Experimental investigation on coal pore-fracture variation and fractal characteristics synergistically affected by solvents for improving clean gas extraction

Chemical solvents instead of pure water being as hydraulic fracturing fluid could effectively increase permeability and improve clean methane extraction efficiency.However,pore-fracture variation features of lean coal synergistically affected by solvents have not been fully understood.Ultrasonic testing,nuclear magnetic resonance analysis,liquid phase mass spectrometry was adopted to comprehensively analyze pore-fracture change characteristics of lean coal treated by combined solvent(NMP and CS_(2)).Meanwhile,quantitative characterization of above changing properties was conducted using geometric fractal theory.Relationship model between permeability,fractal dimension and porosity were established.Results indicate that the end face fractures of coal are well developed after CS2and combined solvent treatments,of which,end face box-counting fractal dimensions range from 1.1227 to 1.4767.Maximum decreases in ultrasonic longitudinal wave velocity of coal affected by NMP,CS_(2)and combined solvent are 2.700%,20.521%,22.454%,respectively.Solvent treatments could lead to increasing amount of both mesopores and macropores.Decrease ratio of fractal dimension Dsis 0.259%–2.159%,while permeability increases ratio of NMR ranges from 0.1904 to 6.4486.Meanwhile,combined solvent could dissolve coal polar and non-polar small molecules and expand flow space.Results could provide reference for solvent selection and parameter optimization of permeability-enhancement technology.

Experimental Study on Hydrodynamic Load Characteristics for A Typical Cross-Section of A Submerged Floating Tunnel

The typical cross-sectional form of a submerged floating tunnel plays a significant role in the dynamic response of the tunnel itself,which directly affects the overall design.In this work,a series of experiments involving wave action on a submerged floating tube cross section is reported to study its hydrodynamic load characteristics.Two typical cross section tube cylinders,circular and rectangular,are chosen.Experiments are carried out in a wave flume with waves of relatively low Keulegan-Carpenter(KC)numbers.Three relative depths of submergence of 0,0.25 and 0.5 are chosen.The measured wave forces in regular waves are used to analyze the horizontal force,vertical force and torque,and then the drag coefficient(Cd)and inertia coefficient(Cm)are derived.The results show that the drag coefficients at low KC numbers are large and decrease sharply with increasing KC number.The inertial coefficient Cm values in the vertical direction are about 70%larger than those in the horizontal direction.With an increase in aspect ratio(the ratio of the height to width of the structure),the ratio of inertia coefficient in the horizontal direction to that in the vertical direction increases remarkably.The inertia force coefficient is very sensitive to the submerged water depth and aspect ratio.The existing results may overestimate the actual force value.

Experimental study of the damage characteristics of rocks containing non-penetrating cracks under cyclic loading

The damage evolution process of non-penetrating cracks often causes some unexpected engineering disasters.Gypsum specimens containing non-penetrating crack(s)are used to study the damage evolution and characteristics under cyclic loading.The results show that under cyclic loading,the relationship between the number of non-penetrating crack(s)and the characteristic parameters(cyclic number,peak stress,peak strain,failure stress,and failure strain)of the pre-cracked specimens can be represented by a decreasing linear function.The damage evolution equation is fitted by calibrating the accumulative plastic strain for each cycle,and the damage constitutive equation is proposed by the concept of effective stress.Additionally,non-penetrating cracks are more likely to cause uneven stress distribution,damage accumulation,and local failure of specimen.The local failure can change the stress distribution and relieve the inhibition of non-penetrating crack extension and eventually cause a dramatic destruction of the specimen.Therefore,the evolution process caused by non-penetrating cracks can be regarded as one of the important reasons for inducing rockburst.These results are expected to improve the understanding of the process of spalling formation and rockburst and can be used to analyze the stability of rocks or rock structures.

Experimental Study on the Variation of Optical Imaging Characteristics with Zenith Angle due to Internal Solitary Waves in Sunglint

Internal solitary waves(ISWs)change the roughness of the sea surface,thus producing dark and bright bands in optical images.However,reasons for changes in imaging characteristics with the solar zenith angle remain unclear.In this paper,the optical imaging pattern of ISWs in sunglint under different zenith angles of the light source is investigated by collecting optical images of ISWs through physical simulation.The experiment involves setting 10 zenith angles of the light source,which are divided into area a the optical images of ISWs in the three areas show dark-bright mode,single bright band,and bright-dark mode,which are consistent with those observed by optical remote sensing.In addition,this study analyzed the percentage of the dark and bright areas of the bands and the change in the relative gray difference and found changes in both areas under different zenith angles of the light source.The MODIS and ASAR images display a similar brightness-darkness distance of the same ISWs.Therefore,the relationship between the brightness-darkness distance and the characteristic half-width of ISWs is determined in accordance with the eKdV theory and the imaging mechanism of ISWs of the SAR image.Overall,the relationship between them in the experiment is almost consistent with the theoretical result.

The occurrence characteristics of oil in shales matrix from organic geochemical screening data and pore structure properties:An experimental study Author links open overlay panel

The occurrence characteristics of shale oil are of great significance to the movability of shale oil.In this study,the occurrence characteristics of oil in the shale matrix at Funing Formation shale in Subei Basin were quantitatively evaluated by organic geochemistry and microscopic pore structure characterization experiments.The Multiple Isothermal Stages Pyrolysis(MIS)experiment results show that the content of total oil,adsorbed oil,and free oil in the shales are 3.15-11.25 mg/g,1.41-4.95 mg/g,and 1.74-6.51 mg/g,respectively.among which the silicon-rich shale has the best oil-bearing.The relative content of free oil shows an increasing trend in pores with pore diameters greater than 3 nm.When the relative content of free oil reaches 100%,the pore size of silicon-rich shale is about 200 nm,while that of calcium-rich shale,clay-rich shale,and siliceous mixed shale is about 10 nm.The occurrence law of adsorbed oil is opposite to that of free oil,which indicates that shale oil will occur in the pores and fractures in a free state in a more extensive pore size range(>200 nm).This study also enables us to further understand the occurrence characteristics of shale oil under the interaction of occurrence state and occurrence space.

Experimental study on the variation of optical remote sensing imaging characteristics of internal solitary waves with wind speed

Optical remote sensing has been widely used to study internal solitary waves(ISWs).Wind speed has an important effect on ISW imaging of optical remote sensing.The light and dark bands of ISWs cannot be observed by optical remote sensing when the wind is too strong.The relationship between the characteristics of ISWs bands in optical remote sensing images and the wind speed is still unclear.The influence of wind speeds on the characteristics of the ISWs bands is investigated based on the physical simulation experiments with the wind speeds of 1.6,3.1,3.5,3.8,and 3.9 m/s.The experimental results show that when the wind speed is 3.9 m/s,the ISWs bands cannot be observed in optical remote sensing images with the stratification of h_(1)∶h_(2)=7∶58,ρ_(1)∶ρ_(2)=1∶1.04.When the wind speeds are 3.1,3.5,and 3.8 m/s,which is lower than 3.9 m/s,the ISWs bands can be obtained in the simulated optical remote sensing image.The location of the band’s dark and light extremum and the band’s peak-to-peak spacing are almost not affected by wind speed.More-significant wind speeds can cause a greater gray difference of the light-dark bands.This provided a scientific basis for further understanding of ISW optical remote sensing imaging.

Experimental study of the effects of a multistage pore-throat structure on the seepage characteristics of sandstones in the Beibuwan Basin:Insights into the flooding mode

To investigate the relationship between grain sizes, seepage capacity, and oil-displacement efficiency in the Liushagang Formation of the Beibuwan Basin, this study identifies the multistage pore-throat structure as a crucial factor through a comparison of oil displacement in microscopic pore-throat experiments. The two-phase flow evaluation method based on the Li-Horne model is utilized to effectively characterize and quantify the seepage characteristics of different reservoirs, closely relating them to the distribution of microscopic pores and throats. It is observed that conglomerate sandstones at different stages exhibit significant heterogeneity and noticeable differences in seepage capacity, highlighting the crucial role played by certain large pore throats in determining seepage capacity and oil displacement efficiency. Furthermore, it was found that the displacement effects of conglomeratic sandstones with strong heterogeneity were inferior to those of conventional homogeneous sandstone, as evidenced by multiple displacement experiments conducted on core samples with varying granularities and flooding systems. Subsequently, core-based experiments on associated gas flooding after water flooding were conducted to address the challenge of achieving satisfactory results in a single displacement mode for reservoirs with significant heterogeneity. The results indicate that the oil recovery rates for associated gas flooding after water flooding increased by 7.3%-16.4% compared with water flooding alone at a gas-oil ratio of approximately 7000 m^(3)/m^(3). Therefore, considering the advantages of gas flooding in terms of seepage capacity, oil exchange ratio, and the potential for two-phase production, gas flooding is recommended as an energy supplement mode for homogeneous reservoirs in the presence of sufficient gas source and appropriate tectonic angle. On the other hand, associated gas flooding after water flooding is suggested to achieve a more favorable development effect compared to a single mode of energy supplementation for strongly heterogeneous sandstone reservoirs.

Experimental Study on Clogging Characteristics of Silt Soft Soil in Nansha District of Guangzhou

The silt soft soil in Nansha District of Guangzhou was the softest soft soil in China. It had the characteristics of high natural water content, high compressibility, long consolidation time, and complex layered distribution of soil layers. These characteristics formed the clogging characteristics of silt soft soil, which greatly increased the construction difficulty and hindered the construction progress. Therefore, based on the basic physical and mechanical properties of silt soft soil in Nansha District of Guangzhou, this paper evaluated the clogging characteristics of three silt soft soil areas in Nansha District of Guangzhou through long-term permeability test, and carried out scanning electron microscope test to explore the influence of different parameters and microstructure on the clogging difficulty of silt soft soil. The results showed that the silt soft soil Zone I and Zone II (shallow layer) in Nansha District of Guangzhou were divided into slight siltation levels, and the silt soft soil Zone III (deep layer) was mild siltation level. Large pores were widely distributed in shallow silt soft soil, while the continuity of large pores in deep silt soft soil was poor. The migration of fine particles that failed to establish contact with surrounding particles in the soil blocks the small pores of seepage and thus produces siltation.

Blast wave characteristics of multi-layer composite charge:Theoretical analysis,numerical simulation,and experimental validation

This article investigates the characteristics of shock wave overpressure generated by multi-layer composite charge under different detonation modes.Combining dimensional analysis and the explosion mechanism of the charge,a peak overpressure prediction model for the composite charge under singlepoint detonation and simultaneous detonation was established.The effects of the charge structure and initiation method on the overpressure field characteristics were investigated in AUTODYN simulation.The accuracy of the prediction model and the reliability of the numerical simulation method were subsequently verified in a series of static explosion experiments.The results reveal that the mass of the inner charge was the key factor determining the peak overpressure of the composite charge under single-point detonation.The peak overpressure in the radial direction improved apparently with an increase in the aspect ratio of the charge.The overpressure curves in the axial direction exhibited a multi-peak phenomenon,and the secondary peak overpressure even exceeded the primary peak at distances of 30D and 40D(where D is the charge diameter).The difference in peak overpressure among azimuth angles of 0-90°gradually decreased with an increase in the propagation distance of the shock wave.The coupled effect of the detonation energy of the inner and outer charge under simultaneous detonation improved the overpressure in both radial and axial directions.The difference in peak overpressure obtained from model prediction and experimental measurements was less than 16.4%.

Dynamic stiffness characteristics of aero-engine elastic support structure and its effects on rotor systems:mechanism and numerical and experimental studies

The support structure of a rotor system is subject to vibration excitation,which results in the stiffness of the support structure varying with the excitation frequency(i.e.,the dynamic stiffness).However,the dynamic stiffness and its effect mechanism have been rarely incorporated in open studies of the rotor system.Therefore,this study theoretically reveals the effect mechanism of dynamic stiffness on the rotor system.Then,the numerical study and experimental verification are conducted on the dynamic stiffness characteristics of a squirrel cage,which is a common support structure for aero-engine.Moreover,the static stiffness experiment is also performed for comparison.Finally,a rotor system model considering the dynamic stiffness of the support structure is presented.The presented rotor model is used to validate the results of the theoretical analysis.The results illustrate that the dynamic stiffness reduces the critical speed of the rotor system and may lead to a new resonance.

Experimental study of the dynamic mechanical responses and failure characteristics of coal under true triaxial confinements

Investigations on the dynamic mechanical properties and failure mechanisms of coal under in-situ stress is essential for the prevention of dynamic disasters in deep coal mines.Thus,a modified true triaxial Hopkinson bar was employed to explore the dynamic mechanical behaviors of coal at different confining pressures(0–20 MPa)and strain rates(40–220 s^(-1)).The results show that the dynamic peak stress is positively correlated with lateral static pre-stressσy andσz,but negatively correlated with axial static prestressσx.At approximate strain rates,increasing the lateral static pre-stress facilitates increasing the dynamic peak stress,but the minimum lateral static pre-stress is the primary factor limiting a significant increase in dynamic peak stress of coal.Furthermore,the dynamic differential stress is linearly related to the logarithm of strain rate,and the peak strain varies linearly with strain rate.However,there is no significant correlation between confining pressure and peak strain.Moreover,X-ray CT images and photographic fracture observations of coal samples show the failure patterns under uniaxial and triaxial conditions are splitting failure and shear failure,respectively.The device provides a viable approach for fully comprehending the dynamic mechanical behaviors of rock-like material in complex stress conditions.

Implications for identification of principal stress directions from acoustic emission characteristics of granite under biaxial compression experiments

The rock fracture characteristics and principal stress directions are crucial for prevention of geological disasters.In this study,we carried out biaxial compression tests on cubic granite samples of 100 mm in side length with different intermediate principal stress gradients in combination with acoustic emission(AE)technique.Results show that the fracture characteristics of granite samples change from‘sudden and aggregated’to‘continuous and dispersed’with the increase of the intermediate principal stress.The effect of increasing intermediate principal stress on AE amplitude is not significant,but it increases the proportions of high-frequency AE signals and shear cracks,which in turn increases the possibility of unstable rock failure.The difference of stress in different directions causes the anisotropy of rock fracture and thus leads to the obvious anisotropic characteristics of wave velocity variations.The anisotropy of wave velocity variations with stress difference is probable to identify the principal stress directions.The AE characteristics and the anisotropy of wave velocity variations of granite under two-dimensional stress are not only beneficial complements for rock fracture characteristic and principal stress direction identification,but also can provide a new analysis method for stability monitoring in practical rock engineering.

Strength and deformation characteristics of irregular columnar jointed rock mass: A combined experimental and theoretical study

The irregularity of jointed network poses a challenge to the determination of field mechanical param-eters of columnar jointed rock mass(CJRM),and a reasonable prediction of deformation and strength characteristics of CJRM is important for engineering construction.The Voronoi diagram and three-dimensional printing technology were used to make an irregular columnar jointed mold,and the irregular CJRM(ICJRM)specimens with different dip directions and dip angles were prepared.Uniaxial compression tests were performed,and the anisotropic strength and deformation characteristics of ICJRM were described.The failure modes and mechanisms were revealed in accordance with the final appearances of the ICJRM specimens.Based on the model test results,the empirical correlations for determining the field deformation and strength parameters of CJRM were derived using the dip angle and modified joint factor.The proposed empirical equations were used in the Baihetan Project,and the calculated mechanical parameters were compared with the field test results and those obtained from the tunneling quality index method.Results showed that the deformation parameters determined by the two proposed methods are all consistent with the field test results,and these two methods can also estimate the strength parameters effectively.

Experimental analysis of the pore structure, relative permeability, and water flooding characteristics of the Yan'an Formation sandstone, southwestern Ordos Basin

The oil and gas potential of the Yan'an Formation in the Ordos Basin has yet to be fully tapped. In this study, the pore structure, mobile fluid saturation, and water flooding micro-mechanism of the Yan'an Formation sandstone are systematically studied through the application of a series of rock physics and fluid experiments. The results show that there is a good positive correlation between porosity and permeability, and the reservoirs are divided into types Ⅰ, Ⅱ, and Ⅲ. Mercury injection tests show that the average pore throat radius of the oil-bearing reservoir ranges from 1 to 7 μm. The displacement pressure of the Yan'an Formation is also relatively low, and it decreases from 0.1 MPa to 0.01 MPa as the rock porosity increases from 11% to 18%. NMR tests show that small (diameter <0.5 μm) and medium pores (diameter ranging from 0.5 to 2.5 μm) are predominant in the reservoir. Different types of reservoirs have different characteristics of relative permeability curve. In addition, when the average oil recovery rate is less than 1 ml/min, the oil displacement efficiency increases faster. However, when the average oil recovery rate is between 1–3.5 ml/min, the oil displacement efficiency is maintained at around 27%–30%. Physical properties of the reservoir, pore-throat structure, experimental pressure difference, and pore volume injected — all have significant effects on oil displacement efficiency. For Type Ⅰ and Type Ⅱ reservoirs, the increase of the pore volume injected has a significant effect on oil displacement efficiency. However, for Type Ⅲ reservoirs, the change of pore volume injected has insignificant effect on oil displacement efficiency. This study provides a reference for the formulation of estimated ultimate recovery (EUR) measures for similar sandstone reservoirs.

Experimental Study on Phase Characteristics of CO2 Injection in BZ13-2 Strong Volatile Oil Reservoir in Bohai Sea Buried Hills

BZ13-2 oil field is a deep submerged strongly volatile reservoir in Bohai Sea. This oil reservoir has the characteristics of high gas oil ratio and small difference in formation pressure and saturation point pressure. It usually adopts gas injection development to avoid crude oil degassing and fast decreasing production capacity. However, the phase characteristics and miscibility mechanism of this high-temperature and high-pressure fluid after gas injection are not clear. Therefore, it is necessary to study the feasibility of CO2 injection to improve oil recovery in near critical volatile oil reservoirs through CO2 injection experiments. In the early stage of the depletion experiment, the content of heavy components in the remaining oil increased significantly, so the depletion method is not conducive to the development of such reservoirs. With the increase of CO2 injection, the volumetric expansion coefficient of formation crude oil increases significantly, while the saturation pressure and formation crude oil viscosity remain basically unchanged. The minimum miscible pressure experiment shows that CO2 injection under formation pressure conditions can achieve multiphase miscibility. Based on experimental research results, the BZ13-2 oilfield is suitable for early gas injection development and can significantly improve recovery.

Optical remote sensing image characteristics of large amplitude convex mode-2 internal solitary waves:an experimental study

A series of experiments are designed to propose a new method to study the characteristics of convex mode-2internal solitary waves(ISWs)in optical remote sensing images using a laboratory-based optical remote sensing simulation platform.The corresponding wave parameters of large-amplitude convex mode-2 ISWs under smooth surfaces are investigated along with the optical remote sensing characteristic parameters.The mode-2 ISWs in the experimentally obtained optical remote sensing image are produced by their overall modulation effect on the water surface,and the extreme points of the gray value of the profile curve of bright-dark stripes appear at the same location as the real optical remote sensing image.The present data extend to a larger range than previous studies,and for the characteristics of large amplitude convex mode-2 ISWs,the experimental results show a second-order dependence of wavelength on amplitude.There is a close relationship between optical remote sensing characteristic parameters and wave parameters of mode-2 ISWs,in which there is a positive linear relationship between the bright-dark spacing and wavelength and a nonlinear relationship with the amplitude,especially when the amplitude is very large,there is a significant increase in bright-dark spacing.

Flume Experiment Investigation on Propagation Characteristics of Tidal Bore in A Curved Channel

Tidal bore is a special and intensive form of flow movement induced by tidal effect in estuary areas, which has complex characteristics of profile, propagation and flow velocity. Although it has been widely studied for the generation mechanism, propagation features and influencing factors, the curved channel will complicate the characteristics of tidal bore propagation, which need further investigation compared with straight channel. In this study, the flume experiments for both undular and breaking bores’ propagation in curved channel are performed to measure the freesurface elevation and flow velocity by ultrasonic sensors and ADV respectively. The propagation characteristics,including tidal bore height, cross-section surface gradient, tidal bore propagation celerity, and flow velocity are obtained for both sides of the curved channel. And three bore intensities are set for each type of tidal bores. The freesurface gradients are consistently enlarged in high-curvature section for undular and breaking bores, but have distinct behaviors in low-curvature section. The spatial distributions of tidal bore propagation celerity and flow velocity are compared between concave and convex banks. This work will provide experimental reference for engineering design of beach and seawall protection, erosion reduction and siltation promotion in estuary areas with the existence of tidal bores.

Study on Load Bearing Characteristics of Novel Expandable Deepwater Drilling Conductor Based on Laboratory Experiment and Field Test

A novel expandable conductor was designed and applied in deep-water drilling to improve the vertical and lateral bearing capacity with a significant reduction of conductor jetting depth and soaking time. The vertical and lateral bearing capability of expandable conductors was depicted based on the ultimate subgrade reaction method and pile foundation bearing theory. The load-bearing characteristics of a laboratory-scale expandable conductor were analyzed through laboratory experiments. The serial simulation experiments are accomplished to study the bearing characteristics(vertical ultimate bearing capacity, lateral soil pressure, and lateral displacement) during the conductor soaking process. The laboratory experimental results show that the larger the length and thickness of expandable materials are,the higher the bearing capacity of the wellhead will be. During the conductor soaking process, the soil pressure around the three expandable conductors increases faster, strings representing a stronger squeezing effect and resulting in higher vertical bearing capacity. Furthermore, the lateral displacement of novel expandable conductor is smaller than that of the conventional conductor. All the advantages mentioned above contributed to the reduction of conductor’s jetting depth and soaking time. Lastly, the application workflow of a novel expandable deep-water drilling conductor was established and the autonomous expandable conductor was successfully applied in the South China Sea with a significant reduction of conductor’s jetting depth and soaking time. According to the soil properties and designed installation depth of the surface conductor, the arrangement of expandable materials should be designed reasonably to meet the safety condition and reduce the construction cost of the subsea wellhead.

Experimental and numerical simulation study of the effect for the anode positions on the discharge characteristics of 300W class low power Hall thrusters

Low-power Hall thruster(LHT) generally has poor discharge efficiency characteristics due to the large surface-to-volume ratio.Aiming to further refine and improve the performance of 300 W class LHT in terms of thrust and efficiency,and to obtain the most optimal operating point,the experimental study of the discharge characteristics for three different anode positions was conducted under the operation of various discharge voltages(100-400 V) and anode mass flow rates(0.65 mg·s-1and 0.95 mg·s-1).The experimental results indicated that the thruster has the most excellent performance in terms of thrust and efficiency etc at a channel length of 27 mm for identical operating conditions.In addition,particle in cell simulations,employed to reveal the underlying physical mechanisms,show that the ionization and acceleration zone is pushed downwards towards the channel exit as the anode moves towards the exit.At the identical operating point,when the channel length is reduced from 32 to 27 mm,the ionization and acceleration zone moves towards the exit,and the parameters such as thrust and efficiency increase due to the high ionization rate,ion number density,and axial electric field.When the channel length is further moved to 24 mm,the parameters in terms of thrust(F) and efficiency(ηa) are reduced as a result of the decreasing ionization efficiency(ηm) and the larger plume divergence angle(α).In this paper,the results indicated that an optimum anode position(ΔL=27 mm) exists for the optimum performance.

Experimental study on the improvement of spray characteristics of aero-engines using gliding arc plasma

A gliding arc plasma fuel atomization actuator suitable for aeroengines was designed,and a gliding arc plasma fuel spray experimental platform was built to address the fuel atomization problem in aeroengine combustion chambers.The spray characteristics for different airflows,fuel flows,and discharge voltages were analyzed using laser particle size analysis.The research shows that the fuel atomization effect is improved from the increased airflow.The decreased fuel flow not only reduces the injection pressure of the fuel but also changes the discharge mode of the gliding arc,which affects reductions in the discharge power and inhibits fuel atomization.Gliding arc discharges accelerate the breaking,atomization,and evaporation of fuel droplets while reducing the particle size,which increases the proportion of small droplets.Compared with the working conditions of plasma-assisted atomization without the gliding arc,the D0.5,D0.9,and average particle size of the fuel droplets are reduced by 4.7%,6.5%,and 4.1%,respectively,when the modulation voltage of the gliding arc power supply is 200 V.