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Cr与B对镍基高温钎料在C_f/SiC陶瓷基复合材料上润湿性的影响 被引量:6
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作者 张勇 张国庆 +1 位作者 何志勇 冯涤 《焊接学报》 EI CAS CSCD 北大核心 2007年第12期93-96,共4页
研究了Cr和B元素对镍基高温钎料在3D-Cf/SiC陶瓷基复合材料上的润湿性的影响。试验结果发现,在真空度小于10-3Pa,工作温度1 100℃,保温时间10 min条件下,当钎料中的Cr元素含量为15%,B元素含量为0.6%时,镍基钎料在Cf/SiC上的润湿角为10&#... 研究了Cr和B元素对镍基高温钎料在3D-Cf/SiC陶瓷基复合材料上的润湿性的影响。试验结果发现,在真空度小于10-3Pa,工作温度1 100℃,保温时间10 min条件下,当钎料中的Cr元素含量为15%,B元素含量为0.6%时,镍基钎料在Cf/SiC上的润湿角为10°,然而B元素含量增加到2.4%后,润湿角增大到62°,表明钎料中的元素B降低钎料在Cf/SiC上的润湿性。钎料中的活性元素Cr对润湿有重要影响。镍基钎料在Cf/SiC上的润湿过程属于反应润湿,润湿界面生成多种碳化物和硅化物。采用扫描电镜与能谱仪分析界面的微观结构与成分,通过X射线衍射仪检测界面产物。 展开更多
关键词 镍基高温钎料 润湿性 Cr/SiC
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含铝、钛元素的镍基高温钎料的表面反应 被引量:2
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作者 梁海 侯万良 《焊接》 北大核心 2015年第9期59-61,76,共3页
研究了硼、碳合金元素和钎焊温度对含铝、钛的镍基高温钎料的表面氧化反应的影响。试验发现,在只含以硅作降熔点元素的镍基活性钎料中,在2×10^(-2)Pa的真空环境下加热,表面氧化反应十分严重,钎料颗粒氧化发黑,不铺展、不润湿;在加... 研究了硼、碳合金元素和钎焊温度对含铝、钛的镍基高温钎料的表面氧化反应的影响。试验发现,在只含以硅作降熔点元素的镍基活性钎料中,在2×10^(-2)Pa的真空环境下加热,表面氧化反应十分严重,钎料颗粒氧化发黑,不铺展、不润湿;在加入0.15%碳元素后,表面氧化反应略有减弱;而在同时加入0.3%左右的硼元素后,钎料颗粒氧化发黑现象消失,表面脱氧化反应强烈,钎料的铺展和润湿性良好;而提高钎焊温度则对活性钎料的表面脱氧反应有利。 展开更多
关键词 镍基高温钎料 活性元素 表面反应
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Interfacial microstructure and mechanical properties of GH99 superalloy and Nb brazed joint using Cu75Pt25 filler 被引量:2
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作者 Wen-qiang LI Sheng-peng HU +3 位作者 Yu-zhen LEI Yu LEI Xiao-guo SONG Ji-cai FENG 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2020年第10期2724-2736,共13页
Cu75Pt25 brazing filler was applied to brazing GH99 superalloy to Nb,and the sound joints were obtained by adjusting brazing parameters.The typical interfacial microstructure of the brazed joint was Nb/Nb7Ni6+NbNi3/Ni... Cu75Pt25 brazing filler was applied to brazing GH99 superalloy to Nb,and the sound joints were obtained by adjusting brazing parameters.The typical interfacial microstructure of the brazed joint was Nb/Nb7Ni6+NbNi3/Ni(s,s)+Cr-rich NbNi3+(NbCr2+NbNi3)/GH99.The effects of brazing temperature and holding time on the interfacial microstructure of GH99/Cu75Pt25/Nb joints were studied.The results showed that the solution and diffusion of Ni atoms from GH99 substrate into brazing seam played a critical role in the interfacial microstructure evolution.As the brazing temperature rose,the Nb−Ni reaction layer was formed instead of the initial Nb3Pt layer,and the thickness increased firstly and then remained constant.The highest shear strength of the joint reached 152 MPa when brazed at 1150℃ for 15 min.All of the joints presented a brittle fracture mode during shear test,and the fracture location changed from Nb3Pt layer to Nb−Ni compounds layer. 展开更多
关键词 nickel-based superalloy NB Cu75Pt25 filler BRAZING microstructure mechanical properties
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Microstructure and shear strength ofγ-TiAl/GH536 joints brazed with Ti-Zr-Cu-Ni-Fe-Co-Mo filler alloy 被引量:10
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作者 Li LI Wei ZHAO +2 位作者 Zhi-xue FENG Jia SUN Xiao-qiang LI 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2020年第8期2143-2155,共13页
The influence of brazing temperature and brazing time on the microstructure and shear strength ofγ-TiAl/GH536 joints brazed with Ti-Zr-Cu-Ni-Fe-Co-Mo filler was investigated using SEM,EDS,XRD and universal testing ma... The influence of brazing temperature and brazing time on the microstructure and shear strength ofγ-TiAl/GH536 joints brazed with Ti-Zr-Cu-Ni-Fe-Co-Mo filler was investigated using SEM,EDS,XRD and universal testing machine.Results show that all the brazed joints mainly consist of four reaction layers regardless of the brazing temperature and brazing time.The thickness of the brazed seam and the average shear strength of the joint increase firstly and then decrease with brazing temperature in the range of 1090-1170℃and brazing time varying from 0 to 20 min.The maximum shear strength of 262 MPa is obtained at 1150℃for 10 min.The brittle Al3NiTi2 and TiNi3 intermetallics are the main controlling factors for the crack generation and deterioration of joint strength.The fracture surface is characterized as typical cleavage fracture and it mainly consists of massive brittle Al3NiTi2 intermetallics. 展开更多
关键词 γ-TiAl alloy Ni-based superalloy vacuum brazing amorphous filler MICROSTRUCTURE shear strength
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