采用了一种全新的方法对金属陶瓷发热体的电阻温度系数(Temperature Coefficient of Resistance,TCR)进行检测。该法利用外加电源对发热体进行动态升温,并连续监测发热体的温度和阻值变化,通过最小二乘法拟合电阻-温度数据,进行数学计...采用了一种全新的方法对金属陶瓷发热体的电阻温度系数(Temperature Coefficient of Resistance,TCR)进行检测。该法利用外加电源对发热体进行动态升温,并连续监测发热体的温度和阻值变化,通过最小二乘法拟合电阻-温度数据,进行数学计算得到TCR值。研究进一步分析了影响检测稳定性的因素,包括红外聚焦方法、测温点位置、连接点位置及输出电压的选择,并验证了新方法测得的数据准确性与重复性。结果表明,新方法与国标法测试结果基本一致,但具有检测时间短、检测限高、检测数据点多等优势,适用于快速批量测试金属陶瓷发热体的TCR值。展开更多
ZrO2-mullite nano-ceramics were fabricated by in-situ controlled crystallizing from SiO2-Al2O3-ZrO2 amorphous bulk. The thermal transformation sequences of the SiO2-Al2O3-ZrO2 amorphous bulk were investigated by X-ray...ZrO2-mullite nano-ceramics were fabricated by in-situ controlled crystallizing from SiO2-Al2O3-ZrO2 amorphous bulk. The thermal transformation sequences of the SiO2-Al2O3-ZrO2 amorphous bulk were investigated by X-ray diffraction, infrared spectrum, scanning electron microscope and differential scanning calorimetric. And the mechanical properties of the nano-ceramics were studied. The results show that the bulks are still in amorphous state at 900 ℃ and the t-ZrO2 forms at about 950 ℃ with a faint spinel-like phase which changes into mullite on further heating. ZrO2 and mullite become major phases at 1 100 ℃ and an amount of m-ZrO2 occur at the same time. The sample heated at 950 ℃ for 2 h and then at 1 100 ℃ for 1 h shows very dense and homogenous microstructure with ball-like grains in size of 20-50 nm. With the increase of crystallization temperature up to 1 350 ℃, the grains grow quickly and some grow into lath-shaped grains with major diameter of 5 μm. After two-step treatment the highest micro-hardness, flexural strength and fracture toughness of the samples are 13.72 GPa, 520 MPa and 5.13 MPa·m1/2, respectively.展开更多
A model of the thermal dissociation process has been developed for the numerical simulation of ceramic powder processing in a d. c. plasma reactor. The temperature histories of zircon grains were calculated based on t...A model of the thermal dissociation process has been developed for the numerical simulation of ceramic powder processing in a d. c. plasma reactor. The temperature histories of zircon grains were calculated based on this model. Comparisons were carried out to determine the effects of plasma gas (N_2 and Ar), free stream temperature (6000-15000K) and Reynolds number (0.0-1.0) as well as particle diameter (20-200μm) on the zircon dissociation process. The influences of proper Nusselt number correlation and variable transport properties were discussed in detail.展开更多
文摘采用了一种全新的方法对金属陶瓷发热体的电阻温度系数(Temperature Coefficient of Resistance,TCR)进行检测。该法利用外加电源对发热体进行动态升温,并连续监测发热体的温度和阻值变化,通过最小二乘法拟合电阻-温度数据,进行数学计算得到TCR值。研究进一步分析了影响检测稳定性的因素,包括红外聚焦方法、测温点位置、连接点位置及输出电压的选择,并验证了新方法测得的数据准确性与重复性。结果表明,新方法与国标法测试结果基本一致,但具有检测时间短、检测限高、检测数据点多等优势,适用于快速批量测试金属陶瓷发热体的TCR值。
基金Project(2003AA332040) supported by the National High Technology Research and Development Program of China
文摘ZrO2-mullite nano-ceramics were fabricated by in-situ controlled crystallizing from SiO2-Al2O3-ZrO2 amorphous bulk. The thermal transformation sequences of the SiO2-Al2O3-ZrO2 amorphous bulk were investigated by X-ray diffraction, infrared spectrum, scanning electron microscope and differential scanning calorimetric. And the mechanical properties of the nano-ceramics were studied. The results show that the bulks are still in amorphous state at 900 ℃ and the t-ZrO2 forms at about 950 ℃ with a faint spinel-like phase which changes into mullite on further heating. ZrO2 and mullite become major phases at 1 100 ℃ and an amount of m-ZrO2 occur at the same time. The sample heated at 950 ℃ for 2 h and then at 1 100 ℃ for 1 h shows very dense and homogenous microstructure with ball-like grains in size of 20-50 nm. With the increase of crystallization temperature up to 1 350 ℃, the grains grow quickly and some grow into lath-shaped grains with major diameter of 5 μm. After two-step treatment the highest micro-hardness, flexural strength and fracture toughness of the samples are 13.72 GPa, 520 MPa and 5.13 MPa·m1/2, respectively.
文摘A model of the thermal dissociation process has been developed for the numerical simulation of ceramic powder processing in a d. c. plasma reactor. The temperature histories of zircon grains were calculated based on this model. Comparisons were carried out to determine the effects of plasma gas (N_2 and Ar), free stream temperature (6000-15000K) and Reynolds number (0.0-1.0) as well as particle diameter (20-200μm) on the zircon dissociation process. The influences of proper Nusselt number correlation and variable transport properties were discussed in detail.
