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AFS-3100型原子荧光光谱仪测定食品中汞含量 被引量:2
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作者 朱国英 《现代农业科技》 2012年第13期298-298,300,共2页
随着人们生活水平的提高,对食品安全的要求越来越高,食品中重金属检测任务越来越重。依据GB/T5009.17-2003《卫生部食品总汞的测定标准方法》,采用AFS-3100型原子荧光光谱仪测定食品中的汞,结果表明,该方法测定值准确度较高,可用于食品... 随着人们生活水平的提高,对食品安全的要求越来越高,食品中重金属检测任务越来越重。依据GB/T5009.17-2003《卫生部食品总汞的测定标准方法》,采用AFS-3100型原子荧光光谱仪测定食品中的汞,结果表明,该方法测定值准确度较高,可用于食品中汞含量的测定。 展开更多
关键词 AFS-3100型原子荧光光谱仪 食品汞含量 检测 前处理 测定方法
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食品中汞的热分解齐化原子吸收测定法 被引量:3
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作者 刘祖强 刘开钳 +2 位作者 白洁冰 邵鹏 李红华 《职业与健康》 CAS 2012年第16期1977-1978,1981,共3页
目的使用直接测汞仪,建立测定食品中汞含量的新方法。方法采用热分解齐化原子吸收法,直接测定食品中汞的含量。结果回归方程为A=0.043 0 Hg+0.0160相关系数为R=0.999 5,线性范围为0.00~10.00 ng,精密度为0.62%~17.2%,回收率为85.8%~1... 目的使用直接测汞仪,建立测定食品中汞含量的新方法。方法采用热分解齐化原子吸收法,直接测定食品中汞的含量。结果回归方程为A=0.043 0 Hg+0.0160相关系数为R=0.999 5,线性范围为0.00~10.00 ng,精密度为0.62%~17.2%,回收率为85.8%~105.8%,检出限为0.03 ngHg。结论该方法操作简便快速,各项指标均可满足食品中汞的测定要求。 展开更多
关键词 直接测 食品含量 热分解齐化原子吸收法
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Distribution of Mercury in a Gadoid Fish Species, Tusk (Brosme brosme), and Its Implication for Food Safety
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作者 Kristine Kvangarsnes Sylvia Frantzen +3 位作者 Kare Julshamn Leif J. Saethret Kjell Nedreaas Amund Maage 《Journal of Food Science and Engineering》 2012年第11期603-615,共13页
The tusk (Brosme brosme) is a popular gadoid fish for human consumption, which also is susceptible to mercury accumulation. However, few data of mercury levels in tusk exist, and it is difficult to compare tusk fish... The tusk (Brosme brosme) is a popular gadoid fish for human consumption, which also is susceptible to mercury accumulation. However, few data of mercury levels in tusk exist, and it is difficult to compare tusk fished from assumed contaminated areas with background levels. The aim of this study was to increase the information of mercury levels observed in tusk from the Northeast Atlantic Ocean. Samples of tusk were collected from seven different localities in open ocean areas, nine along the Norwegian coastal current (NCC), and from two fjord stations. Determinations of mercury in muscle and liver were carried out using inductive coupled plasma mass spectrometry (ICPMS) after microwave-assisted wet digestion. The highest concentrations of mercury in muscle were found in tusk captured from the fjords Hardangerfjord and Sorfjord, and had mean concentrations of mercury at 1.5 and 1.7 mg kg"~ wet weight (ww), respectively, where all of the tusk exceeded EU's upper limit of 0.5 mg kg1 ww. The lowest concentrations of mercury were observed in tusk captured from the open ocean areas, and the concentrations ranged from 0.08 to 0.30 mg kg-1 ww. Mercury concentrations of tusk captured along the NCC ranged from 0.21 to 0.49 mg kg-1 ww. Mercury concentrations increased with the weight of the tusk, and variance analysis (ANOVA) of weight normalized mercury concentrations showed that there were significant differences in mercury concentrations between tusk collected from the open ocean, NCC and fjords, which indicates that differences in mercury concentration between different areas arecaused by other factors. 展开更多
关键词 Tusk MERCURY food safety U-864 ICPMS.
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