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热处理温度对Al_2O_3-TiO_2-MgO等离子喷涂层微观结构和硬度的影响 被引量:3
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作者 陈昆伦 黄勇 +4 位作者 季强 黄太红 李超 宋鹏 陆建生 《材料保护》 CAS CSCD 北大核心 2018年第12期43-45,共3页
为了克服Q235碳钢表面等离子喷涂陶瓷层存在的一些缺陷,先在其表面电弧喷涂Ni-5Al粘结层,再大气等离子喷涂Al_2O_3-TiO_2-MgO陶瓷层。利用扫描电镜(SEM)、能谱仪(EDS)和X射线衍射仪(XRD)研究了氩气气氛中800,900,1 000℃热处理温度对陶... 为了克服Q235碳钢表面等离子喷涂陶瓷层存在的一些缺陷,先在其表面电弧喷涂Ni-5Al粘结层,再大气等离子喷涂Al_2O_3-TiO_2-MgO陶瓷层。利用扫描电镜(SEM)、能谱仪(EDS)和X射线衍射仪(XRD)研究了氩气气氛中800,900,1 000℃热处理温度对陶瓷涂层断面微观形貌、物相组成的影响;利用HMV-2T型显微硬度计测试其显微硬度。结果表明:经过热处理,Al_2O_3-TiO_2-MgO陶瓷涂层中的氧化铝和氧化钛组织相互扩散,组织界面模糊,同时Ni-5Al粘结层与陶瓷涂层与基体也出现了互扩散的现象,形成了扩散层;热处理温度越高,互扩散现象越明显;热处理过程中,陶瓷涂层中扁平状结构演化为相互钉扎,促进了Al_2O_3陶瓷涂层硬度的提高。 展开更多
关键词 大气等离子喷涂 Al2O3-TiO2-MgO涂层 Ar气 热处理温度 陶瓷涂层微观结构 硬度
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Effects of current density on microstructure and properties of plasma electrolytic oxidation ceramic coatings formed on 6063 aluminum alloy 被引量:10
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作者 项南 宋仁国 +3 位作者 庄俊杰 宋若希 陆筱雅 苏旭平 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2016年第3期806-813,共8页
Plasma electrolytic oxidation (PEO) ceramic coatings were fabricated in a silicate-based electrolyte with the addition of potassium fluorozirconate (K2ZrF6) on 6063 aluminum alloy, and the effects of current density o... Plasma electrolytic oxidation (PEO) ceramic coatings were fabricated in a silicate-based electrolyte with the addition of potassium fluorozirconate (K2ZrF6) on 6063 aluminum alloy, and the effects of current density on microstructure and properties of the PEO coatings were studied. It was found that pore density of the coatings decreased with increasing the current density. The tribological and hardness tests suggested that the ceramic coating produced under the current density of 15 A/dm2showed the best mechanical property, which matched well with the phase analysis. Electrochemical impedance spectroscopy (EIS) and potentiodynamic polarization curves proved that the coating obtained under 15 A/dm2 displayed the best anti-corrosion property, which was directly connected with morphologies of coatings. 展开更多
关键词 6063 aluminum alloy ceramic coating plasma electrolytic oxidation(PEO) current density MICROSTRUCTURE mechanical property
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