丸子技术在光电直读光谱分析中的应用

将过筛后的金属试料通过选定筛网在模具中压成圆片状丸子试样，直接在光电直读光谱仪上进行分析。所得数据偏差小于0．003，优于化学分析法测得结果。

A review on in vitro corrosion performance test of biodegradable metallic materials

Extensive in vitro corrosion test systems have been carried out to simulate the in vivo corrosion behavior of biodegradable metallic materials. Various methods have their own unique benefits and limitations. The corrosion mechanism of biodegradable alloys and in vitro corrosion test systems on biodegradable metallic materials are reviewed, to build a reasonable simulated in vitro test system for mimicking the in vivo animal test from the aspects of electrolyte solution selection, surface roughness influence, test methods and evaluation methodology of corrosion rate. Buffered simulated body fluid containing similar components to human blood plasma should be applied as electrolyte solution, such as simulated body fluid （SBF） and culture medium with serum. Surface roughness of samples and ratio of solution volume to sample surface area should be adopted based on the real implant situation, and the dynamic corrosion is preferred. As to the evaluation methodology of corrosion rate, different methods may complement one another.

Modeling and finite element analysis of transduction process of electromagnetic acoustic transducers for nonferromagnetic metal material testing

Facing the problems lack of considering the non-uniform distribution of the static bias magnetic field and computing the panicle displacements in the simulation model of electromagnetic acoustic transducer （EMAT）, a multi-field coupled model was established and the finite element method （FEM） was presented to calculate the entire transduction process. The multi-field coupled model included the static magnetic field, pulsed eddy current field and mechanical field. The FEM equations of the three fields were derived by Garlerkin FEM method. Thus, the entire transduction process of the EMAT was calculated through sequentially coupling the three fields. The transduction process of a Lamb wave EMAT was calculated according to the present model and method. The results show that, by the present method, it is valid to calculate the particle displacement under the given excitation signal and non-uniformly distributed static magnetic field. Calculation error will be brought about if the non-uniform distribution of the static bias magnetic field is neglected.

Research on Online Texture Measurements in Metal Rolling Field

In rolled strip material,the orientation of the crystallites,known as texture,is influenced by various kinds of thermo-mechanical processes,such as casting,plastic deformation,annealing and phase transformation. The modern industry production requires stable product performance,real-time monitoring and full controlling of the quality.The online texture measurement in metal rolling can be used to real-time monitor the whole process, and then feedback control to the production process can be implied to adjust the process parameters to ensure the stability of the products.The principles,advantages and disadvantages of related detection methods(2D X-ray diffraction,neutron diffraction,laser-ultrasonics and electromagnetic acoustic transducers(EMAT)) and the possibility of online measurement are discussed.Finally,2D X-ray diffraction and laser-ultrasonics are employed on online texture measurement,and the schemes of online texture measurement are proposed.

Generalized Aifantis strain gradient plasticity model with internal length scale dependence on grain size,sample size and strain

The internal length scale(ILS)is a dominant parameter in strain gradient plasticity(SGP)theories,which helps to successfully explain the size effect of metals at the microscale.However,the ILS is usually introduced into strain gradient frameworks for dimensional consistency and is model-dependent.Even now,its physical meaning,connection with the microstructure of the material,and dependence on the strain level have not been thoroughly elucidated.In the current work,Aifantis'SGP model is reformulated by incorporating a recently proposed power-law relation for strain-dependent ILS.A further extension of Aifantis'SGP model by including the grain size effect is conducted according to the Hall-Petch formulation,and then the predictions are compared with torsion experiments of thin wires.It is revealed that the ILS depends on the sample size and grain size simultaneously;these dependencies are dominated by the dislocation spacing and can be well described through the strain hardenmg exponent.Furthermore,both the original and generalized Aifantis models provide larger estimated values for the ILS than Fleck-Hutchinson's theory.

Composite structural modeling and tensile mechanical behavior of graphene reinforced metal matrix composites

Owing to its distinguished mechanical stiffness and strength, graphene has become an ideal reinforcing material in kinds of composite materials. In this work, the graphene（reduced graphene oxide） reinforced aluminum（Al）matrix composites were fabricated by flaky powder metallurgy. Tensile tests of pure Al matrix and graphene/Al composites with bioinspired layered structures are conducted.By means of an independently developed Python-based structural modeling program, three-dimensional microscopic structural models of graphene/Al composites can be established, in which the size, shape, orientation, location and content of graphene can be reconstructed in line with the actual graphene/Al composite structures. Elastoplastic mechanical properties, damaged materials behaviors, grapheneAl interfacial behaviors and reasonable boundary conditions are introduced and applied to perform the simulations. Based on the experimental and numerical tensile behaviors of graphene/Al composites, the effects of graphene morphology,graphene-Al interface, composite configuration and failure behavior within the tensile mechanical deformations of graphene/Al composites can be revealed and indicated, respectively.From the analysis above, a good understanding can be brought to light for the deformation mechanism of graphene/Al composites.