In order to improve the quality of clad ingots, diverse physical fields including electromagnetic stirring, power ultrasonic and compound field of ultrasonic and electromagnetic stirring were attempted to prepare clad...In order to improve the quality of clad ingots, diverse physical fields including electromagnetic stirring, power ultrasonic and compound field of ultrasonic and electromagnetic stirring were attempted to prepare clad ingots of 3003/4004 alloys. The solidification structures near the interface in clad ingots were investigated. The experiment results indicate that the solidification structure of 4004 alloy changes from dendritic crystals to petal-like grains when the clad ingot is treated by electromagnetic stirring. With the effect of power ultrasonic, the solidified microstructure of 4004 alloy exhibits the refinement of both primary a(A1) and eutectic silicon. Under the compound field, the primary a(A1) is refined, the morphology of eutectic silicon has a transition from a coarse plate-like form without treatment or thin acicular-like form with power ultrasonic to fine coral-like form.展开更多
Three-layer composite ingot of 4045/3004/4045 aluminum alloys was prepared by direct-chill semi-continuous casting process,the temperature field distribution near the composite interface,macro-morphology,microstructur...Three-layer composite ingot of 4045/3004/4045 aluminum alloys was prepared by direct-chill semi-continuous casting process,the temperature field distribution near the composite interface,macro-morphology,microstructure and composition distribution of the composite interface were investigated.The results show that semi-solid layer with a certain thickness forms near the interface due to the effect of cooling plate,which ensures successful implementation of casting the composite ingot.Two different aluminum alloys are well bonded metallurgically.The mechanical properties of composite interface were measured,the tensile and shearing strengths of composite interface are 105 and 88 MPa,respectively,which proves that the composite interface is a kind of metallurgical bonding.展开更多
AA4045/AA3003 cladding billet was prepared by direct chill semi-continuous casting process. The macrostructures, microstructures, temperature distribution, compositions distribution and the mechanical properties at th...AA4045/AA3003 cladding billet was prepared by direct chill semi-continuous casting process. The macrostructures, microstructures, temperature distribution, compositions distribution and the mechanical properties at the bonding interface were investigated in detail. The results show that the cladding billet with few defects could be obtained by semi-continuous casting process. At the interface, diffusion layer of about 10μm on average formed between the two alloys due to the diffusion of alloy elements in the temperature range from 596 to 632 °C. From the side of AA4045 to the side of AA3003, the Si content has a trend to decrease, while the Mn content has a trend to increase gradually. Tensile strength of the cladding billet reaches 103.7 MPa, the fractured position is located on the AA3003 side, and the shearing strength is 91.1 MPa, revealing that the two alloys were combined metallurgically by mutual diffusion of alloy elements.展开更多
In order to investigate the existing form and action mechanism of minor scandium (Sc) and zirconium (Zr) in AI-Cu-Mg alloy, microstructures of Al-4Cu-1Mg-Sc-Zr alloy under different conditions, including states of...In order to investigate the existing form and action mechanism of minor scandium (Sc) and zirconium (Zr) in AI-Cu-Mg alloy, microstructures of Al-4Cu-1Mg-Sc-Zr alloy under different conditions, including states of as-cast, homogenized, hot-rolled, as-solution and natural aged, were observed by scanning electron microscopy (SEM), X-ray diffractometry (XRD) and transmission electron microscopy (TEM). It is revealed that Sc and Zr are completely dissolved into the supersaturated solid solution in as-cast ingot, but grain refinement is not observed. Coffee-bean-like AI3(Sc, Zr) particles deposit during homogenization of ingot induce an increase in hardness. Al3(Sc, Zr) particles are slightly coarsened in as-solution samples, but they still maintain coherent to matrix, which indicates a high thermal stability of these particles. Good coherency ofAl3(Sc, Zr) particles makes some benefits for inhibiting recrystallization and reserving work-hardening.展开更多
The actual effective partition coefficients of Mg and Cr in a cross-section of a dendrite arm in a direct-chill(DC)-casting ingot of 7475 aluminum alloy are obtained.Meanwhile,by analyzing the microstructure,the mecha...The actual effective partition coefficients of Mg and Cr in a cross-section of a dendrite arm in a direct-chill(DC)-casting ingot of 7475 aluminum alloy are obtained.Meanwhile,by analyzing the microstructure,the mechanism of the heterogeneous distribution of E(Al_(18)Mg_(3)Cr_(2))dispersoids in this DC ingot is revealed.The results show that the actual effective partition coefficients of Mg and Cr are 0.650 and 1.392,respectively,and they describe the heterogeneous distributions of Mg and Cr along the direction of radius of the cross-section of the dendrite arm of the alloy.After homogenization treatment at 470℃ for 24 h,Mg diffuses uniformly,but Cr hardly diffuses.Both the concentrations of Mg and Cr and the sites of heterogeneous nucleation in the alloy are the determinants of the formation of E dispersoids simultaneously.The heat treatment at 250℃ for 72 h provides a large number of the sites of heterogeneous nucleation of the formation of fine E dispersoids that will be formed in the center of the cross-section during the subsequent heat treatment at higher temperature.展开更多
With the experiment and finite element simulation, the influences of power ultrasonic on the solidification structure of 7050 aluminum alloy ingot in semi-continuous casting were researched, and the effects of casting...With the experiment and finite element simulation, the influences of power ultrasonic on the solidification structure of 7050 aluminum alloy ingot in semi-continuous casting were researched, and the effects of casting speed on solidification structure in ultrasonic field were also analyzed. The experiment and simulation results show that the solidification structure of the ingot is homogeneously distributed, and its grain size is obviously refined at ultrasonic power of 240 W. The average grain sizes, which can be seen from the Leica microscope, are less than 100 μm. When the casting speed is 45-50 mm/min, the best grain refinement is obtained.展开更多
基金Project(51074031)supported by the National Natural Science Foundation of ChinaProject supported by the Korea National Project
文摘In order to improve the quality of clad ingots, diverse physical fields including electromagnetic stirring, power ultrasonic and compound field of ultrasonic and electromagnetic stirring were attempted to prepare clad ingots of 3003/4004 alloys. The solidification structures near the interface in clad ingots were investigated. The experiment results indicate that the solidification structure of 4004 alloy changes from dendritic crystals to petal-like grains when the clad ingot is treated by electromagnetic stirring. With the effect of power ultrasonic, the solidified microstructure of 4004 alloy exhibits the refinement of both primary a(A1) and eutectic silicon. Under the compound field, the primary a(A1) is refined, the morphology of eutectic silicon has a transition from a coarse plate-like form without treatment or thin acicular-like form with power ultrasonic to fine coral-like form.
基金Project (2005CB623707) supported by the National Basic Research Program of China
文摘Three-layer composite ingot of 4045/3004/4045 aluminum alloys was prepared by direct-chill semi-continuous casting process,the temperature field distribution near the composite interface,macro-morphology,microstructure and composition distribution of the composite interface were investigated.The results show that semi-solid layer with a certain thickness forms near the interface due to the effect of cooling plate,which ensures successful implementation of casting the composite ingot.Two different aluminum alloys are well bonded metallurgically.The mechanical properties of composite interface were measured,the tensile and shearing strengths of composite interface are 105 and 88 MPa,respectively,which proves that the composite interface is a kind of metallurgical bonding.
基金Project(2012CB723307)supported by the National Basic Research Program of ChinaProject(51204046)supported by the National Natural Science Foundation of ChinaProject(20130042130001)supported by the Doctoral Fund of Ministry of Education of China
文摘AA4045/AA3003 cladding billet was prepared by direct chill semi-continuous casting process. The macrostructures, microstructures, temperature distribution, compositions distribution and the mechanical properties at the bonding interface were investigated in detail. The results show that the cladding billet with few defects could be obtained by semi-continuous casting process. At the interface, diffusion layer of about 10μm on average formed between the two alloys due to the diffusion of alloy elements in the temperature range from 596 to 632 °C. From the side of AA4045 to the side of AA3003, the Si content has a trend to decrease, while the Mn content has a trend to increase gradually. Tensile strength of the cladding billet reaches 103.7 MPa, the fractured position is located on the AA3003 side, and the shearing strength is 91.1 MPa, revealing that the two alloys were combined metallurgically by mutual diffusion of alloy elements.
基金Project(2005DFA50550) supported by International Science and Technology Cooperation Program of ChinaProject(2005CB623705) supported by the National Basic Research Program of China
文摘In order to investigate the existing form and action mechanism of minor scandium (Sc) and zirconium (Zr) in AI-Cu-Mg alloy, microstructures of Al-4Cu-1Mg-Sc-Zr alloy under different conditions, including states of as-cast, homogenized, hot-rolled, as-solution and natural aged, were observed by scanning electron microscopy (SEM), X-ray diffractometry (XRD) and transmission electron microscopy (TEM). It is revealed that Sc and Zr are completely dissolved into the supersaturated solid solution in as-cast ingot, but grain refinement is not observed. Coffee-bean-like AI3(Sc, Zr) particles deposit during homogenization of ingot induce an increase in hardness. Al3(Sc, Zr) particles are slightly coarsened in as-solution samples, but they still maintain coherent to matrix, which indicates a high thermal stability of these particles. Good coherency ofAl3(Sc, Zr) particles makes some benefits for inhibiting recrystallization and reserving work-hardening.
基金financially supported by the National Natural Science Foundation of China(No.51871043)Fundamental Research Funds for the Central Universities of China(No.N180212010)Liaoning Natural Science Foundation of China(No.2019-MS-113)。
文摘The actual effective partition coefficients of Mg and Cr in a cross-section of a dendrite arm in a direct-chill(DC)-casting ingot of 7475 aluminum alloy are obtained.Meanwhile,by analyzing the microstructure,the mechanism of the heterogeneous distribution of E(Al_(18)Mg_(3)Cr_(2))dispersoids in this DC ingot is revealed.The results show that the actual effective partition coefficients of Mg and Cr are 0.650 and 1.392,respectively,and they describe the heterogeneous distributions of Mg and Cr along the direction of radius of the cross-section of the dendrite arm of the alloy.After homogenization treatment at 470℃ for 24 h,Mg diffuses uniformly,but Cr hardly diffuses.Both the concentrations of Mg and Cr and the sites of heterogeneous nucleation in the alloy are the determinants of the formation of E dispersoids simultaneously.The heat treatment at 250℃ for 72 h provides a large number of the sites of heterogeneous nucleation of the formation of fine E dispersoids that will be formed in the center of the cross-section during the subsequent heat treatment at higher temperature.
基金Project(2010CB731700) supported by the National Basic Research Program of China
文摘With the experiment and finite element simulation, the influences of power ultrasonic on the solidification structure of 7050 aluminum alloy ingot in semi-continuous casting were researched, and the effects of casting speed on solidification structure in ultrasonic field were also analyzed. The experiment and simulation results show that the solidification structure of the ingot is homogeneously distributed, and its grain size is obviously refined at ultrasonic power of 240 W. The average grain sizes, which can be seen from the Leica microscope, are less than 100 μm. When the casting speed is 45-50 mm/min, the best grain refinement is obtained.