Fine-grained Mg-6Zn-4Y alloy was prepared by an ingot metallurgy process with hot extrusion at 300 ℃.The microstructure was studied by XRD,OM,SEM and TEM,and the tensile properties were tested at room temperature.The...Fine-grained Mg-6Zn-4Y alloy was prepared by an ingot metallurgy process with hot extrusion at 300 ℃.The microstructure was studied by XRD,OM,SEM and TEM,and the tensile properties were tested at room temperature.The results show that the alloy is composed of α-Mg and W-phase.The microstructure of the as-extruded alloy has a bimodal grain size distribution.The fine grains with the mean size of 1.2 μm are formed by dynamic recrystallization.The coarse grains（about 23% in area fraction） are unrecrystallized regions which are elongated along extrusion direction.The engineering stress—strain curve shows a pronounced yield point.The ultimate tensile strength,yield strength,and elongation are（371±10） MPa,（350±5） MPa and（7±2）%,respectively.The high strengths are attributed to the fine-grained matrix structure enhanced by W-phase particles,nano-scaled precipitates,and strong basal plane texture.展开更多
The Co-Cr-W ternary system was critically assessed using the CALPHAD technique.The solution phases including the liquid,γ-Co,ε-Co and α-Cr were described by a substitutional solution model.The σ,μ and R phases we...The Co-Cr-W ternary system was critically assessed using the CALPHAD technique.The solution phases including the liquid,γ-Co,ε-Co and α-Cr were described by a substitutional solution model.The σ,μ and R phases were described by three-sublattice models of（Co,W）8（Cr,W）4（Co,Cr,W）18,（Co,Cr,W）7W2（Co,Cr,W）4 and（Co,W）27（Cr,W）14（Co,Cr,W）12,respectively,in order to reproduce their homogeneity ranges.A self-consistent set of thermodynamic parameters for each phase was derived.The calculated isothermal sections at 1 000,1 200 and 1 350 ℃ are in good agreement with the experimental data.A eutectoid reaction of R μ＋γ-Co＋σ in this ternary system was predicted to occur at 1 022 ℃.展开更多
The evolution of microstructure and microhardness was studied in a commercial tungsten-25%rhenium(mass fraction)(W-25Re)alloy processed by the high pressure torsion(HPT)procedure under a pressure of7.7GPa up to10revol...The evolution of microstructure and microhardness was studied in a commercial tungsten-25%rhenium(mass fraction)(W-25Re)alloy processed by the high pressure torsion(HPT)procedure under a pressure of7.7GPa up to10revolutions at different temperatures.The results show that the samples processed by10revolutions at room temperature could have the smallest grain size at around0.209μm.High saturation hardness(HV^1200)could be achieved after the rapid strengthening stage for samples processed by10revolutions both at room temperature and at573K.Microstructural observation and analysis from Hall-Patch relationship could reveal that grain refinement and grain boundaries strengthening are the main factors of hardening mechanism in W-25Re alloy.It is also demonstrated that sintered W-25Re sample may have brittle phase separation phenomenon after HPT processing.展开更多
High-Q notch cavities combined with a low-order E-plane fin-line filter are used for designing a sharp-rejection band-pass filter （BPF） at W-band. Based on the conventional E-plane fin-line structure, an E-plane ext...High-Q notch cavities combined with a low-order E-plane fin-line filter are used for designing a sharp-rejection band-pass filter （BPF） at W-band. Based on the conventional E-plane fin-line structure, an E-plane extended cavity is implemented to enhance the suppression at unwanted frequency points near the passband. The passband performance is not disturbed and the whole structure remains simple to be assembled. To extend the suppression bandwidth, two separated notch cavities are designed and arranged at the input and output ends of the fin-line filter, respectively. A prototype BPF is fabricated and measured. Experimental results show that the minimum insertion loss is 2.7 dB over a passband of 1 GHz. The suppression is about 85 dB near 91.7 GHz, which is 2.2 GHz lower than the center frequency. Experimental results agree well with simulation.展开更多
The coarsening behavior ofγʹprecipitate phase at different temperatures and the compressive performance of novel Co-Ni-Al-W superalloy were investigated.Experiment results show that the evolution of the mean radius a...The coarsening behavior ofγʹprecipitate phase at different temperatures and the compressive performance of novel Co-Ni-Al-W superalloy were investigated.Experiment results show that the evolution of the mean radius and volume fraction of theγʹphase obeys the classical Lifshitz-Slyozov-Wagner model.The coarsening rate of theγʹphase exhibits a significant dependence on the aging temperature,which increases from 1.30×10^(−27)m^(3)/s at 800℃to 9.56×10−27 m^(3)/s at 900℃.The activation energy ofγʹphase is mainly influenced by the W diffusion in theγmatrix,presenting as 210 kJ/mol.The prepared Co-Ni-Al-W alloy possesses superb comprehensive properties,particularly the good combination of highγʹsolvus temperature(1221℃)and low density(8.7 g/cm^(3)).Besides,the compressive yield strength of the Co-Ni-Al-W alloy at ambient and high temperatures are higher than that of otherγʹ-strengthened Co-based superalloys.The compressive yield strength of the Co-Ni-Al-W alloy at 850℃is as high as 774 MPa.展开更多
基金Project (50271054) supported by the National Natural Science Foundation of ChinaProject (20070700003) supported by the Doctorate Programs Foundation of Ministry of Education of China+1 种基金Project (102102210031) supported by the Science and Technologies Foundation of Henan Province, ChinaProject (2010A430008) supported by the Natural Science Foundation of Henan Educational Committee of China
文摘Fine-grained Mg-6Zn-4Y alloy was prepared by an ingot metallurgy process with hot extrusion at 300 ℃.The microstructure was studied by XRD,OM,SEM and TEM,and the tensile properties were tested at room temperature.The results show that the alloy is composed of α-Mg and W-phase.The microstructure of the as-extruded alloy has a bimodal grain size distribution.The fine grains with the mean size of 1.2 μm are formed by dynamic recrystallization.The coarse grains（about 23% in area fraction） are unrecrystallized regions which are elongated along extrusion direction.The engineering stress—strain curve shows a pronounced yield point.The ultimate tensile strength,yield strength,and elongation are（371±10） MPa,（350±5） MPa and（7±2）%,respectively.The high strengths are attributed to the fine-grained matrix structure enhanced by W-phase particles,nano-scaled precipitates,and strong basal plane texture.
基金Project(50771027)supported by the National Basic Research Program of ChinaProject(50771027)supported by the National Natural Science Foundation of China
文摘The Co-Cr-W ternary system was critically assessed using the CALPHAD technique.The solution phases including the liquid,γ-Co,ε-Co and α-Cr were described by a substitutional solution model.The σ,μ and R phases were described by three-sublattice models of（Co,W）8（Cr,W）4（Co,Cr,W）18,（Co,Cr,W）7W2（Co,Cr,W）4 and（Co,W）27（Cr,W）14（Co,Cr,W）12,respectively,in order to reproduce their homogeneity ranges.A self-consistent set of thermodynamic parameters for each phase was derived.The calculated isothermal sections at 1 000,1 200 and 1 350 ℃ are in good agreement with the experimental data.A eutectoid reaction of R μ＋γ-Co＋σ in this ternary system was predicted to occur at 1 022 ℃.
基金Project(11402264)supported by the National Natural Science Foundation of ChinaProject(BK20160182)supported by the Natural Science Foundation of Jiangsu Province,ChinaProjects(JUSRP116027,JUSRP51732B)supported by the Fundamental Research Funds from Jiangnan University,China
文摘The evolution of microstructure and microhardness was studied in a commercial tungsten-25%rhenium(mass fraction)(W-25Re)alloy processed by the high pressure torsion(HPT)procedure under a pressure of7.7GPa up to10revolutions at different temperatures.The results show that the samples processed by10revolutions at room temperature could have the smallest grain size at around0.209μm.High saturation hardness(HV^1200)could be achieved after the rapid strengthening stage for samples processed by10revolutions both at room temperature and at573K.Microstructural observation and analysis from Hall-Patch relationship could reveal that grain refinement and grain boundaries strengthening are the main factors of hardening mechanism in W-25Re alloy.It is also demonstrated that sintered W-25Re sample may have brittle phase separation phenomenon after HPT processing.
基金The National Natural Science Foundation of China(No.60921063)
文摘High-Q notch cavities combined with a low-order E-plane fin-line filter are used for designing a sharp-rejection band-pass filter （BPF） at W-band. Based on the conventional E-plane fin-line structure, an E-plane extended cavity is implemented to enhance the suppression at unwanted frequency points near the passband. The passband performance is not disturbed and the whole structure remains simple to be assembled. To extend the suppression bandwidth, two separated notch cavities are designed and arranged at the input and output ends of the fin-line filter, respectively. A prototype BPF is fabricated and measured. Experimental results show that the minimum insertion loss is 2.7 dB over a passband of 1 GHz. The suppression is about 85 dB near 91.7 GHz, which is 2.2 GHz lower than the center frequency. Experimental results agree well with simulation.
基金Natural Science Foundation of Liaoning Province(2023-MSLH-337)。
文摘The coarsening behavior ofγʹprecipitate phase at different temperatures and the compressive performance of novel Co-Ni-Al-W superalloy were investigated.Experiment results show that the evolution of the mean radius and volume fraction of theγʹphase obeys the classical Lifshitz-Slyozov-Wagner model.The coarsening rate of theγʹphase exhibits a significant dependence on the aging temperature,which increases from 1.30×10^(−27)m^(3)/s at 800℃to 9.56×10−27 m^(3)/s at 900℃.The activation energy ofγʹphase is mainly influenced by the W diffusion in theγmatrix,presenting as 210 kJ/mol.The prepared Co-Ni-Al-W alloy possesses superb comprehensive properties,particularly the good combination of highγʹsolvus temperature(1221℃)and low density(8.7 g/cm^(3)).Besides,the compressive yield strength of the Co-Ni-Al-W alloy at ambient and high temperatures are higher than that of otherγʹ-strengthened Co-based superalloys.The compressive yield strength of the Co-Ni-Al-W alloy at 850℃is as high as 774 MPa.
