Thermal stability,crystallization behavior,Vickers hardness and magnetic properties of the Fe41Co7-xNixCr15Mo14C15B6Y2(x=0,1,3,5) bulk metallic glasses were investigated.The Fe41Co7-xNixCr15Mo14C15B6Y2(x=0,1,3,5) ...Thermal stability,crystallization behavior,Vickers hardness and magnetic properties of the Fe41Co7-xNixCr15Mo14C15B6Y2(x=0,1,3,5) bulk metallic glasses were investigated.The Fe41Co7-xNixCr15Mo14C15B6Y2(x=0,1,3,5) metallic glasses were fabricated by copper mold casting method.The thermal stability and crystallization behavior of the metallic glass rods were investigated by differential scanning calorimetry and isothermal experiments.Hardness measurements for samples annealed at different temperatures for different time were carried out at room temperature by the Vickers hardness tester,and magnetic measurements were performed at different temperatures by the vibrating sample magnetometer.It is shown that the addition of Ni does not play a positive role for enlarging ΔTx and GFA from parameter γ(=Tx/(Tg+Tl)),and it can,however,increase the activation energy in the initial stage of crystallization by changing the initial crystallization behavior.The minor addition of Ni can refine the crystal grain obtained from the full crystallization experiment.The primary crystallization causes the decrease of hardness in these alloys,and as the crystallization continues,the hardness in all samples increases instead due to the precipitation of carbide and boride.The annealing temperature has an obvious effect on magnetic properties of these alloys,and the minor addition of Ni can effectively prevent the alloy annealed at high temperature to transform from paramagnetic to ferromagnetic state.展开更多
Spherical carbonyl iron(Fe)powders were coated with magnesioferrite(MgFe2O4)insulating coating layer and then mixed with epoxy-modified silicone resin(ESR).Soft magnetic composites(SMCs)were fabricated by compaction o...Spherical carbonyl iron(Fe)powders were coated with magnesioferrite(MgFe2O4)insulating coating layer and then mixed with epoxy-modified silicone resin(ESR).Soft magnetic composites(SMCs)were fabricated by compaction of the coated powders and annealing treatment.Transmission electron microscopy(TEM),scanning electron microscopy(SEM),energy dispersive spectroscopy(EDS),X-ray diffractometry(XRD)and X-ray photoelectron spectroscopy(XPS)revealed that the MgFe2O4 layer was coated on the surface of the iron powders.The magnetic properties of SMCs were determined using a vibrating sample magnetometer and an auto testing system for magnetic materials.The results showed that the SMCs prepared at 800 MPa and 550℃ exhibited a significant core loss of 167.5 W/kg at 100 kHz and 50 mT.展开更多
A 100MeV compact high intensity H-cyclotron is under design and construction at CIAE which will provide a 75MeV—100MeV,200μA proton beam.The main magnet of this cyclotron adopts an integrally compact structure with ...A 100MeV compact high intensity H-cyclotron is under design and construction at CIAE which will provide a 75MeV—100MeV,200μA proton beam.The main magnet of this cyclotron adopts an integrally compact structure with a fixed field and four sectors,while the hill gap is constantly changeable.This paper reviews the design features of the magnet,numerical simulation results,the inner defects of the magnet including the carbon content segregation and shrinkage porosity,factors related to mechanical design including the tolerance and deformation.The latest progress will also be reported in this paper.展开更多
基金Project(2012CB825700) supported by the National Basic Research Program of China
文摘Thermal stability,crystallization behavior,Vickers hardness and magnetic properties of the Fe41Co7-xNixCr15Mo14C15B6Y2(x=0,1,3,5) bulk metallic glasses were investigated.The Fe41Co7-xNixCr15Mo14C15B6Y2(x=0,1,3,5) metallic glasses were fabricated by copper mold casting method.The thermal stability and crystallization behavior of the metallic glass rods were investigated by differential scanning calorimetry and isothermal experiments.Hardness measurements for samples annealed at different temperatures for different time were carried out at room temperature by the Vickers hardness tester,and magnetic measurements were performed at different temperatures by the vibrating sample magnetometer.It is shown that the addition of Ni does not play a positive role for enlarging ΔTx and GFA from parameter γ(=Tx/(Tg+Tl)),and it can,however,increase the activation energy in the initial stage of crystallization by changing the initial crystallization behavior.The minor addition of Ni can refine the crystal grain obtained from the full crystallization experiment.The primary crystallization causes the decrease of hardness in these alloys,and as the crystallization continues,the hardness in all samples increases instead due to the precipitation of carbide and boride.The annealing temperature has an obvious effect on magnetic properties of these alloys,and the minor addition of Ni can effectively prevent the alloy annealed at high temperature to transform from paramagnetic to ferromagnetic state.
基金Project(2016YFB0700302)supported by the National Key Research and Development Program of ChinaProjects(51862030,51563020)supported by the National Natural Science Foundation of China。
文摘Spherical carbonyl iron(Fe)powders were coated with magnesioferrite(MgFe2O4)insulating coating layer and then mixed with epoxy-modified silicone resin(ESR).Soft magnetic composites(SMCs)were fabricated by compaction of the coated powders and annealing treatment.Transmission electron microscopy(TEM),scanning electron microscopy(SEM),energy dispersive spectroscopy(EDS),X-ray diffractometry(XRD)and X-ray photoelectron spectroscopy(XPS)revealed that the MgFe2O4 layer was coated on the surface of the iron powders.The magnetic properties of SMCs were determined using a vibrating sample magnetometer and an auto testing system for magnetic materials.The results showed that the SMCs prepared at 800 MPa and 550℃ exhibited a significant core loss of 167.5 W/kg at 100 kHz and 50 mT.
文摘A 100MeV compact high intensity H-cyclotron is under design and construction at CIAE which will provide a 75MeV—100MeV,200μA proton beam.The main magnet of this cyclotron adopts an integrally compact structure with a fixed field and four sectors,while the hill gap is constantly changeable.This paper reviews the design features of the magnet,numerical simulation results,the inner defects of the magnet including the carbon content segregation and shrinkage porosity,factors related to mechanical design including the tolerance and deformation.The latest progress will also be reported in this paper.