In order to investigate the real-time cracking behavior of each component of a composite with strong interfacial bonding among lamellae, Ti-18 Nb(at.%) composite was prepared by spark plasma sintering(SPS), followed b...In order to investigate the real-time cracking behavior of each component of a composite with strong interfacial bonding among lamellae, Ti-18 Nb(at.%) composite was prepared by spark plasma sintering(SPS), followed by hot-rolling, annealing, and quenching. The microstructure and mechanical properties were characterized by scanning electron microscopy(SEM), energy dispersive spectroscopy(EDS), micro-region X-ray diffractometry(MRXRD), nanoindentation, and in-situ scanning electron microscopy tensile testing. The results show that the Ti-18 Nb consists of Ti-enriched, diffusion and Nb-enriched zones, and the sharp Nb gradient across different zones leads to inhomogeneous distribution of phase and mechanical properties. A remarkable finding is that the diffusion zones not only enable the cooperative deformation between the brittle Ti-enriched zones and the ductile Nb-enriched zones but also act as the crack-arresters to prevent the local cracks in the Ti-enriched zones from further propagating across the composite.展开更多
Cu47Ti33Zr11Ni6Sn2Si1-based bulk metallic glass matrix composites reinforced with tungsten wires were fabricated by infiltration process at different temperatures (850, 900, 950 and 1000 °C) and time (10, 20 a...Cu47Ti33Zr11Ni6Sn2Si1-based bulk metallic glass matrix composites reinforced with tungsten wires were fabricated by infiltration process at different temperatures (850, 900, 950 and 1000 °C) and time (10, 20 and 30 min) in a quartz or a steel tube. The mechanical tests were carried out by scanning electron microscopy (SEM) and X-ray diffraction (XRD). The results show that the maximum strength and total strain of the composite are 1778 MPa and 2.8% fabricated in steel tube at 900 °C for 10 min, and 1582 MPa and 3.6% fabricated in quartz tube at 850 °C for 10 min, respectively.展开更多
Two kinds of bi-metal composite parts (Sn-15%Pb and Pb-22%Sn bi-metal system, and Al-7%Si and SiCp/6061 MMC bi-metal system) were prepared by the strain-induced melt activated thixo-forging. The interfaces of the bi...Two kinds of bi-metal composite parts (Sn-15%Pb and Pb-22%Sn bi-metal system, and Al-7%Si and SiCp/6061 MMC bi-metal system) were prepared by the strain-induced melt activated thixo-forging. The interfaces of the bi-metal composites were observed by OM and SEM. The observations show that the semisolid metals keep independence during thixo-forging. The solid phases in the semisolid slurries maintain their original morphologies after thixo-forging. The liquid phases near the interface mix together and form a thin layer. The interfaces are bonded firmly with the metallurgical bonding. No oxide layers are found at the interfaces. Strengths of the interfaces were investigated by the micro-hardness test. The experimental results show that the composite interfaces have high strength. However, the agglomerated enhancing particles cause fine defect on the interface of the Al-7%Si and SiCr/6061 MMC bi-metal composite.展开更多
This paper relates to the fabrication of aluminium matrix composites with various amounts of Al 2O 3 fiber and SiC whiskers by rheocasting, powder metallurgy process and liquid metal infiltration process. To analy...This paper relates to the fabrication of aluminium matrix composites with various amounts of Al 2O 3 fiber and SiC whiskers by rheocasting, powder metallurgy process and liquid metal infiltration process. To analyze wetting characteristics, the cross sections of composites are examined by scanning electron microscopy(SEM). The bending tests and microhardness tests are performed to evaluate mechanical properties of composites. The results show that the composites produced by liquid metal infiltration give better properties than those produced by rheocasting or powder metallurgy process, primarily due to the decrease of porosity and reinforcement cluster. For liquid metal infiltration composites, a good adhesion between the fiber and matrix is found. Three points bending test results show that there is an increase in flexural modulus with reinforcement contents. In addition, a series of microhardness tests are conducted to determine the effect of heat treatment on the mechanical property of Al 2O 3/Al composites.展开更多
The stress distribution surrounding the fastener hole in thick laminate mechanical joints is complex. It is time-consuming to analyze the distribution using finite element method. To accurately and efficiently obtain ...The stress distribution surrounding the fastener hole in thick laminate mechanical joints is complex. It is time-consuming to analyze the distribution using finite element method. To accurately and efficiently obtain the stress state around the fastener hole in multi-bolt thick laminate joints, a global-local approach is introduced. In the method, the most seriously damaged zone is 3D modeled by taking the displacement field got from the 2D global model as boundary conditions. Through comparison and analysis there are the following findings: the global-local finite element method is a reliable and efficient way to solve the stress distribution problem; the stress distribution around the fastener hole is quite uneven in through-the-thickness direction, and the stresses of the elements close to the shearing plane are much higher than the stresses of the elements far away from the shearing plane; the out-of-plane stresses introduced by the single-lap joint cannot be ignored due to the delamination failure; the stress state is a useful criterion for further more complex studies involving failure analysis.展开更多
In this paper,we present a review of electron transport properties of magnetic granular films.Magnetic granular films are nanocomposite materials which consist of magnetic nanoparticles embedded in a nonmagnetic matri...In this paper,we present a review of electron transport properties of magnetic granular films.Magnetic granular films are nanocomposite materials which consist of magnetic nanoparticles embedded in a nonmagnetic matrix or assembling of magnetic nanoparticles.According to the style of the nonmagnetic matrix,microstructure and the electron transport mechanism of the films,the magnetic granular films were divided into three groups:(1) magnetic metal-metal granular films,(2) magnetic metal-insulator granular films and(3) magnetic nanocluster-assembled granular films.Moreover,we also systematically review the magnetic properties,transport properties and magnetoresistance effect of size-monodispersed Co and Fe nanocluster-assembled films.展开更多
基金Project(51625404)supported by the National Natural Science Foundation for Distinguished Young Scholar of ChinaProjects(51604104,51504295)supported by the National Natural Science Foundation of China
文摘In order to investigate the real-time cracking behavior of each component of a composite with strong interfacial bonding among lamellae, Ti-18 Nb(at.%) composite was prepared by spark plasma sintering(SPS), followed by hot-rolling, annealing, and quenching. The microstructure and mechanical properties were characterized by scanning electron microscopy(SEM), energy dispersive spectroscopy(EDS), micro-region X-ray diffractometry(MRXRD), nanoindentation, and in-situ scanning electron microscopy tensile testing. The results show that the Ti-18 Nb consists of Ti-enriched, diffusion and Nb-enriched zones, and the sharp Nb gradient across different zones leads to inhomogeneous distribution of phase and mechanical properties. A remarkable finding is that the diffusion zones not only enable the cooperative deformation between the brittle Ti-enriched zones and the ductile Nb-enriched zones but also act as the crack-arresters to prevent the local cracks in the Ti-enriched zones from further propagating across the composite.
文摘Cu47Ti33Zr11Ni6Sn2Si1-based bulk metallic glass matrix composites reinforced with tungsten wires were fabricated by infiltration process at different temperatures (850, 900, 950 and 1000 °C) and time (10, 20 and 30 min) in a quartz or a steel tube. The mechanical tests were carried out by scanning electron microscopy (SEM) and X-ray diffraction (XRD). The results show that the maximum strength and total strain of the composite are 1778 MPa and 2.8% fabricated in steel tube at 900 °C for 10 min, and 1582 MPa and 3.6% fabricated in quartz tube at 850 °C for 10 min, respectively.
基金Project(1343-71333000469) supported by the Funding of Graduate Student Training of Central South University,China
文摘Two kinds of bi-metal composite parts (Sn-15%Pb and Pb-22%Sn bi-metal system, and Al-7%Si and SiCp/6061 MMC bi-metal system) were prepared by the strain-induced melt activated thixo-forging. The interfaces of the bi-metal composites were observed by OM and SEM. The observations show that the semisolid metals keep independence during thixo-forging. The solid phases in the semisolid slurries maintain their original morphologies after thixo-forging. The liquid phases near the interface mix together and form a thin layer. The interfaces are bonded firmly with the metallurgical bonding. No oxide layers are found at the interfaces. Strengths of the interfaces were investigated by the micro-hardness test. The experimental results show that the composite interfaces have high strength. However, the agglomerated enhancing particles cause fine defect on the interface of the Al-7%Si and SiCr/6061 MMC bi-metal composite.
文摘This paper relates to the fabrication of aluminium matrix composites with various amounts of Al 2O 3 fiber and SiC whiskers by rheocasting, powder metallurgy process and liquid metal infiltration process. To analyze wetting characteristics, the cross sections of composites are examined by scanning electron microscopy(SEM). The bending tests and microhardness tests are performed to evaluate mechanical properties of composites. The results show that the composites produced by liquid metal infiltration give better properties than those produced by rheocasting or powder metallurgy process, primarily due to the decrease of porosity and reinforcement cluster. For liquid metal infiltration composites, a good adhesion between the fiber and matrix is found. Three points bending test results show that there is an increase in flexural modulus with reinforcement contents. In addition, a series of microhardness tests are conducted to determine the effect of heat treatment on the mechanical property of Al 2O 3/Al composites.
文摘The stress distribution surrounding the fastener hole in thick laminate mechanical joints is complex. It is time-consuming to analyze the distribution using finite element method. To accurately and efficiently obtain the stress state around the fastener hole in multi-bolt thick laminate joints, a global-local approach is introduced. In the method, the most seriously damaged zone is 3D modeled by taking the displacement field got from the 2D global model as boundary conditions. Through comparison and analysis there are the following findings: the global-local finite element method is a reliable and efficient way to solve the stress distribution problem; the stress distribution around the fastener hole is quite uneven in through-the-thickness direction, and the stresses of the elements close to the shearing plane are much higher than the stresses of the elements far away from the shearing plane; the out-of-plane stresses introduced by the single-lap joint cannot be ignored due to the delamination failure; the stress state is a useful criterion for further more complex studies involving failure analysis.
基金supported by the National Basic Research Program of China (Grant No. 2012CB933103)the National Science Fund for Distinguished Young Scholars (Grant No. 50825101)the National Natural Science Foundation of China (Grant Nos. 50971108 and 51171158)
文摘In this paper,we present a review of electron transport properties of magnetic granular films.Magnetic granular films are nanocomposite materials which consist of magnetic nanoparticles embedded in a nonmagnetic matrix or assembling of magnetic nanoparticles.According to the style of the nonmagnetic matrix,microstructure and the electron transport mechanism of the films,the magnetic granular films were divided into three groups:(1) magnetic metal-metal granular films,(2) magnetic metal-insulator granular films and(3) magnetic nanocluster-assembled granular films.Moreover,we also systematically review the magnetic properties,transport properties and magnetoresistance effect of size-monodispersed Co and Fe nanocluster-assembled films.