The microstructure and magnetic properties of cold rolled non-oriented electrical steel,annealed at 200-1 000 ℃ for 0-240 min with different heating rates,were investigated by optical microscopy,scanning electron mic...The microstructure and magnetic properties of cold rolled non-oriented electrical steel,annealed at 200-1 000 ℃ for 0-240 min with different heating rates,were investigated by optical microscopy,scanning electron microscopy,Epstein frame,and transmission electron microscopy. The results show that the magnetic properties of cold rolled non-oriented electrical steel can be improved by controlling the annealing process to obtain uniform coarse grains with critical sizes after the recovery,recrystallization and growth of grains. Additionally,the annealing temperature influences the magnetic properties more significantly than annealing time,and with the increase of heating-up rate during the annealing process,the magnetic properties of the cold rolled non-oriented electrical steel increase.展开更多
Field emission-scanning electron microscopy(FE-SEM) technique was employed to observe the shape, size and distribution of AlN+MnS inclusions in oriented electrical steels. Specimens used for FE-SEM observation were de...Field emission-scanning electron microscopy(FE-SEM) technique was employed to observe the shape, size and distribution of AlN+MnS inclusions in oriented electrical steels. Specimens used for FE-SEM observation were deeply electrolytic etched at room temperature in non-aqueous acetylacetone(AA) solution. The results indicate that the FE-SEM technique has obvious advantage in specimen preparation. Therefore, it can be easily used to identify the AlN+MnS inclusions and even copper nano-particles in oriented electrical steels with the same analysis accuracy as that by TEM. This technique is a good substitute for TEM and the associated specimen preparation in the observation of inclusions in electrical steels. It will be a powerful technique for routine analysis in the production of grain oriented electrical steels.展开更多
基金Projects(2006-38a) supported by Hunan Valin Lianyuan Iron and Steel Company
文摘The microstructure and magnetic properties of cold rolled non-oriented electrical steel,annealed at 200-1 000 ℃ for 0-240 min with different heating rates,were investigated by optical microscopy,scanning electron microscopy,Epstein frame,and transmission electron microscopy. The results show that the magnetic properties of cold rolled non-oriented electrical steel can be improved by controlling the annealing process to obtain uniform coarse grains with critical sizes after the recovery,recrystallization and growth of grains. Additionally,the annealing temperature influences the magnetic properties more significantly than annealing time,and with the increase of heating-up rate during the annealing process,the magnetic properties of the cold rolled non-oriented electrical steel increase.
基金Project(50471104) supported by the National Natural Science Foundation of China
文摘Field emission-scanning electron microscopy(FE-SEM) technique was employed to observe the shape, size and distribution of AlN+MnS inclusions in oriented electrical steels. Specimens used for FE-SEM observation were deeply electrolytic etched at room temperature in non-aqueous acetylacetone(AA) solution. The results indicate that the FE-SEM technique has obvious advantage in specimen preparation. Therefore, it can be easily used to identify the AlN+MnS inclusions and even copper nano-particles in oriented electrical steels with the same analysis accuracy as that by TEM. This technique is a good substitute for TEM and the associated specimen preparation in the observation of inclusions in electrical steels. It will be a powerful technique for routine analysis in the production of grain oriented electrical steels.
