This work provides a general method for preparing monodisperse, water-soluble and paramagnetic magnetic nanoparticles which are easy to be modified. Firstly, magnetic silica with core-shell structure was prepared acco...This work provides a general method for preparing monodisperse, water-soluble and paramagnetic magnetic nanoparticles which are easy to be modified. Firstly, magnetic silica with core-shell structure was prepared according to a previous work. Then, the magnetic silica was treated with alkali solution to afford magnetic nanoparticles. With the increase of calcination temperature for the preparation of magnetic silica, the crystallinity and the magnetic responsibility of magnetic silica strengthened, meanwhile, the corresponding magnetic nanoparticles kept monodisperse without any aggregation. The magnetic nanoparticles are comprised of cobalt ferrite and a silica coating. The silica coating on the cobalt ferrite facilitates the magnetic nanoparticles well-dissolved and monodisperse in water, and easilv modified.展开更多
A FEM model for a failed industrial example of roll forging was established to analyze the generation mechanisms of the mismatch of size and shape of two spring board.To demonstrate the formulation of these defects,th...A FEM model for a failed industrial example of roll forging was established to analyze the generation mechanisms of the mismatch of size and shape of two spring board.To demonstrate the formulation of these defects,the bites condition and contact status between rectangular groove and workpiece during rolling the first and second spring boards were analyzed.Then,a new oval-diamond groove combining oval groove and diamond groove was presented to eliminate these defects.By analyzing field variables under the same deformation degree,the larger friction can be obtained on the contact surface of workpiece and the oval-diamond groove.The physical experiment validates that the oval-diamond groove can eliminate these defects effectively,and the size of part is in good agreement with design requirement.展开更多
基金Supported by the National Natural Science Foundation of China(20976013)
文摘This work provides a general method for preparing monodisperse, water-soluble and paramagnetic magnetic nanoparticles which are easy to be modified. Firstly, magnetic silica with core-shell structure was prepared according to a previous work. Then, the magnetic silica was treated with alkali solution to afford magnetic nanoparticles. With the increase of calcination temperature for the preparation of magnetic silica, the crystallinity and the magnetic responsibility of magnetic silica strengthened, meanwhile, the corresponding magnetic nanoparticles kept monodisperse without any aggregation. The magnetic nanoparticles are comprised of cobalt ferrite and a silica coating. The silica coating on the cobalt ferrite facilitates the magnetic nanoparticles well-dissolved and monodisperse in water, and easilv modified.
基金Project(51275543)supported by the National Natural Science Foundation of ChinaProject(cstc2009aa3012-1)supported by the Key Program of Chongqing Science and Technology Foundation,China
文摘A FEM model for a failed industrial example of roll forging was established to analyze the generation mechanisms of the mismatch of size and shape of two spring board.To demonstrate the formulation of these defects,the bites condition and contact status between rectangular groove and workpiece during rolling the first and second spring boards were analyzed.Then,a new oval-diamond groove combining oval groove and diamond groove was presented to eliminate these defects.By analyzing field variables under the same deformation degree,the larger friction can be obtained on the contact surface of workpiece and the oval-diamond groove.The physical experiment validates that the oval-diamond groove can eliminate these defects effectively,and the size of part is in good agreement with design requirement.
