Objective: A new indirect composite restorative system with water combingpressure, light, and heat was introduced for the fabrication of inlays and onlays. Methods: Fifteendefected teeth were selected for composite re...Objective: A new indirect composite restorative system with water combingpressure, light, and heat was introduced for the fabrication of inlays and onlays. Methods: Fifteendefected teeth were selected for composite resin inlay and onlay fabrication with Tescera ATL unitequipment. The clinical trial was carried out for 3 months. Results: After 3 months test, 7parameters were checked, 15 Tescera inlays and onlays were demonstrated that exceptional esthetics,all 7 parameters were good and the patients were very satisfied. Conclusion: inlays , which weremade with Tescera ATL restorative system, are esthetics; physical properties of materials areimproved highly, and have a long-lasting durability. This restorative system is worthy to be usedand further studied in dental practice.展开更多
The East China Sea(ECS) is a river-dominated epicontinental sea, linking the Asian continent to the northwestern Pacific via the large rivers originating from Tibetan Plateau. The relevant huge influx of riverine detr...The East China Sea(ECS) is a river-dominated epicontinental sea, linking the Asian continent to the northwestern Pacific via the large rivers originating from Tibetan Plateau. The relevant huge influx of riverine detritus has developed unique sedimentary systems in the ECS during the Quaternary, offering ideal terrestrial archives for reconstructing Quaternary paleoenvironmental changes and studying land-sea interactions. Overall, two characteristic river systems dominate the sedimentary systems and sediment source to sink transport patterns in the ECS, represented by the Changjiang(Yangtze River) and Huanghe(Yellow River) for the large river system and Taiwan rivers for the small river system. Given this, the sediments derived from both river systems bear distinct features in terms of parent rock lithology, provenance weathering and sediment transport. Previous studies mostly focus on either the ‘source' discrimination or the ‘sink' records of the sedimentary system in the ECS, while the source to sink process linking the land and sea, in particular its time scale, has been poorly understood. Here we introduce a newly-developed dating technique, the ‘comminution age' method, which offers a quantitative constraint on the time scale of sediment transfer from its ultimate source to the final depositional sink. This novel method is of great significance for improving our understanding on the earth surface processes including tectonic-climate driven weathering, and sediment recycling in relation to landscape evolution and marine environmental changes. The application of comminution age method in the ECS will provide important constraints on sediment source-to-sink process and more evidences for the construction of late Quaternary paleoenvironmental changes under these unique sedimentary systems.展开更多
On August 25,2015 the CFHL technology for hydroupgrading of syncrude obtained from low-temperature Fischer-Tropsch synthesis had been successfully applied on the first in China 1.0 Mt/a indirect coal liquefaction unit.
The electrochemical behavior of N,N-diethyl-p-nitroso aniline was carried out using SWV （square wave voltammetric） at HMDE. A well defined reduction peak was observed at （-0.214） volt versus the reference electro...The electrochemical behavior of N,N-diethyl-p-nitroso aniline was carried out using SWV （square wave voltammetric） at HMDE. A well defined reduction peak was observed at （-0.214） volt versus the reference electrode （Ag/AgC1/sat. KCI）, calibration curve was constructed in phosphate buffer （pH = 7.0）, the relationship is linear within the concentration range 1.283 × 10.5 M - 3.66 × 10.5 M with the correlation （R = 0.9923）. The serial addition ofCPM （chlorpheniramine maleate） leads to the decrease in the reduction current peak （Ip）, quantitatively, the plot of Alp （Ip - Ip） where, Ip： Peak current of N, N-diethyl-p-nitroso aniline alone, lp： peak current of N,N-diethyl-p-nitroso aniline in the presence of CPM, versus concentration is linear within the concentration range 0.984 × 10-6 M - 9.756 × 10-6 M, the correlation coefficient was 0.9954. The method was successfully applied to determine CPM in different types of pharmaceutical formulations, and compared with standard method from British Pharmacopeia [1].展开更多
EDF R＆D is developing a new calculation scheme based on the transport-Simplified Pn （SPn） approach. The lattice code used is the deterministic code APOLLO2, developed at CEA. The core code is the code COCAGNE, deve...EDF R＆D is developing a new calculation scheme based on the transport-Simplified Pn （SPn） approach. The lattice code used is the deterministic code APOLLO2, developed at CEA. The core code is the code COCAGNE, developed at EDF R＆D. The latter can take advantage of a microscopic depletion solver expected to improve the treatment of spectral history effects. However, the direct use of the microscopic depletion solver is computationally very intensive because very small evolution steps （typically 100 MWd/t） are needed to reach a good accuracy, which is not always compatible with industrial applications. In order to reduce the calculation time associated with the use of the microscopic depletion solver, a predictor-corrector scheme has been implemented within COCAGNE. It enables the use of larger evolution steps, up to 1000 MWd/t. Tests show that the predictor-corrector procedure gives fairly accurate results while significantly reducing the calculation time.展开更多
The role of carbodiimide as dehydrant in the chemo‐,regio‐and stereoselective Pd(Ⅱ/0)‐catalyzed hydrocarboxylation of various alkynes with HCOOH releasing CO in situ is reported for the first time to obtainα,β‐...The role of carbodiimide as dehydrant in the chemo‐,regio‐and stereoselective Pd(Ⅱ/0)‐catalyzed hydrocarboxylation of various alkynes with HCOOH releasing CO in situ is reported for the first time to obtainα,β‐unsaturated carboxylic acids.Both symmetrical and unsymmetrical monoalkynes show good reactivity.Importantly,2,2’‐(1,4‐phenylene)diacrylic acid can also be synthesized in high yield through the dihydrocarboxylation of 1,4‐diethynylbenzene.Besides,an excellent result in gram scale experiment and TON up to 900 can be obtained,displaying the efficiency of this protocol.Notably,regulating the types and concentrations of dehydrant can control the CO generation,avoiding directly operating toxic CO and circumventing sensitivity issue to the CO amount.On the basis of the attractive features of formic acid including easy preparation through CO_(2) hydrogenation and efficient liberation of CO,this protocol using formic acid as bridging reagent between CO_(2) and CO can be perceived as an indirect utilization of CO_(2),offering an alternative method for preparing acrylic acid analogues.展开更多
The single event effect(SEE) is an important consideration in electronic devices used in space environments because it can lead to spacecraft anomalies and failures. The linear energy transfer(LET) of ions is commonly...The single event effect(SEE) is an important consideration in electronic devices used in space environments because it can lead to spacecraft anomalies and failures. The linear energy transfer(LET) of ions is commonly investigated in studies of SEE. The use of a thin detector is an economical way of directly measuring the LET in space. An LET telescope consists of a thin detector as the front detector(D1), along with a back detector that indicates whether D1 was penetrated. The particle radiation effect monitor(PREM) introduced in this paper is designed to categorize the LET into four bins of 0.2–0.4, 0.4–1.0, 1.0–2.0 and 2.0–20 Me V·cm^2/mg, and one integral bin of LET>20 Me V·cm^2/mg. After calibration with heavy ions and Geant4 analysis, the LET boundaries of the first four bins are determined to be 0.236, 0.479, 1.196, 2.254, and 17.551 Me V·cm^2/mg, whereas that of the integral bin is determined to be LET>14.790 Me V·cm^2/mg. The acceptances are calculated by Geant4 analysis as 0.452, 0.451, 0.476, 0.446, and 1.334, respectively. The LET accuracy is shown to depend on the thickness of D1; as D1 is made thinner, the accuracy of the measured values increases.展开更多
文摘Objective: A new indirect composite restorative system with water combingpressure, light, and heat was introduced for the fabrication of inlays and onlays. Methods: Fifteendefected teeth were selected for composite resin inlay and onlay fabrication with Tescera ATL unitequipment. The clinical trial was carried out for 3 months. Results: After 3 months test, 7parameters were checked, 15 Tescera inlays and onlays were demonstrated that exceptional esthetics,all 7 parameters were good and the patients were very satisfied. Conclusion: inlays , which weremade with Tescera ATL restorative system, are esthetics; physical properties of materials areimproved highly, and have a long-lasting durability. This restorative system is worthy to be usedand further studied in dental practice.
基金supported by the Key Laboratory of Marine Hydrocarbon Resources and Environmental Geology (MRE201402)the National Natural Science Foundation of China (41306040, 41225020)the Foundation of Key Laboratory of Yangtze River Water Environment (YRWEF 201305)
文摘The East China Sea(ECS) is a river-dominated epicontinental sea, linking the Asian continent to the northwestern Pacific via the large rivers originating from Tibetan Plateau. The relevant huge influx of riverine detritus has developed unique sedimentary systems in the ECS during the Quaternary, offering ideal terrestrial archives for reconstructing Quaternary paleoenvironmental changes and studying land-sea interactions. Overall, two characteristic river systems dominate the sedimentary systems and sediment source to sink transport patterns in the ECS, represented by the Changjiang(Yangtze River) and Huanghe(Yellow River) for the large river system and Taiwan rivers for the small river system. Given this, the sediments derived from both river systems bear distinct features in terms of parent rock lithology, provenance weathering and sediment transport. Previous studies mostly focus on either the ‘source' discrimination or the ‘sink' records of the sedimentary system in the ECS, while the source to sink process linking the land and sea, in particular its time scale, has been poorly understood. Here we introduce a newly-developed dating technique, the ‘comminution age' method, which offers a quantitative constraint on the time scale of sediment transfer from its ultimate source to the final depositional sink. This novel method is of great significance for improving our understanding on the earth surface processes including tectonic-climate driven weathering, and sediment recycling in relation to landscape evolution and marine environmental changes. The application of comminution age method in the ECS will provide important constraints on sediment source-to-sink process and more evidences for the construction of late Quaternary paleoenvironmental changes under these unique sedimentary systems.
文摘On August 25,2015 the CFHL technology for hydroupgrading of syncrude obtained from low-temperature Fischer-Tropsch synthesis had been successfully applied on the first in China 1.0 Mt/a indirect coal liquefaction unit.
文摘The electrochemical behavior of N,N-diethyl-p-nitroso aniline was carried out using SWV （square wave voltammetric） at HMDE. A well defined reduction peak was observed at （-0.214） volt versus the reference electrode （Ag/AgC1/sat. KCI）, calibration curve was constructed in phosphate buffer （pH = 7.0）, the relationship is linear within the concentration range 1.283 × 10.5 M - 3.66 × 10.5 M with the correlation （R = 0.9923）. The serial addition ofCPM （chlorpheniramine maleate） leads to the decrease in the reduction current peak （Ip）, quantitatively, the plot of Alp （Ip - Ip） where, Ip： Peak current of N, N-diethyl-p-nitroso aniline alone, lp： peak current of N,N-diethyl-p-nitroso aniline in the presence of CPM, versus concentration is linear within the concentration range 0.984 × 10-6 M - 9.756 × 10-6 M, the correlation coefficient was 0.9954. The method was successfully applied to determine CPM in different types of pharmaceutical formulations, and compared with standard method from British Pharmacopeia [1].
文摘EDF R＆D is developing a new calculation scheme based on the transport-Simplified Pn （SPn） approach. The lattice code used is the deterministic code APOLLO2, developed at CEA. The core code is the code COCAGNE, developed at EDF R＆D. The latter can take advantage of a microscopic depletion solver expected to improve the treatment of spectral history effects. However, the direct use of the microscopic depletion solver is computationally very intensive because very small evolution steps （typically 100 MWd/t） are needed to reach a good accuracy, which is not always compatible with industrial applications. In order to reduce the calculation time associated with the use of the microscopic depletion solver, a predictor-corrector scheme has been implemented within COCAGNE. It enables the use of larger evolution steps, up to 1000 MWd/t. Tests show that the predictor-corrector procedure gives fairly accurate results while significantly reducing the calculation time.
文摘The role of carbodiimide as dehydrant in the chemo‐,regio‐and stereoselective Pd(Ⅱ/0)‐catalyzed hydrocarboxylation of various alkynes with HCOOH releasing CO in situ is reported for the first time to obtainα,β‐unsaturated carboxylic acids.Both symmetrical and unsymmetrical monoalkynes show good reactivity.Importantly,2,2’‐(1,4‐phenylene)diacrylic acid can also be synthesized in high yield through the dihydrocarboxylation of 1,4‐diethynylbenzene.Besides,an excellent result in gram scale experiment and TON up to 900 can be obtained,displaying the efficiency of this protocol.Notably,regulating the types and concentrations of dehydrant can control the CO generation,avoiding directly operating toxic CO and circumventing sensitivity issue to the CO amount.On the basis of the attractive features of formic acid including easy preparation through CO_(2) hydrogenation and efficient liberation of CO,this protocol using formic acid as bridging reagent between CO_(2) and CO can be perceived as an indirect utilization of CO_(2),offering an alternative method for preparing acrylic acid analogues.
基金supported by the National Natural Science Foundation of China(Grant No.41374181)the National Key Scientific Instrument and Equipment Development ProjectsChina(Grant No.2012YQ03014207)
文摘The single event effect(SEE) is an important consideration in electronic devices used in space environments because it can lead to spacecraft anomalies and failures. The linear energy transfer(LET) of ions is commonly investigated in studies of SEE. The use of a thin detector is an economical way of directly measuring the LET in space. An LET telescope consists of a thin detector as the front detector(D1), along with a back detector that indicates whether D1 was penetrated. The particle radiation effect monitor(PREM) introduced in this paper is designed to categorize the LET into four bins of 0.2–0.4, 0.4–1.0, 1.0–2.0 and 2.0–20 Me V·cm^2/mg, and one integral bin of LET>20 Me V·cm^2/mg. After calibration with heavy ions and Geant4 analysis, the LET boundaries of the first four bins are determined to be 0.236, 0.479, 1.196, 2.254, and 17.551 Me V·cm^2/mg, whereas that of the integral bin is determined to be LET>14.790 Me V·cm^2/mg. The acceptances are calculated by Geant4 analysis as 0.452, 0.451, 0.476, 0.446, and 1.334, respectively. The LET accuracy is shown to depend on the thickness of D1; as D1 is made thinner, the accuracy of the measured values increases.
