Partial transient liquid phase （PTLP） bonding of TiC cermet to 06Cr19Ni10 stainless steel was carried out. Impulse pressuring was used to reduce the bonding time, and a Ti/Cu/Nb interlayer was employed to alleviate ...Partial transient liquid phase （PTLP） bonding of TiC cermet to 06Cr19Ni10 stainless steel was carried out. Impulse pressuring was used to reduce the bonding time, and a Ti/Cu/Nb interlayer was employed to alleviate the detrimental effect of interfacial reaction products on the bonding strength. Successful bonding was achieved at 885℃ under a pulsed pressure of 2-10 MPa within durations in the range of 2-8 min, which was notably shortened in comparison with conventional PTLP bonding. Microstructure characterization revealed the o- phase with a limit solubility of Nb, a sequence of Ti-Cu intermetallic phases and solid solutions of Ni and Cu in α＋β Ti in the reaction zone. The maximum shear strength of 106.7 MPa was obtained when the joint was bonded for 5 rain, indicating that a robust metallurgical bonding was achieved. Upon shear loading, the joints fractured along the Ti-Cu intermetallics interface and spread to the interior of TiC cermet in a brittle cleavage manner.展开更多
The functional piezoelectric ceramic smart aggregate(SA) sensors and actuators,based on piezoelectric ceramic materials such as lead zirconium titanate(PZT),were embedded into the reinforced concrete beams with three-...The functional piezoelectric ceramic smart aggregate(SA) sensors and actuators,based on piezoelectric ceramic materials such as lead zirconium titanate(PZT),were embedded into the reinforced concrete beams with three-point bending under static loading for purposes of damage detection.The SA actuators generated the desired sine sweep excitation signals online and the SA sensors received and detected real-time signals before and after damage.The wavelet analysis and statistical characteristics about damage signals were used as a signal processing and analysis tool to extract the optimal damage information and establish a statistical damage detection algorithm.The damage index-based wavelet analysis and damage probability-based probability and statistics were proposed by PZT wavebased theory and active health monitoring technology.The results showed that the existence of cracks inside largely attenuated the amplitude of active monitoring signal after the damage of beam and the attenuation was related to the severity degree of damage.The innovative statistical algorithm of damage pattern detection based PZT-SA can effectively determine damage probability and damage degree,and provide a prediction for the critical damage location of reinforced concrete structures.The developed method can be utilized for the structural health comprehensive monitoring and damage detection on line of various large-scale concrete structures.展开更多
16Mn steel, 1Cr18Ni9 stainless steel, thermal sprayed Al2O3-TiO2 ceramic coating and nylon1010-5 %Al2O3 coating were tested with an erosion -corrosion tester.The effects of pH values and slurry velocities on the erosi...16Mn steel, 1Cr18Ni9 stainless steel, thermal sprayed Al2O3-TiO2 ceramic coating and nylon1010-5 %Al2O3 coating were tested with an erosion -corrosion tester.The effects of pH values and slurry velocities on the erosion-corrosion behavior of the materials tested were determined. The erosion-corrosion behavior of the materials tested changes with pH values and presents different change tendencies. The erosion-corrosion rates of the materials are increased with slurry velocities. The erosion-corrosion mechanisms for the steels and the coatings are considerably different.展开更多
A new style Ni-containing alumina ceramic foam based continuous three-dimensional interconnected skeleton was prepared by impregnating a polymeric sponge with aqueous ceramic slurry.Subsequently,alumina ceramic foam/s...A new style Ni-containing alumina ceramic foam based continuous three-dimensional interconnected skeleton was prepared by impregnating a polymeric sponge with aqueous ceramic slurry.Subsequently,alumina ceramic foam/steel metal matrix composites(MMCs) were prepared successfully by sand mold casting technique.The microstructure and mechanical properties of MMCs were investigated by SEM,EDS and compressive test.The results show that the depth of infiltration is about 40 μm to the bonding interface of ceramic/steel and the fracture strength σmax and plastic strain limit εp of composite are 520 MPa and 11.2%,respectively.The fretting wear mechanism of MMCs is mainly performed at the oxidative wear mode with lower load/friction frequency and the predominant oxidation wear together with slight adhesive wear and abrasive wear multiple mode with higher load/ friction frequency.Moreover,the infiltration bonding and continuous three-dimensional interconnected ceramic skeleton play a vital role in the stability of the bonding interface and excellent mechanical properties.展开更多
Abstract： An alloy steel/alumina composite was successfully fabricated by pressureless infiltration of X10CrNil8-8 steel melt on 30% （mass fraction） Ni-containing alumina based composite ceramic （Ni/Al2O3） at 1 6...Abstract： An alloy steel/alumina composite was successfully fabricated by pressureless infiltration of X10CrNil8-8 steel melt on 30% （mass fraction） Ni-containing alumina based composite ceramic （Ni/Al2O3） at 1 600 ℃. The infiltration quality and interfacial bonding behavior were investigated by SEM, EDS, XRD and tensile tests. The results show that there is an obvious interfacial reaction layer between the alloying steel and the Ni/Al2O3 composite ceramic. The interfacial reactive products are （FexAly）3O4 intermetallic phase and （AlxCry）2O3 solid solution. The interracial bonding strength is as high as about 67.5 MPa. The bonding mechanism of X10CrNi 18-8 steel with the composite ceramic is that Ni inside the ceramic bodies dissolves into the alloy melt and transforms into liquid channels, consequently inducing the steel melt infiltrating and filling in the pores and the liquid channels. Moreover, the metallurgical bonding and interfacial reactive bonding also play a key role on the stability of the bonding interface.展开更多
In this paper,the BaO-0.6ZnO-xTiO2 ceramics with x=2.5-2.8 have been prepared by the conventional solid-state ceramic route for the purpose of investigating the effect of TiO2 content on the microwave dielectric prope...In this paper,the BaO-0.6ZnO-xTiO2 ceramics with x=2.5-2.8 have been prepared by the conventional solid-state ceramic route for the purpose of investigating the effect of TiO2 content on the microwave dielectric properties.The XRD results showed that the main crystal phase in the sintered ceramics was Ba4ZnTi11O27 and that the additional phases:Ba2ZnTi5O13 and BaZn2.03Ti3.93O10.89 were presented,depending on the TiO2 contents.The SEM photographs of the samples sintered at 1200℃ for 2 h showed a high compact microstructure.Because the phase composition of ceramics samples was changed with TiO2 content,the dielectric constant(εr),the quality factor values(Q×f) and the temperature coefficient of resonant frequency(τf) were first increased,continuously came up to a peak value,and then let up.It was lucky to find that the sample with composition BaO-0.6ZnO-2.7TiO2 had both the maximum dielectric constant εr=36.1 and the maximum Q×f value of 29320 GHz,and more importantly,it had an acceptable temperature coefficient of resonant frequency τf=10.45 ppm/℃.展开更多
基金Project(51421001)supported by the National Natural Science Foundation of ChinaProjects(106112015CDJXZ138803,106112015CDJXY130003)supported by the Fundamental Research Funds for the Central Universities,China
文摘Partial transient liquid phase （PTLP） bonding of TiC cermet to 06Cr19Ni10 stainless steel was carried out. Impulse pressuring was used to reduce the bonding time, and a Ti/Cu/Nb interlayer was employed to alleviate the detrimental effect of interfacial reaction products on the bonding strength. Successful bonding was achieved at 885℃ under a pulsed pressure of 2-10 MPa within durations in the range of 2-8 min, which was notably shortened in comparison with conventional PTLP bonding. Microstructure characterization revealed the o- phase with a limit solubility of Nb, a sequence of Ti-Cu intermetallic phases and solid solutions of Ni and Cu in α＋β Ti in the reaction zone. The maximum shear strength of 106.7 MPa was obtained when the joint was bonded for 5 rain, indicating that a robust metallurgical bonding was achieved. Upon shear loading, the joints fractured along the Ti-Cu intermetallics interface and spread to the interior of TiC cermet in a brittle cleavage manner.
基金Supported by Science and Technology Project of Ministry of Housing and Urban-Rural Development(No.2011k211)"11th Five-Year" Science and Technology Research Project of Education Department,Jilin Province(No.200925)Liaoning Structure Engineering Key Laboratory 2009 Open Fund(JG2009 2007-08)
文摘The functional piezoelectric ceramic smart aggregate(SA) sensors and actuators,based on piezoelectric ceramic materials such as lead zirconium titanate(PZT),were embedded into the reinforced concrete beams with three-point bending under static loading for purposes of damage detection.The SA actuators generated the desired sine sweep excitation signals online and the SA sensors received and detected real-time signals before and after damage.The wavelet analysis and statistical characteristics about damage signals were used as a signal processing and analysis tool to extract the optimal damage information and establish a statistical damage detection algorithm.The damage index-based wavelet analysis and damage probability-based probability and statistics were proposed by PZT wavebased theory and active health monitoring technology.The results showed that the existence of cracks inside largely attenuated the amplitude of active monitoring signal after the damage of beam and the attenuation was related to the severity degree of damage.The innovative statistical algorithm of damage pattern detection based PZT-SA can effectively determine damage probability and damage degree,and provide a prediction for the critical damage location of reinforced concrete structures.The developed method can be utilized for the structural health comprehensive monitoring and damage detection on line of various large-scale concrete structures.
文摘16Mn steel, 1Cr18Ni9 stainless steel, thermal sprayed Al2O3-TiO2 ceramic coating and nylon1010-5 %Al2O3 coating were tested with an erosion -corrosion tester.The effects of pH values and slurry velocities on the erosion-corrosion behavior of the materials tested were determined. The erosion-corrosion behavior of the materials tested changes with pH values and presents different change tendencies. The erosion-corrosion rates of the materials are increased with slurry velocities. The erosion-corrosion mechanisms for the steels and the coatings are considerably different.
基金Project(51271080) supported by the National Natural Science Foundation of ChinaProject(2012JSSPITP1968) supported by the Innovative Foundation for Students of Jiangsu Province,ChinaProject(CKJB201204) supported by the Innovation Fund of Nanjing Institute of Technology,China
文摘A new style Ni-containing alumina ceramic foam based continuous three-dimensional interconnected skeleton was prepared by impregnating a polymeric sponge with aqueous ceramic slurry.Subsequently,alumina ceramic foam/steel metal matrix composites(MMCs) were prepared successfully by sand mold casting technique.The microstructure and mechanical properties of MMCs were investigated by SEM,EDS and compressive test.The results show that the depth of infiltration is about 40 μm to the bonding interface of ceramic/steel and the fracture strength σmax and plastic strain limit εp of composite are 520 MPa and 11.2%,respectively.The fretting wear mechanism of MMCs is mainly performed at the oxidative wear mode with lower load/friction frequency and the predominant oxidation wear together with slight adhesive wear and abrasive wear multiple mode with higher load/ friction frequency.Moreover,the infiltration bonding and continuous three-dimensional interconnected ceramic skeleton play a vital role in the stability of the bonding interface and excellent mechanical properties.
基金Project(2009ZM0296) supported by the Fundamental Research Funds for the Central Universities in China
文摘Abstract： An alloy steel/alumina composite was successfully fabricated by pressureless infiltration of X10CrNil8-8 steel melt on 30% （mass fraction） Ni-containing alumina based composite ceramic （Ni/Al2O3） at 1 600 ℃. The infiltration quality and interfacial bonding behavior were investigated by SEM, EDS, XRD and tensile tests. The results show that there is an obvious interfacial reaction layer between the alloying steel and the Ni/Al2O3 composite ceramic. The interfacial reactive products are （FexAly）3O4 intermetallic phase and （AlxCry）2O3 solid solution. The interracial bonding strength is as high as about 67.5 MPa. The bonding mechanism of X10CrNi 18-8 steel with the composite ceramic is that Ni inside the ceramic bodies dissolves into the alloy melt and transforms into liquid channels, consequently inducing the steel melt infiltrating and filling in the pores and the liquid channels. Moreover, the metallurgical bonding and interfacial reactive bonding also play a key role on the stability of the bonding interface.
文摘In this paper,the BaO-0.6ZnO-xTiO2 ceramics with x=2.5-2.8 have been prepared by the conventional solid-state ceramic route for the purpose of investigating the effect of TiO2 content on the microwave dielectric properties.The XRD results showed that the main crystal phase in the sintered ceramics was Ba4ZnTi11O27 and that the additional phases:Ba2ZnTi5O13 and BaZn2.03Ti3.93O10.89 were presented,depending on the TiO2 contents.The SEM photographs of the samples sintered at 1200℃ for 2 h showed a high compact microstructure.Because the phase composition of ceramics samples was changed with TiO2 content,the dielectric constant(εr),the quality factor values(Q×f) and the temperature coefficient of resonant frequency(τf) were first increased,continuously came up to a peak value,and then let up.It was lucky to find that the sample with composition BaO-0.6ZnO-2.7TiO2 had both the maximum dielectric constant εr=36.1 and the maximum Q×f value of 29320 GHz,and more importantly,it had an acceptable temperature coefficient of resonant frequency τf=10.45 ppm/℃.
