为充分开发汉麻的应用价值并获得较柔软的棉型化汉麻织物,通过进一步优化选择性氧化汉麻织物制备工艺方案,在单因素方案和正交试验设计的基础上协同利用BBD试验和RSM分析法,以活泼率作为响应值,回归分析高碘酸钠用量、氧化时间、氧化温...为充分开发汉麻的应用价值并获得较柔软的棉型化汉麻织物,通过进一步优化选择性氧化汉麻织物制备工艺方案,在单因素方案和正交试验设计的基础上协同利用BBD试验和RSM分析法,以活泼率作为响应值,回归分析高碘酸钠用量、氧化时间、氧化温度各自变量因素及其交互作用影响。结果表明:正交设计和RSM法优化结果一致,柔软棉型化汉麻织物制备的最佳工艺为:高碘酸钠13 g L,氧化时间1.5 h,氧化温度50℃。优化结果合理可行,在此优化条件下,棉型化汉麻织物活泼率增大、强力损失小、亲水性变好。展开更多
A new composite photocatalyst of modified oyster shell powder/Ce-N-TiO<sub>2</sub> was prepared by sol-gel method. Based on single factor experiment, Ce doping rate, N doping rate and calcination temperatu...A new composite photocatalyst of modified oyster shell powder/Ce-N-TiO<sub>2</sub> was prepared by sol-gel method. Based on single factor experiment, Ce doping rate, N doping rate and calcination temperature were taken as input variables. Based on the central composite design (BBD) response surface model, two functional relationship models between three independent variables and glyphosate removal rate were established to evaluate the influence degree of independent variables and interaction on catalyst. The significance of the model and regression coefficient was tested by variance analysis. The analysis of the obtained data showed that the degradation performance of the composite photocatalyst was significantly affected by the calcination temperature and the rate of N doping, while the rate of Ce doping had little effect;at the calcination temperature of 505.440°C, the degradation rate of glyphosate reached the maximum of 82.15% under the preparation conditions of 17.057 mol% N doping and 0.165 mol% Ce doping, respectively.展开更多
文摘为充分开发汉麻的应用价值并获得较柔软的棉型化汉麻织物,通过进一步优化选择性氧化汉麻织物制备工艺方案,在单因素方案和正交试验设计的基础上协同利用BBD试验和RSM分析法,以活泼率作为响应值,回归分析高碘酸钠用量、氧化时间、氧化温度各自变量因素及其交互作用影响。结果表明:正交设计和RSM法优化结果一致,柔软棉型化汉麻织物制备的最佳工艺为:高碘酸钠13 g L,氧化时间1.5 h,氧化温度50℃。优化结果合理可行,在此优化条件下,棉型化汉麻织物活泼率增大、强力损失小、亲水性变好。
文摘A new composite photocatalyst of modified oyster shell powder/Ce-N-TiO<sub>2</sub> was prepared by sol-gel method. Based on single factor experiment, Ce doping rate, N doping rate and calcination temperature were taken as input variables. Based on the central composite design (BBD) response surface model, two functional relationship models between three independent variables and glyphosate removal rate were established to evaluate the influence degree of independent variables and interaction on catalyst. The significance of the model and regression coefficient was tested by variance analysis. The analysis of the obtained data showed that the degradation performance of the composite photocatalyst was significantly affected by the calcination temperature and the rate of N doping, while the rate of Ce doping had little effect;at the calcination temperature of 505.440°C, the degradation rate of glyphosate reached the maximum of 82.15% under the preparation conditions of 17.057 mol% N doping and 0.165 mol% Ce doping, respectively.
