formation of a discrete mononuclear zinc(II) complex Zn(Hpydc)2(H2O). It crystallizes in monoclinic space group C2/c with a = 17.9947(8), b = 7.1875(3), c = 12.5895(4) , b = 110.802(2), V = 1522.14(10) 3, Z = 4, Mr = 415.61, (C14H10N2O9Zn), Dc = 1.814g/cm3, = 16.71cm-1, F(000) = 840, R = 0.0505, wR = 0.1144. Each zinc(II) is coordinated to two nitrogen and three oxygen atoms of which two nitrogen and two oxygen atoms are from two pydc ligands, and one oxygen atom from the coordinated water molecule to form an irregular polyhedral geometry. The complex is linked further into a three-dimensional structure through the weak interactions of hydrogen bonds between the two oxygen atoms. IR spectrum of the complex is also discussed.
文摘In order to investigate the microstructure evolution and gain complete isothermal solidification time, transient liquid phase (TLP) bonding of IN-738LC superalloy was carried out using powdered AMS 4777 as the filler metal. The influence of gap size and bonding time on the joints was investigated. For example, complete isothermal solidification time for 40μm gap size was obtained as 45 min. In the case of lack of completion of isothermal solidification step, the remained molten interlayer cooled in the bonding zone under non-equilibrium condition andγ–γ′ eutectic phase formed in that area. The relationship between gap size and holding time was not linear. With the increase in gap size, eutectic phase width became thicker. In the diffusion affected zone, a much larger amount of alloying elements were observed reaching a peak. These peaks might be due to the formation of boride or silicide intermetallic. With the increase in gap size, the time required for bonding will increase, so the alloying elements have more time for diffusion and distribution in farther areas. As a result, concentrations of alloying elements decreased slightly with the increase in the gap size. The present bi-phasic model did not properly predict the complete isothermal solidification time for IN-738LC-AMS 4777-IN-738LC TLP bonding system.
基金Supported by NSFC & Microsoft Asia (60372048)China TRAPOYT, NSFC key project (60496316)+2 种基金863 Project (2005AA123910)RFDP (20050701007)MOE Key Project (104171).
文摘A reduced state Soft Input Soft Output (SISO) a posteriori probability algorithm for Seri-ally Concatenated Continuous Phase Modulation (SCCPM) is proposed in this paper. Based on the Reduced State Sequence Detection (RSSD),it has more general form compared with other reduced state SISO algorithms. The proposed algorithm can greatly reduce the state number,thus leads to the computation complexity reduction. It also minimizes the degradation in Euclidean distance with decision feedback in the reduced state trellis. Analysis and simulation results show that the perform-ance degradation is little with proper reduction scheme.
文摘Fatigue properties of Al7075-T6 alloy joined by temperature gradient transient liquid phase(TGTLP) diffusion bonding using liquid gallium interlayer was investigated. The fatigue specimen was jointed at 460 °C under 10 MPa pressure for 10 min. The TLP bonded samples were homogenized at 465 °C for 2 h and then T6-heat treated. The fatigue life of Al7075-T6 alloy was determined as 107 cycles under 90 MPa while the fatigue life of TLP bonded sample under this stress amplitude was 1.2×106 cycles, which is about 10% of the total Al7075 alloy fatigue life. The fatigue fracture surfaces of Al7075 sample and TGTLP bonded sample were studied using scanning electron microscope to characterize the nucleation sites and crack growth stages in both samples.
文摘Transient liquid phase bonding of two dissimilar alloys Al 2024 and Ti?6Al?4V using Cu?22%Zn interlayer was carried out at 510 °C under vacuum of 0.01 Pa for various bonding time. In order to characterize the microstructure evolution in the joint zone, scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) and X-ray diffraction (XRD) were applied. The results show that joint formation is attributed to the solid-state diffusion of Cu and Zn into Ti?6Al?4V and Al 2024 alloys followed by eutectic formation and isothermal solidification along the Cu?Zn/Al 2024 interface. The hardness of the joints at the interface increases with an increase in bonding time which can be attributed to formation of intermetallic compounds such as Al2Cu, TiCu3, Al4.2Cu3.2Zn0.7, Al0.71Zn0.29, Ti2Cu, TiAl3 and TiZn16 in the joint zone. Moreover, shear strength of the joint reaches the highest value of 37 MPa at bonding time of 60 min.
文摘Isothermal solidification process of a dissimilar transient liquid phase (TLP) bonding of FSX-414/MBF80/IN738 system was simulated by finite difference method. The TLP joint model was divided into two parts and a moving liquid /solid interface model was used for the parts. Diffusion equations were solved for each half of the joints simultaneously up to the end of isothermal solidification. The completion time of isothermal solidification, concentration profiles and position of the solid/liquid interface for each half were calculated. The intersection of the solid/liquid interfaces of two halves was considered the end of isothermal solidification. To obtain some required diffusion data, TLP bonding of FSX-414/MBF80/IN738 was performed at different temperature and time under vacuum atmosphere. The calculated results show good agreement with the experimental results.
文摘For the modified demodulation arithmetic of 3×3 coupler, the processing software built on the basis of Labview is able to demodulate asymmetric 3×3 coupler signal and do further spectrum analysis. It shows that the measured frequency ranges from 10 Hz to 1 000 Hz and phase range is covered by -10 rad^10 rad. The phase sensitivity is 0.5 V/rad. This system is proved to show high resolution and wide dynamic range.