Bonding enhancement of cold rolling TA1 P-Ti/AA6061 composite plates via surface oxidation treatment

TA1 P-Ti/AA6061 composite plate was produced by oxidizing the surface of the titanium plate and adopting a cold roll bonding process.The results revealed that the oxide film(Ti6O)prepared on the surface of TA1 pure titanium was easy to crack during the cold roll bonding,thereby promoting the formation of an effective mechanical interlock at the interface,which can effectively reduce the minimum reduction rate of the composite plates produced by cold rolling of titanium and aluminium plates.Moreover,the composite plate subjected to oxidation treatment exhibited high shear strength,particularly at a 43%reduction rate,achieving a commendable value of 117 MPa.Based on oxidation treatment and different reduction rates,the annealed composite plates at temperatures of 400,450,and 500°C displayed favorable resistance to interface delamination,highlighting their remarkable strength-plasticity compatibility as evidenced by a maximum elongation of 31.845%.

起诉裁量权行使状况之实证分析

我国起诉裁量权行使形态复杂,存在以不起诉的法定形式行使方式和退处中的隐性行使方式。实证研究表明,刑事政策和检察机关内部指导规则对起诉裁量权行使程度的抑扬变化和行使方式的选择均有突出影响。在实行宽严相济刑事政策、构建和谐社会的背景下,检察机关应当调整不起诉率等内部机制,引导起诉裁量权科学行使,并应当区别严重性程度不同的犯罪,贯彻刑法谦抑原则,轻重刑罚协调适用,以期真正化解矛盾,实现有效犯罪控制。

Effects of stoichiometric ratio La/Mg on structures and electrochemical performances of as-cast and annealed La-Mg-Ni-based A_2B_7-type electrode alloys

In order to investigate the influences of the stoichiometric ratio of La/Mg （increasing La and decreasing Mg on the same mole ratio） on the structure and electrochemical performances of the La-Mg-Ni-based A2B7-type electrode alloy, the as-cast and the annealed ternary Lao.8＋xMgo.2_xNi3.5 （x=0-0.05） electrode alloys were prepared. The characterization of electrode alloys by X-ray diffraction （XRD） and scanning electron microscopy （SEM） shows that all the as-cast and the annealed alloys hold two major phases of （La,Mg）2Ni7 and LaNi5 as well as a residual phase of LaNi3. Moreover, the increase of La/Mg ratio brings on a decline of （La,Mg）2Ni7 phase and a rise of LaNi5 and LaNi3 phases. The variation of La/Mg ratio gives rise to an evident change of the electrochemical performances of the alloys. The discharge capacities of the as-cast and the annealed alloys evidently decrease with growing the La/Mg ratio, while the cycle stabilities of the alloys visibly augment under the same condition. Furthermore, the high rate discharge ability （HRD）, the electrochemical impedance spectrum （EIS）, the Tafel polarization curves, and the potential step measurements all indicate that the electrochemical kinetic properties of the alloy electrodes increase with the La/Mg ratio rising.

Electrical Transport Properties of Annealed Undoped InP

The electrical properties of annealed undoped n type InP are studied by temperature dependent Hall effect (TDH) and current voltage ( I V ) measurements for semiconducting and semi insulating samples,respectively.Defect band conduction in annealed semiconducting InP can be observed from TDH measurement,which is similar to those of as grown unintentionally doped InP with low carrier concentration and moderate compensation.The I V curves of annealed undoped SI InP exhibit ohmic property in the applied field region up to the onset of breakdown.Such a result is different from that of as grown Fe doped SI InP which has a nonlinear region in I V curve explained by the theory of space charge limited current.

Effect of annealing treatment on morphologies and gas sensing properties of ZnO nanorods

The high-temperature stabilization of ZnO nanorods synthesized by hydrothermal treatment was investigated. The structure and morphologies of ZnO nanorods were characterized by XRD and SEM, respectively. The thermal stability of ZnO nanorods was also detected by thermal gravity analyzing. Thermal annealing treatment results indicate that ZnO nanorods are fundamentally stable when annealing temperature is lower than 600 ℃. When annealing temperature is beyond 600℃, the diameters of ZnO nanorods obviously decrease and the aggravating tendency of nanorods between each other also increase. Annealing treatment can greatly influence the gas sensing properties of ZnO nanorods. Comparing with ZnO nanorods without annealing treatment, the gas sensing property of ZnO nanorods to H2 with concentration of 2.5×10-6 can increase from 2.22 to 3.56. ZnO nanorods annealed at 400 ℃ exhibit optimum gas sesing property to H2 gas.

Influence of pre-strain and heat treatment on subsequent deformation behavior of extruded AZ31 Mg alloy

Pre-compression and heat treatment were performed on an extruded AZ31 Mg alloy,and their effects on subsequent deformation behavior were investigated.The results show that at low temperature annealing(170 ℃ for 4 h),the extruded samples with and without annealing exhibit a nearly equivalent yield stress(~148 MPa) because their microstructures are nearly unchanged.However,under the same annealing condition,the yield stress of sample with pre-twinning and subsequent annealing(~225 MPa) is higher than that of the pre-twinned one(~200 MPa).The former sample presents a hardening effect because the solute atoms segregated on twin boundaries lead to a strengthening effect.The pre-twinned sample annealed at 400 ℃ for 1 h shows a higher ultimate elongation(~28%) than the pre-twinned one(~15%),but its yield stress(~125 MPa) is much lower than that of the pre-twinned one(~200 MPa).

An investigation on electrochemical performances of as-cast and annealed La_(0.8)Mg_(0.2)Ni_(3.3)Co_(0.2)Si_x(x=0-0.2)alloy electrodes for Ni/MH battery application

The La-Mg-Ni-based A2B7-type La0.5Mg0.2Ni3.3Co0.2Six （x=0-0.2） electrode alloys were prepared by casting and annealing. The influences of the additional silicon and the annealing treatment on the structure and electrochemical performances of the alloys were investigated systemically. Both of the analyses of XRD and SEM reveal that the as-cast and annealed alloys are of a multiphase structure, involving two main phases （La, Mg）2Ni7 and LaNi5 as well as one minor phase LaNi3. The addition of Si and annealing treatment bring on an evident change in the phase abundances and cell parameters of （La, Mg）2Ni7 and LaNi5 phase for the alloy without altering its phase structure. The phase abundances decrease from 74.3% （x=0） to 57.8% （x=0.2） for the （La, Mg）2Ni7 phase, and those of LaNi5 phase increase from 20.2% （x^0） to 37.3% （x=0.2）. As for the electrochemical measurements, adding Si and performing annealing treatment have engendered obvious impacts. The cycle stability of the alloys is improved dramatically, being enhanced from 80.3% to 93.7% for the as-annealed （950 ℃） alloys with Si content increasing from 0 to 0.2. However, the discharge capacity is reduced by adding Si, from 399.4 to 345.3 mA.h/g as the Si content increases from 0 to 0.2. Furthermore, such addition makes the electrochemical kinetic properties of the alloy electrodes first increase and then decrease. Also, it is found that the overall electrochemical properties of the alloys first augment and then fall with the annealing temperature rising.

Structure and properties of AZ31B magnesium alloy sheets processed by repeatedly unidirectional bending at different temperatures

Repeatedly unidirectional bending(RUB) was applied to the magnesium alloy sheet to improve the basal texture.The effect of RUB temperature on resulting structure and room temperature properties was investigated.The texture components of the sheet undergoing RUB at recovery temperature were similar to those of the sheet undergoing RUB at room temperature(RT).As the RUB temperature increased to above recrystallization temperature,the texture components became more disperse and the pyramidal components increased.With the increase of RUB temperature,the grain size near the surface of the sheets undergoing RUB tended to grow up.When the sheets were processed by RUB at medium-high temperature followed by annealing at 533 K,the yield strength and fracture elongation were lower than those of the cold rolled sheet;however,the Erichsen value was slightly higher than that of the cold rolled sheet.The sheet undergoing RUB at RT followed by annealing at 533 K represented the best mechanical properties.

Microstructural evolution and mechanical properties of selective laser melted Ti-6Al-4V induced by annealing treatment

Ti-6Al-4V specimens were fabricated by selective laser melting(SLM)to study the effect of thermal treatment on the phase transformation,elemental diffusion,microstructure,and mechanical properties.The results show that vanadium enriches around the boundary ofαphases with increasing annealing temperature to 973 K,andα′phases transform intoα+βat 973 K.The typicalα′martensite microstructure transforms to fine-scale equiaxed microstructure at 973 K and the equiaxed microstructure significantly coarsens with increasing annealing temperature to 1273 K.The SLM Ti-6Al-4V alloy annealed at 973 K exhibits a well-balanced combination of strength and ductility((1305±25)MPa and(37±3)%,respectively).

Microstructure and Property of Al‑FeCoNiCrAl High Entropy Alloy Composite Coating on Ti‑6Al‑4V During Annealing Using MA Method

Al-FeCoNiCrAl high entropy alloy(HEA) composite coatings were prepared on Ti-6Al-4V via highenergy mechanical alloying(MA). The microstructures and phase composition of the coatings were studied. A continuous and dense coating could be fabricated at a ratio of 35%(weight fraction)Al-FeCoNiCrAl after 4 h milling.The results showed that the thickness of the composite coatings increased first and then decreased with the increase of milling time. And the hardness of coating increased with the increase of milling time. The phase changed during the annealing process. Part of the initial body-centered cubic(BCC)phase of the composite coatings changed into the L12 phase,(Ni,Co)3Al4 and σ phase after annealing above 550 ℃. Ordered BCC was found in the coatings after annealing above 750 ℃. Only BCC and ordered BCC appeared in coatings after annealing above 1 050 ℃. The hardness of the coatings after annealing at 550 ℃ and 750 ℃ was higher than before because of spinodal decomposition and high hardness σ phase. The hardness of the coatings after annealing at 1 050 ℃ decreased because residual stress released.

Preparation and characterization of carbonyl iron soft magnetic composites with magnesioferrite insulating coating layer

Spherical carbonyl iron(Fe)powders were coated with magnesioferrite(MgFe2O4)insulating coating layer and then mixed with epoxy-modified silicone resin(ESR).Soft magnetic composites(SMCs)were fabricated by compaction of the coated powders and annealing treatment.Transmission electron microscopy(TEM),scanning electron microscopy(SEM),energy dispersive spectroscopy(EDS),X-ray diffractometry(XRD)and X-ray photoelectron spectroscopy(XPS)revealed that the MgFe2O4 layer was coated on the surface of the iron powders.The magnetic properties of SMCs were determined using a vibrating sample magnetometer and an auto testing system for magnetic materials.The results showed that the SMCs prepared at 800 MPa and 550℃ exhibited a significant core loss of 167.5 W/kg at 100 kHz and 50 mT.

Comparative study of microstructure and corrosion resistance of electroless Ni-W-P coatings treated by laser and furnace-annealing

A comparative study of amorphous electroless Ni-W-P coatings on mild steel substrate treated by a high power diode laser and furnace annealing was presented.Effects of different laser operating parameters and furnace-annealing conditions on microstructures,in terms of crystallisation,pores formation and grain growth,were investigated using SEM/EDX and XRD. Corrosion behaviours of these coatings before and after various treatments were evaluated with anodic polarisation in 0.5 mol/L H2SO4 solution.The results show that the furnace-annealing produces either a mixture of nanocrystallined Ni and amorphous phases or precipitated Ni3P phase distributed in nanocrystallined Ni-based matrix,depending on annealing temperatures,whilst the laser treatment under the operating conditions only produces nanocrystallined Ni-based matrix with Ni3P precipitates.Corrosion performance of the coatings treated by both the laser and the furnace-annealing is dependent on the annealing temperature and laser operating conditions.Corrosion mechanisms of various treated-coatings were discussed in the consideration of phase constitutes and proportion,grain sizes of both Ni and Ni3P phases,pores formation and residual stresses.

Effect of duplex aging on microstructure and mechanical properties of near-βtitanium alloy processed by isothermal multidirectional forging

The effects of sub-transus(α+β)annealing treatment(ST),followed by single aging(SA)or duplex aging(DA)on the microstructural evolution and mechanical properties of near-βTi-4Al-1Sn-2Zr-5Mo-8V-2.5Cr(mass fraction,%)alloy were investigated using optical microscopy,scanning electron microscopy,and transmission electron microscopy.The results show that the finer secondaryαphase precipitates in the alloy after DA than SA(e.g.,149 nm for SA and 69 nm for DA,both after ST at 720℃).The main reason is that the pre-aging step(300℃)in the DA process leads to the formation of intermediateωphase nanoparticles,which assist in the nucleation of the acicular secondaryαphase precipitates.In addition,the strength of the alloy after DA is higher than that of SA at the specific ST temperature.A good combination is achieved in the alloy subjected to ST at 750℃,followed by DA(UTS:1450 MPa,EL:3.87%),which is due to the precipitation of nanoscale secondaryαphase by DA.In conclusion,DA is a feasible process for this new near-βtitanium alloy.

Bonding interface zone of Mg-Gd-Y/Mg-Zn-Gd laminated composite fabricated by equal channel angular extrusion

In order to improve the mechanical properties and corrosion resistance of Mg alloys,the equal channel angular extrusion (ECAE)was employed to fabricate the Mg-5Gd-5Y/Mg-2Zn-1Gd(GW55/ZG21)laminated composites.After fabrication and annealing treatment,the microstructural evolution,phase constitution,microhardness,and bonding strength were investigated on the bonding interface zone of GW55/ZG21 laminated composites.The bonding interface zone of GW55/ZG21 laminated composites comprises a lot of Mg3(Y,Gd)2Zn3 particles along the bonding interface,some rod Mg24(Y,Gd)5 phases on GW55 side,and a precipitation free zone(PFZ)on ZG21 side.After annealing treatment,Mg3(Y,Gd)2Zn3 particles along the bonding interface increase, rod Mg24(Y,Gd)5 phases on GW55 side decrease,and PFZ is broadened.Meanwhile,the hardness on the bonding interface zone decreases and the bonding strength increases from 126 MPa to 162 MPa.

Manufacturing techniques of armor strips excavated from Emperor Qin Shi Huang's mausoleum,China

The chemical compositions and microstructures of the armor strips excavated from the Emperor Qin Shi Huang's mausoleum were examined systematically by using optical microscopy and electron microscopy.It was found that the armor strips were made of pure copper.Based on the morphology of α-Cu recrystal grain and copper sulphide(Cu2S) inclusions in the armor strips,the manufacturing techniques were proposed as follows:smelting pure copper,casting a lamellar plate,forming the cast ingots into sheets through repeated cold forging combined with annealing heat treatment,and finally cutting the sheets into filaments.Furthermore,through the deformation of copper sulphide(Cu2S) inclusions in the strips,the work rate during forging was evaluated and calculated to be close to 75%.

Improvement of hydrogen embrittlement and stress corrosion cracking by annealing for Al-4.4Mg-0.6Mn alloy

With no annealing treatment, cathodic polarization trends in 5083F A1 alloy revealed concentration polarization and activation polarization. However, the annealed specimens have lower current densities at corrosion protection potential compared to the non-annealed specimen. The results of SSRTs conducted in seawater at the applied potential range of-l.8 V to -0.5 V indicated that the maximum tensile strength, elongation, and time-to-fracture had high values at applied potentials of -0.7 to -1.4 V. The maximum tensile strength, elongation, and time-to-f？acture decreased when the potential values were beyond this range in either anodic or cathodic direction. In general, the increased shear lip caused by annealing treatment indicates elongation. Time-to-fracture would likely increase with elongation. Potentials between -0.5 V to -0.6 V were found to be in the region of stress corrosion cracking. The corrosion protection zone was determined to be -0.7 V to -J,4 V because these potential ranges produced good mechanical properties. Potential less than -1.4 V produced a fractured surface with a mixture of dimples （ductile fractures） and a quasi-cleavage pattern resulting from the effects of hydrogen gas.

Microstructure and mechanical properties of Al-5.8Mg-Mn-Sc-Zr alloy after annealing treatment

An A1-5.8Mg-0.4Mn-0.35（Sc＋Zr） （mass fraction, %） alloy sheet was prepared using water chilling copper mould ingot metallurgy processing which was protected by active flux. The influence of stabilizing annealing on mechanical properties and microstructure of the cold rolling sheet was studied. The results show that the strength and hardness of the alloy decrease, while the elongation increases with increasing the stabilizing annealing temperature. With the increase of stabilizing annealing time, the strength and hardness of the alloy drop slightly but its ductility exhibits no change. Partial recovery and recrystallization orderly occur with the increase of annealing temperature during stabilizing treatment. Only different degrees of recovery occur in the alloys annealed below 400 ℃ for 1 h. Partial recrystallization occurs after annealed at 450 ℃ for 1 h. By annealing at 300 ℃ for 1 h, the alloy can obtain the optimum application values of δb, δ0.2 and δ, which are 436 MPa, 327 MPa and 16.7%, respectively.

Noise degradation system using Wiener filter and CORDIC based FFT/IFFT processor

On augmentation of past work, an effective Wiener filter and its application for noise suppression combined with a formed CORDIC based FFT/IFFT processor with improved speed were executed. The pipelined methodology was embraced for expanding the execution of the system. The proposed Wiener filter was planned in such an approach to evacuate the iteration issues in ordinary Wiener filter. The division process was supplanted by a productive inverse and multiplication process in the proposed design. An enhanced design for matrix inverse with reduced computation complexity was executed. The wide-ranging framework processing was focused around IEEE-754 standard single precision floating point numbers. The Wiener filter and the entire system design was integrated and actualized on VIRTEX 5 FPGA stage and re-enacted to approve the results in Xilinx ISE 13.4. The results show that a productive decrease in power and area is developed by adjusting the proposed technique for speech signal noise degradation with latency of n/2 clock cycles and substantial throughput result per every 12 clock cycles for n-bit precision. The execution of proposed design is exposed to be 31.35% more effective than that of prevailing strategies.

Design of Rapid Thermal Processing for Large Diameter Wafer

The relationship between the arrangement of tungsten-halogen lamps and the uniformity of irradiance received by the wafer is discussed, and a sort of axial-symmetrical lamps-array is designed to guarantee that the irradiation on the edge is approximately the same as the one on the center of the wafer. The magnitude of temperature on the wafer vs. the power of tungsten-halogen lamps is calculated numerically.

Background Subtraction and Frame Difference Based Moving Object Detection for Real-Time Surveillance

A new real-time algorithm is proposed in this paperfor detecting moving object in color image sequencestaken from stationary cameras.This algorithm combines a temporal difference with an adaptive background subtraction where the combination is novel.Ⅷ1en changes OCCUr.the background is automatically adapted to suit the new conditions.Forthe background model,a new model is proposed with each frame decomposed into regions and the model is based not only upon single pixel but also on the characteristic of a region.The hybrid presentationincludes a model for single pixel information and a model for the pixel’s neighboring area information.This new model of background can both improve the accuracy of segmentation due to that spatialinformation is taken into account and salientl5r speed up the processing procedure because porlion of neighboring pixel call be selected into modeling.The algorithm was successfully used in a video surveillance systern and the experiment result showsit call obtain a clearer foreground than the singleframe difference or background subtraction method.