Texture and grain boundary character distribution of Cu interconnects with different line width for as-deposited and annealed conditions were measured by EBSD. All specimens appear mixed texture and （111） texture is...Texture and grain boundary character distribution of Cu interconnects with different line width for as-deposited and annealed conditions were measured by EBSD. All specimens appear mixed texture and （111） texture is the dominate component.As-deposited interconnects undergo the phenomenon of self-annealing at RT,in which some abnormally large grains are found. Lower aspect ratio of lines and anneal treatment procured larger grains and stronger （111） texture. Meanwhile, the intensity proportion of other textures with lower strain energy to （111） texture is decreased. As-deposited specimens reveal （111）（112？ and （111） （231） components, （111） （110） component appeared and （111） （112？ and （111） （231） components were developed during the annealing process. High angle boundaries are dominant in all specimens, boundaries with a misorientation of 55°-60° and ∑3 ones in higher proportion, followed by lower boundaries with a misorientation of 35°-40° and 29 boundaries. As the aspect ratio of lines and anneal treatment increase,there is a gradual in- crement in ∑3 boundaries and a decrease in ∑9 boundaries.展开更多
We link different microstructures to tribological behaviors of Ti-50.8 Ni(mole fraction, %) in reciprocating mode at room temperature(20 ℃). Hot-rolled alloys with B2 phase exhibit lower coefficient of friction and w...We link different microstructures to tribological behaviors of Ti-50.8 Ni(mole fraction, %) in reciprocating mode at room temperature(20 ℃). Hot-rolled alloys with B2 phase exhibit lower coefficient of friction and wear rate compared to the ones with B19?. Stress-induced martensitic transformation occurs during sliding. However, multi-pass hot rolling weakens the wear resistance. In this study, microstructures were characterized through electron backscatter diffraction and transmission electron microscopy(EBSD/TEM). From the concept of energy conservation, the effects of weak intensity of hot-rolled textures on the wear resistance are minimal. Based on the result that the alloy with a higher portion of coincidence site lattice boundaries shows lower martensitic start transformation temperature in the DSC curves than that with higher KAM values, the delay on B2-B19? transformation from {112}B2 twins outweighs dislocations. Moreover, widely distributed small-angle grain boundaries owing to dynamic recovery improve the wear resistance effectively compared to those that are well-recrystallized.展开更多
Background and objective:Intra-corporeal delta-shaped anastomosis(IDA)is an important development in laparoscopic digestive-tract reconstruction.We applied it in laparoscopic right hemicolectomy for right colon cancer...Background and objective:Intra-corporeal delta-shaped anastomosis(IDA)is an important development in laparoscopic digestive-tract reconstruction.We applied it in laparoscopic right hemicolectomy for right colon cancer and compared the short-term outcomes between the patients treated with IDA and conventional extracorporeal anastomosis(EA).Methods:Between 1 January 2016 and 1 October 2017,36 and 50 patients who underwent IDA and EA,respectively,were included.Data on clinicopathological characteristics,surgical outcomes,post-operative recovery and complications were collected and compared between the two groups.Results:Surgical outcomes and clinicopathological characteristics were similar between the two groups except the length of incision,which was significantly shorter in the IDA group than in the EA group(4.660.6 vs 5.660.7 cm,P<0.001).The time to ground activities,fluid diet intake and post-operative hospitalization did not differ between the groups;however,the time to first flatus was significantly shorter in the IDA group than in the EA group(2.860.5 vs 3.260.8 days,P=0.004).The post-operative visual analogue scale for pain was lower in the IDA group than in the EA group on post-operative Day 1(4.060.7 vs 4.561.0,P=0.002)and post-operative Day 3(2.760.6 vs 3.460.6,P<0.001).The surgical complication rates were 8.3 and 16.0%in the IDA and EA groups(P=0.470),respectively.No complications such as anastomotic bleeding,stenosis and leakage occurred in any patient.Conclusions:IDA is safe and feasible and shows more satisfactory short-term outcomes than EA.展开更多
文摘Texture and grain boundary character distribution of Cu interconnects with different line width for as-deposited and annealed conditions were measured by EBSD. All specimens appear mixed texture and （111） texture is the dominate component.As-deposited interconnects undergo the phenomenon of self-annealing at RT,in which some abnormally large grains are found. Lower aspect ratio of lines and anneal treatment procured larger grains and stronger （111） texture. Meanwhile, the intensity proportion of other textures with lower strain energy to （111） texture is decreased. As-deposited specimens reveal （111）（112？ and （111） （231） components, （111） （110） component appeared and （111） （112？ and （111） （231） components were developed during the annealing process. High angle boundaries are dominant in all specimens, boundaries with a misorientation of 55°-60° and ∑3 ones in higher proportion, followed by lower boundaries with a misorientation of 35°-40° and 29 boundaries. As the aspect ratio of lines and anneal treatment increase,there is a gradual in- crement in ∑3 boundaries and a decrease in ∑9 boundaries.
基金financially supported by the National Natural Science Foundation of China-Aerospace Science and Technology Corporation of China Aerospace Advanced Manufacturing Technology Research Joint Fund (U1737204)the National Natural Science Foundation of China (51673205)the Key Research Program of Frontier Science,Chinese Academy of Sciences (QYZDJ-SSW-SLH056)。
文摘We link different microstructures to tribological behaviors of Ti-50.8 Ni(mole fraction, %) in reciprocating mode at room temperature(20 ℃). Hot-rolled alloys with B2 phase exhibit lower coefficient of friction and wear rate compared to the ones with B19?. Stress-induced martensitic transformation occurs during sliding. However, multi-pass hot rolling weakens the wear resistance. In this study, microstructures were characterized through electron backscatter diffraction and transmission electron microscopy(EBSD/TEM). From the concept of energy conservation, the effects of weak intensity of hot-rolled textures on the wear resistance are minimal. Based on the result that the alloy with a higher portion of coincidence site lattice boundaries shows lower martensitic start transformation temperature in the DSC curves than that with higher KAM values, the delay on B2-B19? transformation from {112}B2 twins outweighs dislocations. Moreover, widely distributed small-angle grain boundaries owing to dynamic recovery improve the wear resistance effectively compared to those that are well-recrystallized.
基金This work was supported by Beijing Terry Fox Run Foundation of Cancer Foundation of China(No.LC2016B10)Chinese Academy of Medical Sciences Initiative for Innovative Medicine(CAMS-2017-I2M-4-002)Postgraduate Innovation Fund Project of Peking Union Medical College in 2018(2018-1002-02-26).
文摘Background and objective:Intra-corporeal delta-shaped anastomosis(IDA)is an important development in laparoscopic digestive-tract reconstruction.We applied it in laparoscopic right hemicolectomy for right colon cancer and compared the short-term outcomes between the patients treated with IDA and conventional extracorporeal anastomosis(EA).Methods:Between 1 January 2016 and 1 October 2017,36 and 50 patients who underwent IDA and EA,respectively,were included.Data on clinicopathological characteristics,surgical outcomes,post-operative recovery and complications were collected and compared between the two groups.Results:Surgical outcomes and clinicopathological characteristics were similar between the two groups except the length of incision,which was significantly shorter in the IDA group than in the EA group(4.660.6 vs 5.660.7 cm,P<0.001).The time to ground activities,fluid diet intake and post-operative hospitalization did not differ between the groups;however,the time to first flatus was significantly shorter in the IDA group than in the EA group(2.860.5 vs 3.260.8 days,P=0.004).The post-operative visual analogue scale for pain was lower in the IDA group than in the EA group on post-operative Day 1(4.060.7 vs 4.561.0,P=0.002)and post-operative Day 3(2.760.6 vs 3.460.6,P<0.001).The surgical complication rates were 8.3 and 16.0%in the IDA and EA groups(P=0.470),respectively.No complications such as anastomotic bleeding,stenosis and leakage occurred in any patient.Conclusions:IDA is safe and feasible and shows more satisfactory short-term outcomes than EA.
