德国波恩Rheinishe Friedrich—Wilhelms大学学者K.Lachenmeier等人在“EjEAFChe,Electronic Journal of Environmental,Agricultural and Food Chemistry”2006,5(3),1380~1388页上用英文发表的文章报道一种实验设计使固相微...德国波恩Rheinishe Friedrich—Wilhelms大学学者K.Lachenmeier等人在“EjEAFChe,Electronic Journal of Environmental,Agricultural and Food Chemistry”2006,5(3),1380~1388页上用英文发表的文章报道一种实验设计使固相微萃取法从橙汁中提取香味物的条件最优化(同时进行GC和GC/MS分析)。展开更多
Unfavorable fishy odour is an inevitable problem in aquatic products. In the present study, headspace solid-phase mi- croextraction gas chromatography mass spectrometry (HS-SPME-GC-MS) analysis of volatiles from unt...Unfavorable fishy odour is an inevitable problem in aquatic products. In the present study, headspace solid-phase mi- croextraction gas chromatography mass spectrometry (HS-SPME-GC-MS) analysis of volatiles from untreated samples and three deodorized samples (under the optimal conditions) ofPaphia undulata enzymatic hydrolysate revealed that the compounds contrib- uting to the distinctive odor were 1-octen-3-ol, n-hexanal, n-heptanal, 2,4-heptadienal, and 2,4-decadienal, whereas n-pentanal, n-octanal, n-octanol, benzaldehyde, 2-ethylfuran and 2-pentylfuran were the main contributors to the aromatic flavor. The deodoriz- ing effects of activated carbon (AC) adsorption, yeast extract (YE) masking and tea polyphenol (TP) treatment on a P. undulata en- zymatic hydrolysate were investigated using orthogonal experiments with sensory evaluation as the index. The following optimized deodorization conditions were obtained: AC adsorption (35 mg mL-1, 80℃, 40 rain), YE masking (7 mgmL l, 45 ℃, 30 min) and TP treatment (0.4mgmL-l, 40℃, 50min). AC adsorption effectively removed off-flavor volatile aldehydes and ketones. YE masking modified the odor profile by increasing the relative contents of aromatic compounds and decreasing the relative contents of aldehydes and ketones. The TP treatment was not effective in reducing the odor score, but it significantly reduced the relative content of alde- hydes while increasing that of alkanes. It is also notable that TP effectively suppressed trimethylamine (TMA) formation in a P. un- dulate hydrolysate solution for a period of 72 h.展开更多
[Objective] The aim was to study the aromas composition of plum fruit. [Method] The aroma components of six kinds of plum fruits were analyzed by SPME, detected and identified by GC-MS.[Result] 85 kinds of aroma subst...[Objective] The aim was to study the aromas composition of plum fruit. [Method] The aroma components of six kinds of plum fruits were analyzed by SPME, detected and identified by GC-MS.[Result] 85 kinds of aroma substances were separated and identified, including 40 kinds of common components.The experiments had good reproducibility by strictly controlling the desorption temperature, time and sample holding time.The obtained chromatographic peak retention time and the normalized area variation coefficient CV% values were between 0.03% -0.54% and 5.85% -18.08% by experimenting the five precision of AoLi13.The qualitative and quantitative were fully meet repeatability requirements for test samples. [Conclusion] The study provided scientific basis for the development and process of plum industry in China.展开更多
The study of multi-modal communication has only recently been extended to innate and learned interactions between flowers and their animal visitors, and usually only to pollinators. Here we studied the relevance of fl...The study of multi-modal communication has only recently been extended to innate and learned interactions between flowers and their animal visitors, and usually only to pollinators. Here we studied the relevance of floral scent and visual display of a night blooming, putatively hawkmoth-pollinated plant Oenothera acaulis (Onagraceae) in the attraction of non-native cockroaches Blatta orientalis (Blattodea: Blattidae), which function as facultative floral larcenists in coastal habitats of central Chile. We experimentally decoupled visual (corolla) and olfactory (fragrance) stimuli by presenting paper corollas and green mesh bags, with or without a freshly-picked natural flower inside. We then contrasted the behavioral responses of roaches in these treatments with those to the natural combination of traits in actual flowers and their respective control treatments, measuring the roaches' frequency of first visits, mean and total residence time spent in each treatment. The roaches primarily used olfactory cues when approaching O. acaulis flowers at two biologically relevant spatial scales. In addition, the presence of conspecific roaches had a strong influence on recruitment to the experimental arena, increasing the statistical differences among treatments. Our results suggest a primacy of floral fragrance over visual stimuli in the foraging responses of B. orientalis. Olfactory cues were necessary and sufficient to attract the roaches, and the visual cues presented in our manipulations only marginally increased their attraction within a 20 cm diameter of the stimulus. The full spectrum of floral visitation behavior was not elicited by the artificial flowers, suggesting the need for additional tactile or contact chemosensory stimuli not provided by paper. Although the nitrogenous scent compounds that we found in O. acaulis flowers are almost exclusively found in hawkmoth-pollinated flowers, the attractiveness of these compounds to a non-native, facultative flower-visiting insect indicates that they do not function as pollinator-specific signals for hawkmoth attraction .展开更多
贴心的妈妈总是会在各种节日前为宝宝准备好应景的礼物。现在就特别为你带来全球最新万圣节主题的各式潮玩小物及服装配饰,相信会给你的宝宝和家人带来别样惊喜!Xia Home Fashions南瓜鬼脸包去参加万圣节派对一定要在细节上花点工夫才...贴心的妈妈总是会在各种节日前为宝宝准备好应景的礼物。现在就特别为你带来全球最新万圣节主题的各式潮玩小物及服装配饰,相信会给你的宝宝和家人带来别样惊喜!Xia Home Fashions南瓜鬼脸包去参加万圣节派对一定要在细节上花点工夫才能让你在一众人中脱颖而出!Xia Home Fashions推出的这款万圣节主题包袋,一双传神的大眼睛出现在包袋的正面,配合各种色彩和细节变身成一系列有趣的包袋造型。让宝宝拎上它去参加万圣节派对狂欢吧!展开更多
文摘德国波恩Rheinishe Friedrich—Wilhelms大学学者K.Lachenmeier等人在“EjEAFChe,Electronic Journal of Environmental,Agricultural and Food Chemistry”2006,5(3),1380~1388页上用英文发表的文章报道一种实验设计使固相微萃取法从橙汁中提取香味物的条件最优化(同时进行GC和GC/MS分析)。
基金supported by the Public Science and Technology Research Funds Projects of Ocean (No.201305018)the National Key Technology Research and Development Program for the 12th Five-Year Plan (No.2012BAD33B10)+3 种基金the National Natural Science Foundation of Guangdong, China (Nos. 2014A 030310351 and 2014A030310338)the Innovative Development of Marine Economy Regional Demonstration Projects of Guangdong (Nos.SZHY2012-B01-004 and GD2013-B03-001)the Science and Technology Planning Project of Guangdong Province, China (Nos.2013B 090800002 and 2015B090904003)the National Science Foundation for Young Scientists of China (No.31101271)
文摘Unfavorable fishy odour is an inevitable problem in aquatic products. In the present study, headspace solid-phase mi- croextraction gas chromatography mass spectrometry (HS-SPME-GC-MS) analysis of volatiles from untreated samples and three deodorized samples (under the optimal conditions) ofPaphia undulata enzymatic hydrolysate revealed that the compounds contrib- uting to the distinctive odor were 1-octen-3-ol, n-hexanal, n-heptanal, 2,4-heptadienal, and 2,4-decadienal, whereas n-pentanal, n-octanal, n-octanol, benzaldehyde, 2-ethylfuran and 2-pentylfuran were the main contributors to the aromatic flavor. The deodoriz- ing effects of activated carbon (AC) adsorption, yeast extract (YE) masking and tea polyphenol (TP) treatment on a P. undulata en- zymatic hydrolysate were investigated using orthogonal experiments with sensory evaluation as the index. The following optimized deodorization conditions were obtained: AC adsorption (35 mg mL-1, 80℃, 40 rain), YE masking (7 mgmL l, 45 ℃, 30 min) and TP treatment (0.4mgmL-l, 40℃, 50min). AC adsorption effectively removed off-flavor volatile aldehydes and ketones. YE masking modified the odor profile by increasing the relative contents of aromatic compounds and decreasing the relative contents of aldehydes and ketones. The TP treatment was not effective in reducing the odor score, but it significantly reduced the relative content of alde- hydes while increasing that of alkanes. It is also notable that TP effectively suppressed trimethylamine (TMA) formation in a P. un- dulate hydrolysate solution for a period of 72 h.
基金Supported by Hebei Handan Key Research Subject(2011-33)
文摘[Objective] The aim was to study the aromas composition of plum fruit. [Method] The aroma components of six kinds of plum fruits were analyzed by SPME, detected and identified by GC-MS.[Result] 85 kinds of aroma substances were separated and identified, including 40 kinds of common components.The experiments had good reproducibility by strictly controlling the desorption temperature, time and sample holding time.The obtained chromatographic peak retention time and the normalized area variation coefficient CV% values were between 0.03% -0.54% and 5.85% -18.08% by experimenting the five precision of AoLi13.The qualitative and quantitative were fully meet repeatability requirements for test samples. [Conclusion] The study provided scientific basis for the development and process of plum industry in China.
基金Acknowledgements We thank F. Salinas and A. Villagra for their help finding Oenothera acaulis populations in coastal Central Chile, and S. Herrera and R. Yuri for their help with the field experiments. We acknowledge J. C. Ortuzar, J. Alcayaga, M. Cannals and D. Dominguez, A. Jimenez and R. Suarez for their statistical advices and constructive comments. Special thanks to R. Kaiser for the generous gift of authentic standard compounds for 3-methyl butyraldoxime and 2-methyl butyraldoxime for GC-MS analysis of floral scent. This research was funded by postdoctoral FONDECYT grant No 3095002 to C. A. Villagra, US National Science Foundation grant DEB-0317217 to R. A. Raguso and Contracts ICM P02-005 and PFB-23 to the Instituto de Ecologfa y Biodiversidad. Finally, we are thanks to Shmutzer family and BioParque Puquen staff, Los Molles, V Region, Comuna de La Ligua, Chile for their hospitality and involvement.
文摘The study of multi-modal communication has only recently been extended to innate and learned interactions between flowers and their animal visitors, and usually only to pollinators. Here we studied the relevance of floral scent and visual display of a night blooming, putatively hawkmoth-pollinated plant Oenothera acaulis (Onagraceae) in the attraction of non-native cockroaches Blatta orientalis (Blattodea: Blattidae), which function as facultative floral larcenists in coastal habitats of central Chile. We experimentally decoupled visual (corolla) and olfactory (fragrance) stimuli by presenting paper corollas and green mesh bags, with or without a freshly-picked natural flower inside. We then contrasted the behavioral responses of roaches in these treatments with those to the natural combination of traits in actual flowers and their respective control treatments, measuring the roaches' frequency of first visits, mean and total residence time spent in each treatment. The roaches primarily used olfactory cues when approaching O. acaulis flowers at two biologically relevant spatial scales. In addition, the presence of conspecific roaches had a strong influence on recruitment to the experimental arena, increasing the statistical differences among treatments. Our results suggest a primacy of floral fragrance over visual stimuli in the foraging responses of B. orientalis. Olfactory cues were necessary and sufficient to attract the roaches, and the visual cues presented in our manipulations only marginally increased their attraction within a 20 cm diameter of the stimulus. The full spectrum of floral visitation behavior was not elicited by the artificial flowers, suggesting the need for additional tactile or contact chemosensory stimuli not provided by paper. Although the nitrogenous scent compounds that we found in O. acaulis flowers are almost exclusively found in hawkmoth-pollinated flowers, the attractiveness of these compounds to a non-native, facultative flower-visiting insect indicates that they do not function as pollinator-specific signals for hawkmoth attraction .
文摘贴心的妈妈总是会在各种节日前为宝宝准备好应景的礼物。现在就特别为你带来全球最新万圣节主题的各式潮玩小物及服装配饰,相信会给你的宝宝和家人带来别样惊喜!Xia Home Fashions南瓜鬼脸包去参加万圣节派对一定要在细节上花点工夫才能让你在一众人中脱颖而出!Xia Home Fashions推出的这款万圣节主题包袋,一双传神的大眼睛出现在包袋的正面,配合各种色彩和细节变身成一系列有趣的包袋造型。让宝宝拎上它去参加万圣节派对狂欢吧!