Thin plates of 21% Cr ferritic stainless steel welded by pulsed gas tungsten arc welding at different pulse frequencies were investigated for the microstructure characteristics and hardness behavior.The welds containe...Thin plates of 21% Cr ferritic stainless steel welded by pulsed gas tungsten arc welding at different pulse frequencies were investigated for the microstructure characteristics and hardness behavior.The welds contained columnar grains in the outer part and fine equiaxed grains in the central region due to the pulsed process.展开更多
Carbon encapsulated iron nanoparticles (CEINPs) with very thin shells and good core-shell structures were prepared by DC arc discharge at argon intake temperature (AIT) of 800 ℃. The results of high resolution tr...Carbon encapsulated iron nanoparticles (CEINPs) with very thin shells and good core-shell structures were prepared by DC arc discharge at argon intake temperature (AIT) of 800 ℃. The results of high resolution transmission electron microscope (HRTEM), energy dispersive X-ray (EDX) spectroscope, X-ray diffraction (XRD), and X-ray photoelectron spectroscope (XPS) characterizations on the product B show that the thickness of the carbon shells of CEINPs in the product B is in the range of ca. 0.5-5.3 nm, i. e., which can be as thin as only two layers of graphite. The average diameter of the CEINPs is about 24. 7 nm. The total content of Fe element in the product B is 77.0 wt%. The saturation magnetization (Ms) and coercivity (Hc) of the product B are 107.4 emu/g and 143 Oe. resnectivelv. The formation of the CEINPs in the oroduct B is discussed briefly.展开更多
文摘Thin plates of 21% Cr ferritic stainless steel welded by pulsed gas tungsten arc welding at different pulse frequencies were investigated for the microstructure characteristics and hardness behavior.The welds contained columnar grains in the outer part and fine equiaxed grains in the central region due to the pulsed process.
文摘Carbon encapsulated iron nanoparticles (CEINPs) with very thin shells and good core-shell structures were prepared by DC arc discharge at argon intake temperature (AIT) of 800 ℃. The results of high resolution transmission electron microscope (HRTEM), energy dispersive X-ray (EDX) spectroscope, X-ray diffraction (XRD), and X-ray photoelectron spectroscope (XPS) characterizations on the product B show that the thickness of the carbon shells of CEINPs in the product B is in the range of ca. 0.5-5.3 nm, i. e., which can be as thin as only two layers of graphite. The average diameter of the CEINPs is about 24. 7 nm. The total content of Fe element in the product B is 77.0 wt%. The saturation magnetization (Ms) and coercivity (Hc) of the product B are 107.4 emu/g and 143 Oe. resnectivelv. The formation of the CEINPs in the oroduct B is discussed briefly.