Microstructure and mechanical properties of AZ61 Mg alloy during isothermal multi-axial forging （MAF） were studied. The mechanisms of grain refinement and relationship between the microstructures and mechanical prop...Microstructure and mechanical properties of AZ61 Mg alloy during isothermal multi-axial forging （MAF） were studied. The mechanisms of grain refinement and relationship between the microstructures and mechanical properties were discussed. The results show that the average grain size decreases with increasing the number of MAF passes. The grains are significantly refined at the 1st and 2nd MAF passes, and gradually refined at higher MAF passes. The initial grain size of 148 lam decreases to about 14 gm after 6 MAF passes. The grain refinement occurs mainly by continuous dynamic recrystallization. With increasing the MAF passes, both the tensile strength and the elongation to failure of the alloy are significantly enhanced.展开更多
The mechanical properties, microstructure and tensile fracture of Ti-6.5AI-IMo-IV-2Zr large section bars produced by three diffrent forging processes were investigated. The results show that when billet forging and fi...The mechanical properties, microstructure and tensile fracture of Ti-6.5AI-IMo-IV-2Zr large section bars produced by three diffrent forging processes were investigated. The results show that when billet forging and finish forging were conducted by means of fullering at high and low temperature of r-region, respectively; the microstructure of forged bar is coarse Widmanstaten structure; the mechanical properties, especially the reduction of cross-sectional area, are poor, and the room temperature tensile fracture presents a brittle feature. While billet forging was carried out by upset-fullering at high temperature of the r-region, and finish forging was proceeded through fullering at （a＋fl）-region, the microstructure of forged bar was a duplex structure, the bar has better comprehensive mechanical properties, and the room temperature tensile fracture reveals a ductile feature. In order to obtain qualified Ti-6.SAI-IMo-IV-2Zr alloy bar, it is the key that as-cast microstructure should be completely broken during billet forging, and the forging temperature and deformation are also well controlled upon finishing forging.展开更多
In order to reveal the differences caused by forging and rolling process for titanium ingots, hot compression behavior, mechanical properties and the microstructures of forged billets and rolled ones were investigated...In order to reveal the differences caused by forging and rolling process for titanium ingots, hot compression behavior, mechanical properties and the microstructures of forged billets and rolled ones were investigated in detail using Gleeble-1500 thermal mechanical simulator, universal testing machine and optical microscope （OM）. The compression deformation experimental data of commercially pure titanium （CP-Ti） were mapped to be a T vs lg diagram in which data fall into three distinct regions, i.e., three-stage work hardening, two-stage work hardening and flow softening, which can be separated by border lines at 17.5 and 15.4 for lg Z, where Z represents the Zener-Hollomon parameter. The deformation twin is found to have higher Z-value corresponding to the work hardening region. The differences in microstructures and mechanical properties for two kinds of billets indicate that forged billet consists of deformation twins and some twin intersections, and many twins cross the grain boundaries. However, nearly no twins can be seen in the microstructure of billet formed by rolling under optical microscope （OM）, but there are equiaxed and platelike grains. Tensile tests and Vickers hardness test indicate that yield strength, tensile strength and microhardness of the samples after forging are higher than those after rolling.展开更多
TiC nanoparticle-reinforced Mg−4Zn−0.5Ca matrix nanocomposites were processed by combining multidirectional forging(MDF)and extrusion(EX).The grain size of the nanocomposite after MDF+EX multi-step deformation was sig...TiC nanoparticle-reinforced Mg−4Zn−0.5Ca matrix nanocomposites were processed by combining multidirectional forging(MDF)and extrusion(EX).The grain size of the nanocomposite after MDF+EX multi-step deformation was significantly decreased compared with that processed only by MDF.The average size of the recrystallized grains gradually increased after EX with increasing the number of MDF passes at 270℃.However,the grain size significantly decreased by MDF processing at 310℃.Both fine and coarse MgZn2 phases appeared in the(MDF+EX)-processed nanocomposites,and their volume fractions gradually increased with increasing the number of MDF passes before EX.Ultrahigh tensile properties(yield strength of^404 MPa,ultimate tensile strength of^450.3 MPa and elongation of^5.2%)were obtained in the nanocomposite after three MDF passes at 310℃ followed by EX.This was attributed to the refinement of the recrystallized grains,together with the improved Orowan strengthening provided by the precipitated MgZn2 particles that were generated by MDF+EX multi-step deformation.展开更多
To improve the environmental benefits and solve the problems of large shrinkage and high brittleness, the partial replacement of calcined kaolin by fly ash as a raw material for geopolymer synthesis and the influences...To improve the environmental benefits and solve the problems of large shrinkage and high brittleness, the partial replacement of calcined kaolin by fly ash as a raw material for geopolymer synthesis and the influences of polypropylene (PP) fiber on the mechanical properties and volume stability were investigated. The results show that compressive strength of the geopolymer containing 33.3%(mass fraction) fly ash by steam curing at 80 ℃ for 6 d is improved by 35.5%. The 3-day compressive strength, flexural strength and impacting energy of geopolymers containing 0.05%PP fiber increase by 67.8%, 36.1% and 6.25%, while the shrinkage and modulus of compressibility decrease by 38.6% and 31.3%, respectively. The results of scanning electron microscopy (SEM) and the appearances of crack growths confirm that PP fiber can offer a bridging effect over the harmful pores and defects and change the expanding ways of cracks, resulting in a great improvement of strength and toughness.展开更多
文摘Microstructure and mechanical properties of AZ61 Mg alloy during isothermal multi-axial forging （MAF） were studied. The mechanisms of grain refinement and relationship between the microstructures and mechanical properties were discussed. The results show that the average grain size decreases with increasing the number of MAF passes. The grains are significantly refined at the 1st and 2nd MAF passes, and gradually refined at higher MAF passes. The initial grain size of 148 lam decreases to about 14 gm after 6 MAF passes. The grain refinement occurs mainly by continuous dynamic recrystallization. With increasing the MAF passes, both the tensile strength and the elongation to failure of the alloy are significantly enhanced.
文摘The mechanical properties, microstructure and tensile fracture of Ti-6.5AI-IMo-IV-2Zr large section bars produced by three diffrent forging processes were investigated. The results show that when billet forging and finish forging were conducted by means of fullering at high and low temperature of r-region, respectively; the microstructure of forged bar is coarse Widmanstaten structure; the mechanical properties, especially the reduction of cross-sectional area, are poor, and the room temperature tensile fracture presents a brittle feature. While billet forging was carried out by upset-fullering at high temperature of the r-region, and finish forging was proceeded through fullering at （a＋fl）-region, the microstructure of forged bar was a duplex structure, the bar has better comprehensive mechanical properties, and the room temperature tensile fracture reveals a ductile feature. In order to obtain qualified Ti-6.SAI-IMo-IV-2Zr alloy bar, it is the key that as-cast microstructure should be completely broken during billet forging, and the forging temperature and deformation are also well controlled upon finishing forging.
文摘In order to reveal the differences caused by forging and rolling process for titanium ingots, hot compression behavior, mechanical properties and the microstructures of forged billets and rolled ones were investigated in detail using Gleeble-1500 thermal mechanical simulator, universal testing machine and optical microscope （OM）. The compression deformation experimental data of commercially pure titanium （CP-Ti） were mapped to be a T vs lg diagram in which data fall into three distinct regions, i.e., three-stage work hardening, two-stage work hardening and flow softening, which can be separated by border lines at 17.5 and 15.4 for lg Z, where Z represents the Zener-Hollomon parameter. The deformation twin is found to have higher Z-value corresponding to the work hardening region. The differences in microstructures and mechanical properties for two kinds of billets indicate that forged billet consists of deformation twins and some twin intersections, and many twins cross the grain boundaries. However, nearly no twins can be seen in the microstructure of billet formed by rolling under optical microscope （OM）, but there are equiaxed and platelike grains. Tensile tests and Vickers hardness test indicate that yield strength, tensile strength and microhardness of the samples after forging are higher than those after rolling.
基金Projects(51771129,51401144,51771128)supported by the National Natural Science Foundation of China,Project supported by the Outstanding Innovative Teams of Higher Learning Institutions of Shanxi,ChinaProjects(2015021067,201601D011034)supported by the Natural Science Foundation of Shanxi Province,China+1 种基金Project(201703D421039)supported by the International Cooperation in Shanxi,ChinaProject supported by the China Scholarship Council。
文摘TiC nanoparticle-reinforced Mg−4Zn−0.5Ca matrix nanocomposites were processed by combining multidirectional forging(MDF)and extrusion(EX).The grain size of the nanocomposite after MDF+EX multi-step deformation was significantly decreased compared with that processed only by MDF.The average size of the recrystallized grains gradually increased after EX with increasing the number of MDF passes at 270℃.However,the grain size significantly decreased by MDF processing at 310℃.Both fine and coarse MgZn2 phases appeared in the(MDF+EX)-processed nanocomposites,and their volume fractions gradually increased with increasing the number of MDF passes before EX.Ultrahigh tensile properties(yield strength of^404 MPa,ultimate tensile strength of^450.3 MPa and elongation of^5.2%)were obtained in the nanocomposite after three MDF passes at 310℃ followed by EX.This was attributed to the refinement of the recrystallized grains,together with the improved Orowan strengthening provided by the precipitated MgZn2 particles that were generated by MDF+EX multi-step deformation.
基金Project(2006AA06Z225) supported by the National High-Tech Research and Development Program of China
文摘To improve the environmental benefits and solve the problems of large shrinkage and high brittleness, the partial replacement of calcined kaolin by fly ash as a raw material for geopolymer synthesis and the influences of polypropylene (PP) fiber on the mechanical properties and volume stability were investigated. The results show that compressive strength of the geopolymer containing 33.3%(mass fraction) fly ash by steam curing at 80 ℃ for 6 d is improved by 35.5%. The 3-day compressive strength, flexural strength and impacting energy of geopolymers containing 0.05%PP fiber increase by 67.8%, 36.1% and 6.25%, while the shrinkage and modulus of compressibility decrease by 38.6% and 31.3%, respectively. The results of scanning electron microscopy (SEM) and the appearances of crack growths confirm that PP fiber can offer a bridging effect over the harmful pores and defects and change the expanding ways of cracks, resulting in a great improvement of strength and toughness.
