Microstructural evolution and dynamic recrystallization(DRX)mechanisms of a Ti-48Al-2Cr-2Nb(at.%)alloy prepared by selective electron beam melting(SEBM)during hot deformation at 1150℃and 0.1 s^(-1)were investigated b...Microstructural evolution and dynamic recrystallization(DRX)mechanisms of a Ti-48Al-2Cr-2Nb(at.%)alloy prepared by selective electron beam melting(SEBM)during hot deformation at 1150℃and 0.1 s^(-1)were investigated by hot compression tests,optical microscope(OM),scanning electron microscope(SEM),electron back-scattered diffraction(EBSD)and transmission electron microscope(TEM).The results show that the initial microstructure of the as-SEBMed alloy exhibits layers of coarseγgrains and fineγ+α_(2)+(α_(2)/γ)lamellar mixture grains alternately along the building direction.During the early stage of hot deformation,deformation twins tend to form within the coarse grains,facilitating subsequent deformation,and a small number of DRX grains appear in the fine-grained regions.With the increase of strain,extensive DRX grains are formed through different DRX mechanisms in both coarse and fine-grained regions,involving discontinuous dynamic recrystallization mechanism(DDRX)in the fine-grained regions and a coexistence of DDRX and continuous dynamic recrystallization(CDRX)in the coarsegrained regions.展开更多
Ti_(2)AlNb-based alloy was joined in a continuous drive friction welding machine under different rotational rates(500,1000 and 1500 r/min).The microstructure and mechanical properties of the joints were investigated.I...Ti_(2)AlNb-based alloy was joined in a continuous drive friction welding machine under different rotational rates(500,1000 and 1500 r/min).The microstructure and mechanical properties of the joints were investigated.It is shown that the weld zone(WZ) is fully composed of recrystallized B2 phase,and the grain size decreases with increasing rotational rate.The thermo-mechanically affected zone(TMAZ) suffers severe deformation during welding,due to which most of original precipitation phase is dissolved and streamlines are present.In the heat affected zone(HAZ),only the fine O phase is dissolved.The as-welded joint produced using 1000 r/min has the best mechanical properties,whose strength and elongation are both close to those of the base metal,while the as-welded joint obtained using 500 r/min exhibits the worst mechanical properties.Post-weld annealing treatment annihilates the deformation microstructure and fine O phase precipitates in the joints,consequently improving the mechanical properties significantly.Decomposed α_(2) phase is a weakness for the mechanical performance of the joint since microcracks are apt to form in it in the tensile test.展开更多
Grain refinement of AZ31 Mg alloy during cyclic extrusion compression （CEC） at 225-400 ℃ was investigated quantitatively by electron backscattering diffraction （EBSD）. Results show that an ultrafine grained micro...Grain refinement of AZ31 Mg alloy during cyclic extrusion compression （CEC） at 225-400 ℃ was investigated quantitatively by electron backscattering diffraction （EBSD）. Results show that an ultrafine grained microstructure of AZ31 alloy is obtained only after 3 passes of CEC at 225 ℃. The mean misorientation and the fraction of high angle grain boundaries （HAGBs） increase gradually by lowering extrusion temperature. Only a small fraction of {101^-2} twinning is observed by EBSD in AZ31 Mg alloys after 3 passes of CEC. Schmid factors calculation shows that the most active slip system is pyramidal slip {101^-1}〈1120〉and basal slip {0001}〈1120〉 at 225-350 ℃ and 400 ℃, respectively. Direct evidences at subgrain boundaries support the occurrence of continuous dynamic recrystallization （CDRX） mechanism in grain refinement of AZ31 Mg alloy processed by CEC.展开更多
A cellular automaton（CA） modeling of discontinuous dynamic recrystallization（DDRX） of a near-α Ti-6Al-2Zr-1Mo-1V（TA15） isothermally compressed in the β single phase field was presented.In the CA model,nucleati...A cellular automaton（CA） modeling of discontinuous dynamic recrystallization（DDRX） of a near-α Ti-6Al-2Zr-1Mo-1V（TA15） isothermally compressed in the β single phase field was presented.In the CA model,nucleation of the β-DDRX and the growth of recrystallized grains（re-grains） were considered and visibly simulated by the CA model.The driving force of re-grain growth was provided by dislocation density accumulating around the grain boundaries.To verify the CA model,the predicted flow stress by the CA model was compared with the experimental data.The comparison showed that the average relative errors were10.2%,10.1%and 6%,respectively,at 1.0,0.1 and 0.01 s^-1 of 1020 ℃,and were 10.2%,11.35%and 7.5%,respectively,at 1.0,0.1and 0.01 s^-1 of 1050 ℃.The CA model was further applied to predicting the average growth rate,average re-grain size and recrystallization kinetics.The simulated results showed that the average growth rate increases with the increasing strain rate or temperature,while the re-grain size increases with the decreasing strain rate;the volume fraction of recrystallization decreases with the increasing strain rate or decreasing temperature.展开更多
基金the financial supports from the Shaanxi Province Key Research and Development Projects,China(No.2023KXJ-071)the National Natural Science Foundation of China(Nos.52274402,52174381)。
文摘Microstructural evolution and dynamic recrystallization(DRX)mechanisms of a Ti-48Al-2Cr-2Nb(at.%)alloy prepared by selective electron beam melting(SEBM)during hot deformation at 1150℃and 0.1 s^(-1)were investigated by hot compression tests,optical microscope(OM),scanning electron microscope(SEM),electron back-scattered diffraction(EBSD)and transmission electron microscope(TEM).The results show that the initial microstructure of the as-SEBMed alloy exhibits layers of coarseγgrains and fineγ+α_(2)+(α_(2)/γ)lamellar mixture grains alternately along the building direction.During the early stage of hot deformation,deformation twins tend to form within the coarse grains,facilitating subsequent deformation,and a small number of DRX grains appear in the fine-grained regions.With the increase of strain,extensive DRX grains are formed through different DRX mechanisms in both coarse and fine-grained regions,involving discontinuous dynamic recrystallization mechanism(DDRX)in the fine-grained regions and a coexistence of DDRX and continuous dynamic recrystallization(CDRX)in the coarsegrained regions.
基金the financial supports from the Science and Technology Special Project, China (No. K19168)the National Science and Technology Major Project of China (No. 2017-VI-0004-0075)the National Natural Science Foundation of China (No. 52231002)。
文摘Ti_(2)AlNb-based alloy was joined in a continuous drive friction welding machine under different rotational rates(500,1000 and 1500 r/min).The microstructure and mechanical properties of the joints were investigated.It is shown that the weld zone(WZ) is fully composed of recrystallized B2 phase,and the grain size decreases with increasing rotational rate.The thermo-mechanically affected zone(TMAZ) suffers severe deformation during welding,due to which most of original precipitation phase is dissolved and streamlines are present.In the heat affected zone(HAZ),only the fine O phase is dissolved.The as-welded joint produced using 1000 r/min has the best mechanical properties,whose strength and elongation are both close to those of the base metal,while the as-welded joint obtained using 500 r/min exhibits the worst mechanical properties.Post-weld annealing treatment annihilates the deformation microstructure and fine O phase precipitates in the joints,consequently improving the mechanical properties significantly.Decomposed α_(2) phase is a weakness for the mechanical performance of the joint since microcracks are apt to form in it in the tensile test.
基金Projects(50674067,51074106,51374145)supported by the National Natural Science Foundation of ChinaProject(09JC1408200)supported by the Science and Technology Commission of Shanghai Municipality,China+1 种基金Project(2011BAE22B01-5)supported by the National Key Technology R&D Program of ChinaProjects(182000/S10,192450/I30)supported by the Research Council of Norway
文摘Grain refinement of AZ31 Mg alloy during cyclic extrusion compression （CEC） at 225-400 ℃ was investigated quantitatively by electron backscattering diffraction （EBSD）. Results show that an ultrafine grained microstructure of AZ31 alloy is obtained only after 3 passes of CEC at 225 ℃. The mean misorientation and the fraction of high angle grain boundaries （HAGBs） increase gradually by lowering extrusion temperature. Only a small fraction of {101^-2} twinning is observed by EBSD in AZ31 Mg alloys after 3 passes of CEC. Schmid factors calculation shows that the most active slip system is pyramidal slip {101^-1}〈1120〉and basal slip {0001}〈1120〉 at 225-350 ℃ and 400 ℃, respectively. Direct evidences at subgrain boundaries support the occurrence of continuous dynamic recrystallization （CDRX） mechanism in grain refinement of AZ31 Mg alloy processed by CEC.
基金Projects (50935007,51175428) supported by the National Natural Science Foundation of ChinaProject (2010CB731701) supported by the National Basic Research Program of China+2 种基金Project (NPU-FFR-JC20100229) supported by the Foundation for Fundamental Research of Northwestern Polytechnical University in ChinaProject (27-TZ-2010) supported by the Research Fund of the State Key Laboratory of Solidification Processing,ChinaProject (B08040) supported by the Program of Introducing Talents of Discipline to University,China
文摘A cellular automaton（CA） modeling of discontinuous dynamic recrystallization（DDRX） of a near-α Ti-6Al-2Zr-1Mo-1V（TA15） isothermally compressed in the β single phase field was presented.In the CA model,nucleation of the β-DDRX and the growth of recrystallized grains（re-grains） were considered and visibly simulated by the CA model.The driving force of re-grain growth was provided by dislocation density accumulating around the grain boundaries.To verify the CA model,the predicted flow stress by the CA model was compared with the experimental data.The comparison showed that the average relative errors were10.2%,10.1%and 6%,respectively,at 1.0,0.1 and 0.01 s^-1 of 1020 ℃,and were 10.2%,11.35%and 7.5%,respectively,at 1.0,0.1and 0.01 s^-1 of 1050 ℃.The CA model was further applied to predicting the average growth rate,average re-grain size and recrystallization kinetics.The simulated results showed that the average growth rate increases with the increasing strain rate or temperature,while the re-grain size increases with the decreasing strain rate;the volume fraction of recrystallization decreases with the increasing strain rate or decreasing temperature.
