Two experimental single crystal superalloys, Ru-free alloy and Ru-containing alloy with [001] orientation, other alloying element contents being basically kept same, were cast in the directionally solidified furnace. ...Two experimental single crystal superalloys, Ru-free alloy and Ru-containing alloy with [001] orientation, other alloying element contents being basically kept same, were cast in the directionally solidified furnace. The effect of Ru on the stress rupture properties of the single crystal superalloy was investigated at (980 ℃, 250 MPa), (1100 ℃, 140 MPa) and (1120 ℃, 140 MPa). The results show that Ru can enhance high temperature stress rupture properties of single crystal superalloy. The improvement effect of Ru addition on stress rupture properties decreases with increasing test temperature. The γ′ coarsening and rafting directionally are observed in Ru-free alloy and Ru-containing alloy after stress rupture test. Needle shaped TCP phases precipitated in both of alloys after stress rupture test at (1100 ℃, 140 MPa) and (1120 ℃, 140 MPa) and no TCP phase was observed in both of alloys after stress rupture test (980 ℃, 250 MPa). The precipitate volume fraction of TCP phases is significantly decreased by the addition of Ru. At last, the relationship between the microstructure change with Ru addition and improvement of stress rupture properties was discussed.展开更多
The phase precipitation behavior and tensile properties of an as-cast Ni-based alloy,IN617B alloy,after solution heat treatment and long-term aging treatment were investigated.Ti(C,N),M6C and M23C6 are the primary pre...The phase precipitation behavior and tensile properties of an as-cast Ni-based alloy,IN617B alloy,after solution heat treatment and long-term aging treatment were investigated.Ti(C,N),M6C and M23C6 are the primary precipitates in as-cast microstructure.After solution heat treatment,most of carbides dissolve into the matrix except a few fine Ti(C,N)within grains.During long-term aging at 700°C,the phase precipitation behaviors of the alloy are characterized as follows:(1)M23C6 carbides at grain boundaries(GBs)transform from film-like shape to cellular shape and gradually coarsen due to the decrease of the surface energy and element aggregation to GBs;(2)M23C6 carbides within grains have a bar-like morphology with a preferential growth direction[110]and have a cube-on-cube coherent orientation relationship with the matrixγ;(3)γ?particles inhibit the coarsening of M23C6 within grains by constraining the diffusion of formation elements.Furthermore,the tensile strength of the alloy obviously increases,but the ductility significantly decreases after the aging for 5000 h.The alloy has a relatively stable microstructure which guarantees the excellent tensile properties during long-term aging.展开更多
The structural evolution of dislocation network is closely related to y' rafting and tensile properties. In this work, the effects of strain rate and temperature on the structural evolution of interface dislocatio...The structural evolution of dislocation network is closely related to y' rafting and tensile properties. In this work, the effects of strain rate and temperature on the structural evolution of interface dislocation network in Ni-based superalloys are studied by molecular dynamics simulations. The correlation between the evolution of dislocation network and tensile properties is also explored. The results indicate that the dislocation network shows different degrees of deformation and damage at various strain rates and temperatures. The ),' rafting depends on the damage structure of dislocation network at various strain rates and tem- peratures. Moreover, the tensile properties of interface in Ni-based superalloys are closely related to the evolution of disloca- tion network and dislocation motion mechanisms.展开更多
文摘Two experimental single crystal superalloys, Ru-free alloy and Ru-containing alloy with [001] orientation, other alloying element contents being basically kept same, were cast in the directionally solidified furnace. The effect of Ru on the stress rupture properties of the single crystal superalloy was investigated at (980 ℃, 250 MPa), (1100 ℃, 140 MPa) and (1120 ℃, 140 MPa). The results show that Ru can enhance high temperature stress rupture properties of single crystal superalloy. The improvement effect of Ru addition on stress rupture properties decreases with increasing test temperature. The γ′ coarsening and rafting directionally are observed in Ru-free alloy and Ru-containing alloy after stress rupture test. Needle shaped TCP phases precipitated in both of alloys after stress rupture test at (1100 ℃, 140 MPa) and (1120 ℃, 140 MPa) and no TCP phase was observed in both of alloys after stress rupture test (980 ℃, 250 MPa). The precipitate volume fraction of TCP phases is significantly decreased by the addition of Ru. At last, the relationship between the microstructure change with Ru addition and improvement of stress rupture properties was discussed.
基金Project(51571191)supported by the National Natural Science Foundation of ChinaProject(NY 20150102)supported by the National Energy Administration Program of China
文摘The phase precipitation behavior and tensile properties of an as-cast Ni-based alloy,IN617B alloy,after solution heat treatment and long-term aging treatment were investigated.Ti(C,N),M6C and M23C6 are the primary precipitates in as-cast microstructure.After solution heat treatment,most of carbides dissolve into the matrix except a few fine Ti(C,N)within grains.During long-term aging at 700°C,the phase precipitation behaviors of the alloy are characterized as follows:(1)M23C6 carbides at grain boundaries(GBs)transform from film-like shape to cellular shape and gradually coarsen due to the decrease of the surface energy and element aggregation to GBs;(2)M23C6 carbides within grains have a bar-like morphology with a preferential growth direction[110]and have a cube-on-cube coherent orientation relationship with the matrixγ;(3)γ?particles inhibit the coarsening of M23C6 within grains by constraining the diffusion of formation elements.Furthermore,the tensile strength of the alloy obviously increases,but the ductility significantly decreases after the aging for 5000 h.The alloy has a relatively stable microstructure which guarantees the excellent tensile properties during long-term aging.
基金supported by the National Natural Science Foundation of China (Grant Nos. 11072026 and 11102139)the Fundamental Research Funds for the Central Universities (Grant No. 2009JBZ015)China Postdoctoral Science Foundation (Grant No. 20110491205)
文摘The structural evolution of dislocation network is closely related to y' rafting and tensile properties. In this work, the effects of strain rate and temperature on the structural evolution of interface dislocation network in Ni-based superalloys are studied by molecular dynamics simulations. The correlation between the evolution of dislocation network and tensile properties is also explored. The results indicate that the dislocation network shows different degrees of deformation and damage at various strain rates and temperatures. The ),' rafting depends on the damage structure of dislocation network at various strain rates and tem- peratures. Moreover, the tensile properties of interface in Ni-based superalloys are closely related to the evolution of disloca- tion network and dislocation motion mechanisms.