To improve the machinability of optical glass and achieve optical parts with satisfied surface quality and dimensional accuracy, scratching experiments with increasing cutting depth were conducted on glass SF6 to eval...To improve the machinability of optical glass and achieve optical parts with satisfied surface quality and dimensional accuracy, scratching experiments with increasing cutting depth were conducted on glass SF6 to evaluate the influence of cutting fluid properties on the machinability of glass. The sodium carbonate solution of 10.5% concentration was chosen as cutting fluid. Then the critical depths in scratching experiments with and without cutting fluid were examined. Based on this, turning experiments were carried out, and the surface quality of SF6 was assessed. Compared with the process of dry cutting, the main indexes of surface roughness decrease by over 70% totally. Experimental results indicated that the machinability of glass SF6 can be improved by using the sodium carbonate solution as cutting fluid.展开更多
Organic solar cells （OSCs） is a new generation of solar cells have emerged as an alternative to conventional Si-based solar cells owing to their advantages of low cost, ease of fabrication and their potential for th...Organic solar cells （OSCs） is a new generation of solar cells have emerged as an alternative to conventional Si-based solar cells owing to their advantages of low cost, ease of fabrication and their potential for the manufacture of flexible and large area solar cells. So we chose that part to beginning study of the material and all parameters effects in environmental condition because the solar cell working in environment. In this study the fabrication of poly（3-hexylthiophene） （P3HT） and [6,6]-phenyl C61-butyric acid methyl ester （PCBM） blend flexible thin film using spin coating was reported. Process parameters like solvent, electron donor to acceptor ratio, concentration and temperature were also studied. We used solvent systems to make active layer of P3HT：PCBM composite and PEDOT：PSS as a buffer layer. Highest absorption was obtained for the flexible thin film made with 1：1 and 1：0.75 ratio of P3HT to PCBM. Chloroform solvent in 40 gm/ml concentration at 90 ~C was the optimum conditions to make flexible device.展开更多
Paclitaxel(PTX) is an effective anticancer drug with poor solubility in water.Recently,much effort has been devoted into alternative formulations of PTX for improving its aqueous solubility.In this study,PTX and poly(...Paclitaxel(PTX) is an effective anticancer drug with poor solubility in water.Recently,much effort has been devoted into alternative formulations of PTX for improving its aqueous solubility.In this study,PTX and poly(L-lactic acid)(PLLA) were co-precipitated by a supercritical antisolvent(SAS) process using dichloromethane(DCM) and the mixtures of DCM/ethanol(EtOH) or DCM/dimethyl sulfoxide(DMSO) as the solvent,with super-critical carbon dioxide as the antisolvent.The effects of solvent,solvent ratio,temperature,pressure,polymer con-centration and solution flow rate on particle morphology,mass median diameter(Dp50) and PTX loading were in-vestigated using single-factor method.The particle samples were characterized using X-ray diffraction(XRD),scanning electron microscopy(SEM),laser diffraction particle size analyzer and high pressure liquid chromatogra-phy(HPLC).XRD results indicate that the micronized PTX is dispersed into the PLLA matrix in an amorphous form.SEM indicates that the solvent and the solvent ratio have great effect on the particle morphologies,and particle morphology is good at the volume ratio of DCM/EtOH of 50/50.For the mixed DCM/EtOH solvent,Dp50 increases with the increase of the temperature,pressure,PLLA concentration and solution flow rate,and PTX loading in-creases with pressure.Suitable operating conditions for the experimental system are as follows:DCM/EtOH 50/50(by volume),35 ℃,10-12 MPa,PLLA concentration of 5 g·L-1 and solution flow rate of 0.5 ml·min-1.展开更多
基金Supported by National Natural Science Foundation of China (No. 50775057)
文摘To improve the machinability of optical glass and achieve optical parts with satisfied surface quality and dimensional accuracy, scratching experiments with increasing cutting depth were conducted on glass SF6 to evaluate the influence of cutting fluid properties on the machinability of glass. The sodium carbonate solution of 10.5% concentration was chosen as cutting fluid. Then the critical depths in scratching experiments with and without cutting fluid were examined. Based on this, turning experiments were carried out, and the surface quality of SF6 was assessed. Compared with the process of dry cutting, the main indexes of surface roughness decrease by over 70% totally. Experimental results indicated that the machinability of glass SF6 can be improved by using the sodium carbonate solution as cutting fluid.
文摘Organic solar cells （OSCs） is a new generation of solar cells have emerged as an alternative to conventional Si-based solar cells owing to their advantages of low cost, ease of fabrication and their potential for the manufacture of flexible and large area solar cells. So we chose that part to beginning study of the material and all parameters effects in environmental condition because the solar cell working in environment. In this study the fabrication of poly（3-hexylthiophene） （P3HT） and [6,6]-phenyl C61-butyric acid methyl ester （PCBM） blend flexible thin film using spin coating was reported. Process parameters like solvent, electron donor to acceptor ratio, concentration and temperature were also studied. We used solvent systems to make active layer of P3HT：PCBM composite and PEDOT：PSS as a buffer layer. Highest absorption was obtained for the flexible thin film made with 1：1 and 1：0.75 ratio of P3HT to PCBM. Chloroform solvent in 40 gm/ml concentration at 90 ~C was the optimum conditions to make flexible device.
基金Supported by the National Natural Science Foundation of China (21076084)the Fundamental Research Funds for the Central Universities (2011ZZ0006)the Open Project Program of Provincial Key Laboratory of Green Processing Technology and Product Safety of Natural Products
文摘Paclitaxel(PTX) is an effective anticancer drug with poor solubility in water.Recently,much effort has been devoted into alternative formulations of PTX for improving its aqueous solubility.In this study,PTX and poly(L-lactic acid)(PLLA) were co-precipitated by a supercritical antisolvent(SAS) process using dichloromethane(DCM) and the mixtures of DCM/ethanol(EtOH) or DCM/dimethyl sulfoxide(DMSO) as the solvent,with super-critical carbon dioxide as the antisolvent.The effects of solvent,solvent ratio,temperature,pressure,polymer con-centration and solution flow rate on particle morphology,mass median diameter(Dp50) and PTX loading were in-vestigated using single-factor method.The particle samples were characterized using X-ray diffraction(XRD),scanning electron microscopy(SEM),laser diffraction particle size analyzer and high pressure liquid chromatogra-phy(HPLC).XRD results indicate that the micronized PTX is dispersed into the PLLA matrix in an amorphous form.SEM indicates that the solvent and the solvent ratio have great effect on the particle morphologies,and particle morphology is good at the volume ratio of DCM/EtOH of 50/50.For the mixed DCM/EtOH solvent,Dp50 increases with the increase of the temperature,pressure,PLLA concentration and solution flow rate,and PTX loading in-creases with pressure.Suitable operating conditions for the experimental system are as follows:DCM/EtOH 50/50(by volume),35 ℃,10-12 MPa,PLLA concentration of 5 g·L-1 and solution flow rate of 0.5 ml·min-1.
