Titanium-matrix composites have important and wide applications in the transport and aerospace industries. The current research was focused on powder metallurgy processing of in-situ reinforced titanium-matrix composi...Titanium-matrix composites have important and wide applications in the transport and aerospace industries. The current research was focused on powder metallurgy processing of in-situ reinforced titanium-matrix composite with Ti B whiskers. The Ti-6Al-4V alloy and B4 C additive powders were used as raw materials. Two different consolidation techniques, namely press-and-sintering and spark plasma sintering, were selected. It was observed that in-situ Ti B whiskers were formed during sintering in both methods. The changes in size, aspect ratio and distribution of in-situ whiskers in different composite samples were monitored. The effect of spark plasma sintering temperature on the synthesis of in-situ whiskers was also investigated. Based on the microstructural observations(optical microscopy and scanning electron microscopy) and the energy dispersive spectroscopy analysis, it was concluded that increasing the spark plasma sintering temperature from 900 to 1100 °C would lead to the complete formation of in-situ Ti B whiskers and reduced porosity content.展开更多
The mathematical models were developed to predict the ultimate tensile strength (UTS) and hardness of Al/TiB2 MMCs fabricated by in situ reaction process. The process parameters include temperature, reaction time an...The mathematical models were developed to predict the ultimate tensile strength (UTS) and hardness of Al/TiB2 MMCs fabricated by in situ reaction process. The process parameters include temperature, reaction time and mass fraction of TiB2. The in-situ casting was carried out based on three-factor five-level central composite rotatable design using response surface methodology (RSM). The validation of the model was carried out using ANOVA. The mathematical models developed for the mechanical properties were predicted at 95% confidence limit.展开更多
文摘Titanium-matrix composites have important and wide applications in the transport and aerospace industries. The current research was focused on powder metallurgy processing of in-situ reinforced titanium-matrix composite with Ti B whiskers. The Ti-6Al-4V alloy and B4 C additive powders were used as raw materials. Two different consolidation techniques, namely press-and-sintering and spark plasma sintering, were selected. It was observed that in-situ Ti B whiskers were formed during sintering in both methods. The changes in size, aspect ratio and distribution of in-situ whiskers in different composite samples were monitored. The effect of spark plasma sintering temperature on the synthesis of in-situ whiskers was also investigated. Based on the microstructural observations(optical microscopy and scanning electron microscopy) and the energy dispersive spectroscopy analysis, it was concluded that increasing the spark plasma sintering temperature from 900 to 1100 °C would lead to the complete formation of in-situ Ti B whiskers and reduced porosity content.
文摘The mathematical models were developed to predict the ultimate tensile strength (UTS) and hardness of Al/TiB2 MMCs fabricated by in situ reaction process. The process parameters include temperature, reaction time and mass fraction of TiB2. The in-situ casting was carried out based on three-factor five-level central composite rotatable design using response surface methodology (RSM). The validation of the model was carried out using ANOVA. The mathematical models developed for the mechanical properties were predicted at 95% confidence limit.