The samples of brazed diamond grits with NiCr brazing alloy are prepared in vacuum and argon gas. The microstructures are analyzed with scanning electron microscope （SEM）, energy dispersive X-ray spectroscopy （EDS...The samples of brazed diamond grits with NiCr brazing alloy are prepared in vacuum and argon gas. The microstructures are analyzed with scanning electron microscope （SEM）, energy dispersive X-ray spectroscopy （EDS） and X-ray diffraction（XRD）. The effects of brazing atmospheres on the as-brazed NiCr brazing alloy composite structures and interracial microstructure are studied between diamond grits and brazing alloy. Results show that： （1） There are different composite structures of as-brazed NiCr brazing alloy under different oxygen partial pressures in vacuum and argon gas. B203 exists on the surface of the brazed samples under argon gas furnace brazing. It indicates that oxygen plays an important role in the resultants of as-brazed NiCr brazing alloy during the brazing process. （2） There are different interfacial microstructures in different brazing atmospheres, but the main reaction product is chromium carbides. The chromium carbides in argon gas furnace brazing grow in a disordered form, but those in vacuum furnace brazing grow radiated. And the scale of grains in argon gas is smaller than those in vacuum.展开更多
CdS/ZnS core-shell microparticles were prepared by a simple two-step method combining ultrasonic spray pyrolysis and chemical bath deposition.The core-shell structures showed enhanced photocatalytic properties compare...CdS/ZnS core-shell microparticles were prepared by a simple two-step method combining ultrasonic spray pyrolysis and chemical bath deposition.The core-shell structures showed enhanced photocatalytic properties compared with those of CdS or ZnS spherical particles.CdS/ZnS photocatalysts with different amount of ZnS loaded as shells were prepared by adjusting the concentrations of Zn and S precursors during synthesis.The optical properties and photocatalytic activity for hydrogen production were investigated and the amount of ZnS loaded as shell was optimized.Thermal annealing and hydrothermal sulfurization treatments were applied to the core-shell structure and both treatments enhanced the material＇s photocatalytic activity and stability by eliminating crystalline defects and surface states.The result showed that thermal annealing treatment improved the bulk crystallinity and hydrothermal sulfurization improved the surface properties.The sample subjected to both treatments showed the highest photocatalytic activity.These results indicate that CdS/ZnS core-shell microspheres are a simple structure that can be used as efficient photocatalysts.The hydrothermal sulfurization treatment may also be a useful surface treatment for metal sulfide photocatalysts.The simple two-step method provides a promising approach to the large-scale synthesis of core-shell microsphere catalysts.展开更多
To avoid the isolation between the external and the internal information of enterprise information systems, a four-layer integrated framework is proposed on the basis of integrating Web2. 0 and the service- oriented a...To avoid the isolation between the external and the internal information of enterprise information systems, a four-layer integrated framework is proposed on the basis of integrating Web2. 0 and the service- oriented architecture （SOA）, which contains the data layer, the service layer, the presentation layer and the collaboration layer. The presentation layer plays the key role, converging the external information from the collaboration layer to the inside of information system （IS）, and diffusing the internal information from the service layer to public users. This framework can also illustrate how users contribute to producing new services, and how web services are integrated to collaborate with public users.展开更多
Static corrections using the conventional method are basically conducted in two steps, the weathering correction followed by the correction from the top of the sub-weathering to the unified datum. However, the convent...Static corrections using the conventional method are basically conducted in two steps, the weathering correction followed by the correction from the top of the sub-weathering to the unified datum. However, the conventional method fails to well deal with statics problems in case the top of the sub-weathering is sharply undulated and the lateral velocity of the sub-weathering varies significantly. This brings us to the introduction of a smooth intermediate reference datum （IRD） located under the top of the sub-weathering, which helps to further increase the accuracy of statics based on the weathering corrections, and ensures the imaging quality. Good results based on the IRD technique have been achieved in the complex areas in western China. This paper discusses the IRD functions, its application requirements, and selection of related parameters. Some typical sections for comparison are also given in this paper.展开更多
基金Supported by the National Natural Science Foundation of China(50475040)the Aeronautical Science Foundation of China(2005ZH52060)the Natural Science Foundation of Jiangsu Province(BK2006723)~~
文摘The samples of brazed diamond grits with NiCr brazing alloy are prepared in vacuum and argon gas. The microstructures are analyzed with scanning electron microscope （SEM）, energy dispersive X-ray spectroscopy （EDS） and X-ray diffraction（XRD）. The effects of brazing atmospheres on the as-brazed NiCr brazing alloy composite structures and interracial microstructure are studied between diamond grits and brazing alloy. Results show that： （1） There are different composite structures of as-brazed NiCr brazing alloy under different oxygen partial pressures in vacuum and argon gas. B203 exists on the surface of the brazed samples under argon gas furnace brazing. It indicates that oxygen plays an important role in the resultants of as-brazed NiCr brazing alloy during the brazing process. （2） There are different interfacial microstructures in different brazing atmospheres, but the main reaction product is chromium carbides. The chromium carbides in argon gas furnace brazing grow in a disordered form, but those in vacuum furnace brazing grow radiated. And the scale of grains in argon gas is smaller than those in vacuum.
基金supported by the National Natural Science Foundation of China(51202186,51323011)the Fundamental Research Funds for the Central University(xjj2016039)~~
文摘CdS/ZnS core-shell microparticles were prepared by a simple two-step method combining ultrasonic spray pyrolysis and chemical bath deposition.The core-shell structures showed enhanced photocatalytic properties compared with those of CdS or ZnS spherical particles.CdS/ZnS photocatalysts with different amount of ZnS loaded as shells were prepared by adjusting the concentrations of Zn and S precursors during synthesis.The optical properties and photocatalytic activity for hydrogen production were investigated and the amount of ZnS loaded as shell was optimized.Thermal annealing and hydrothermal sulfurization treatments were applied to the core-shell structure and both treatments enhanced the material＇s photocatalytic activity and stability by eliminating crystalline defects and surface states.The result showed that thermal annealing treatment improved the bulk crystallinity and hydrothermal sulfurization improved the surface properties.The sample subjected to both treatments showed the highest photocatalytic activity.These results indicate that CdS/ZnS core-shell microspheres are a simple structure that can be used as efficient photocatalysts.The hydrothermal sulfurization treatment may also be a useful surface treatment for metal sulfide photocatalysts.The simple two-step method provides a promising approach to the large-scale synthesis of core-shell microsphere catalysts.
基金Open Foundation of Key Laboratory of Information Management and Information Economics (NoF0607-42)
文摘To avoid the isolation between the external and the internal information of enterprise information systems, a four-layer integrated framework is proposed on the basis of integrating Web2. 0 and the service- oriented architecture （SOA）, which contains the data layer, the service layer, the presentation layer and the collaboration layer. The presentation layer plays the key role, converging the external information from the collaboration layer to the inside of information system （IS）, and diffusing the internal information from the service layer to public users. This framework can also illustrate how users contribute to producing new services, and how web services are integrated to collaborate with public users.
文摘Static corrections using the conventional method are basically conducted in two steps, the weathering correction followed by the correction from the top of the sub-weathering to the unified datum. However, the conventional method fails to well deal with statics problems in case the top of the sub-weathering is sharply undulated and the lateral velocity of the sub-weathering varies significantly. This brings us to the introduction of a smooth intermediate reference datum （IRD） located under the top of the sub-weathering, which helps to further increase the accuracy of statics based on the weathering corrections, and ensures the imaging quality. Good results based on the IRD technique have been achieved in the complex areas in western China. This paper discusses the IRD functions, its application requirements, and selection of related parameters. Some typical sections for comparison are also given in this paper.
