A series of heat treatments using the orthogonal experiment method were performed to study the microstruc- ture and mechanical properties of 1Cr12NiMo martensitic stainless steel containing various nitrogen content ad...A series of heat treatments using the orthogonal experiment method were performed to study the microstruc- ture and mechanical properties of 1Cr12NiMo martensitic stainless steel containing various nitrogen content addition. The results indicate that the optimal heat treatment is annealing at 830 ℃ for 1 h, austenitizing at 985 ℃ for 1 h followed by oil quenching, and tempering at 630 ℃ for 4 h followed by air cooling, Nitrogen addition to 1Cr12NiMo steel can effectively hinder the austenite grain growth, refine the martensite lath, and increase the strength and hardness. The impact toughness of this steel only shows a minor decrease as the nitrogen content increases.展开更多
In view of developing novel alloys for applications in supercritical water-cooled reactor fuel cladding and in-core components, a 12%Cr reduced activation ferrite/martensite(RAFM) steel with good corrosion resistance ...In view of developing novel alloys for applications in supercritical water-cooled reactor fuel cladding and in-core components, a 12%Cr reduced activation ferrite/martensite(RAFM) steel with good corrosion resistance and irradiation performance was developed. V and Ta were added to form fine MX type carbonitrides and enhance the high temperature creep rupture strength. Microstructure stability of the steel during long-term aging at 650 C was studied experimentally combined with the simulation of ThermoCalc and DICTRA software. The results show that the precipitates in the steel during long-term aging contain M23C6, MX and Laves phase. M23C6 carbides play a major role in the stabilization of the tempered martensite lath structure by exerting a large Zener pinning force as compared with MX and Laves phase.Adding V and Ta in the steel can not only promote MX precipitation, but also refine M23C6 carbides and thus improve the thermal stability of lath/subgrains, which is beneficial to the improvement of high temperature microstructure stability of the 12%Cr RAFM steel.展开更多
基金supported by the National Key Technology R&D Program,China(No.2011BAA06B02)
文摘A series of heat treatments using the orthogonal experiment method were performed to study the microstruc- ture and mechanical properties of 1Cr12NiMo martensitic stainless steel containing various nitrogen content addition. The results indicate that the optimal heat treatment is annealing at 830 ℃ for 1 h, austenitizing at 985 ℃ for 1 h followed by oil quenching, and tempering at 630 ℃ for 4 h followed by air cooling, Nitrogen addition to 1Cr12NiMo steel can effectively hinder the austenite grain growth, refine the martensite lath, and increase the strength and hardness. The impact toughness of this steel only shows a minor decrease as the nitrogen content increases.
基金supported by the National Basic Research Program of China (Grant No. 2007CB209801)the National Natural Science Fundation of China (Grant No. 51371030)the National High Technology Research and Development Program of China (Grant No. 2013AA031601)
文摘In view of developing novel alloys for applications in supercritical water-cooled reactor fuel cladding and in-core components, a 12%Cr reduced activation ferrite/martensite(RAFM) steel with good corrosion resistance and irradiation performance was developed. V and Ta were added to form fine MX type carbonitrides and enhance the high temperature creep rupture strength. Microstructure stability of the steel during long-term aging at 650 C was studied experimentally combined with the simulation of ThermoCalc and DICTRA software. The results show that the precipitates in the steel during long-term aging contain M23C6, MX and Laves phase. M23C6 carbides play a major role in the stabilization of the tempered martensite lath structure by exerting a large Zener pinning force as compared with MX and Laves phase.Adding V and Ta in the steel can not only promote MX precipitation, but also refine M23C6 carbides and thus improve the thermal stability of lath/subgrains, which is beneficial to the improvement of high temperature microstructure stability of the 12%Cr RAFM steel.