An accurate flow stress model was established by considering the parameters of strain rate,strain and temperature as well asβ→a+βphase transformation in order to develop the plastic forming theory of TC18 titanium ...An accurate flow stress model was established by considering the parameters of strain rate,strain and temperature as well asβ→a+βphase transformation in order to develop the plastic forming theory of TC18 titanium alloy.Firstly,the phase transition kinetics of TC18 titanium alloy during isothermal and continuous cooling at 1073 and 1273 K was studied by thermodynamic calculation,meanwhile,the relationship of volume fraction of phase transition with temperature and time was obtained.Constitutive models were calculated by investigating flow behaviors under hot compression tests with the strain rates of 0.001-1s^(-1) and temperatures of 973-1223 K in the singleβand a+βregions in TC18 titanium alloy,respectively.By combining the phase transformation dynamic kinetics with constitutive models,an accurate flow stress model was established,providing theoretical basis and data support for the hot forging of TC18 titanium alloy.展开更多
The microstructural evolution of a 18R single phase （S 18） alloy during annealing at 773 K for 100 h was investigated in order to reveal the formation mechanism of 14H phase. The results showed that the as-cast S 18...The microstructural evolution of a 18R single phase （S 18） alloy during annealing at 773 K for 100 h was investigated in order to reveal the formation mechanism of 14H phase. The results showed that the as-cast S 18 alloy was composed of 18R phase （its volume fraction exceeds 93%）, W particles and α-Mg phase. The 18R phase in S18 alloy was thermally stable and was not transformed into 14H long period stacking ordered （LPSO） phase during annealing. However, 14H lamellas formed within tiny α-Mg slices, and their average size and volume fraction increased with prolonging annealing time. Moreover, the 14H phase is nucleated within α-Mg independently on the basis of basal stacking faults （SFs）. The broadening growth of 14H lamellas is an interface-controlled process which involves ledges on basal planes, while the lengthening growth is a diffusion-controlled process and is associated with diffusion of solute atoms. The formation mechanism of 14H phase in this alloy could be explained as α-Mg＇→α-Mg＋14H.展开更多
A series of single bcc,bcc plus fcc duplex and single fcc microcrystalline coatings of 1Cr18Ni9Ti stainless steel were prepared by using sputtering technique.The resistance against pitting corrosion was studied by mea...A series of single bcc,bcc plus fcc duplex and single fcc microcrystalline coatings of 1Cr18Ni9Ti stainless steel were prepared by using sputtering technique.The resistance against pitting corrosion was studied by measurements of pitting corrosion potentials and electrochemical noise during initiation of corrosion pits.The results show that the sputtered coatings with single bcc phase or single fcc structure are more resistant to pitting corrosion than those with bcc plus fcc duplex phase structure.展开更多
used－silical capillary columns containing heptakis（2、3、6－tri－o－pentyl）-β-cyclodextrinand dibenzo-18-crown-6 were prepared．By studying the selectivity of mixed stationary phases forsome solute pairs.as well a...used－silical capillary columns containing heptakis（2、3、6－tri－o－pentyl）-β-cyclodextrinand dibenzo-18-crown-6 were prepared．By studying the selectivity of mixed stationary phases forsome solute pairs.as well as comparing with the heptakis（2．3、6-tri-O-pentyl）-β-cyclodextrin and thedibenzo-18-crown-6 used as individual stationary phase、the synergistic effects were observed.These effects were affected by the column temperature．mixed ratio and linear velocity of carrier gas．展开更多
Globally,about 70% of cervical cancers are associated with human papillomavirus (HPV)-16 or HPV-18 infection.A meta-analysis of epidemiologic studies in China showed that HPV was present in 98% of cervical cancer samp...Globally,about 70% of cervical cancers are associated with human papillomavirus (HPV)-16 or HPV-18 infection.A meta-analysis of epidemiologic studies in China showed that HPV was present in 98% of cervical cancer samples.The HPV-16/18 AS04-adjuvanted vaccine Cervarix has shown a high level of protection against HPV-16/18 infections and associated cervical lesions.This phase Ⅰ trial (NCT00549900) assessed the safety,tolerability,and immunogenicity of the vaccine in Chinese.Thirty healthy Chinese females,aged 15 to 45 years with a median age of 29.5 years,received three doses of Cervarix in Months 0,1,and 6.Safety was assessed via recording solicited local and systemic symptoms within 7 days and unsolicited symptoms within 30 days after each vaccination.Serious adverse events,new onset of chronic diseases,and other medically significant conditions were recorded throughout this trial.As an exploratory objective,HPV-16/18 antibody titers were determined by enzyme-linked immunosorbent assay in serum samples collected in Months 0 and 7.Pain at the injection site was the most frequently reported local symptom.Two subjects reported medically significant adverse events.Both cases were assessed as unrelated to vaccination by the investigator.In Month 7,100% seroconversion was observed for both anti-HPV-16 and anti-HPV-18 with high geometric mean antibody titers.HPV-16/18 AS04-adjuvanted vaccine,evaluated for the first time in Chinese females,was generally well tolerated and immunogenic,as previously shown in global studies.展开更多
The effect of trace amount of active element Si on the wetting and interface characteristics of 1Cr18Ni11Nb/TiO was investigated. Based on the results, a new binder phase for TiO based cermets imitated gold materials ...The effect of trace amount of active element Si on the wetting and interface characteristics of 1Cr18Ni11Nb/TiO was investigated. Based on the results, a new binder phase for TiO based cermets imitated gold materials was developed, and the related mechanisms were studied. The results indicated that there was small wet-ability of the 1Cr18Ni11Nb alloy on TiO, and the interface binding strength of 1Cr18Ni11Nb/TiO was low. 1.5%Si in 1Cr18Ni11Nb could not only make the alloy wet TiO, but also lead to mutual dissolving near the interface, forming high interface binding strength and matching with the thermal expansion coefficient of TiO.展开更多
为了满足对电网谐波治理的要求,提出了一种新颖的双18脉波整流器拓扑结构。首先介绍了其工作原理,然后分析了相移变压器的功能以及消谐原理,推导出进线电源中电流的解析表达式,最后对这种新型的拓扑结构进行了仿真和实验研究。仿真和实...为了满足对电网谐波治理的要求,提出了一种新颖的双18脉波整流器拓扑结构。首先介绍了其工作原理,然后分析了相移变压器的功能以及消谐原理,推导出进线电源中电流的解析表达式,最后对这种新型的拓扑结构进行了仿真和实验研究。仿真和实验的结果表明,这种双18脉冲整流器不仅能实现36脉波整流的效果,使其满足IEEE Standard 519-1992标准的要求,而且该拓扑结构还可以消除由于制造等原因而造成相移角误差所引起的残留在单个相移变压器中的第5、7等低次谐波。该拓扑结构具有优良的工作性能和良好的工业应用前景。展开更多
The synergistic effect is investigated in mixed gas chromatographic stationary phase containing dibenzo-18-crown-6 and resorcarene derivative, with benzene/cyclohexane, halogenated hydrocarbon, aromatics, ketone, phen...The synergistic effect is investigated in mixed gas chromatographic stationary phase containing dibenzo-18-crown-6 and resorcarene derivative, with benzene/cyclohexane, halogenated hydrocarbon, aromatics, ketone, phenol, alcohol and aniline derivatives as the sample compound pairs. This separation effect is affected by temperature, mixing ratio of stationary phases and linear velocity of carrier gas.展开更多
基金supported by Chongqing Talent Plan:Leading Talents in Innovation and Entrepreneurship,China(No.CQYC201903051)University Innovation Research Group of Chongqing,China(No.CXQT20023)+4 种基金Qingnian Project of Science and Technology Research Program of Chongqing Municipal Education Commission,China(No.KJQN202001106)China Postdoctoral Science Foundation(No.2021M700556)Natural Science Foundation of Chongqing,China(No.cstc2021jcyj-bsh X0114)Natural Science Foundation of China(Nos.U20A20234,51874062)Chongqing Foundation and Advanced Research Project,China(No.cstc2019jcyj-zdxm X0010)。
基金Funded by the National Natural Science Foundation of China(No.52075058)the Natural Science Foundation of Chongqing(No.cstc2021jcyj-msxmX1112)the Research and Demonstration of Key Technologies for Forging High-performance Aluminum Alloys for Aerospace Applications(No.Z20210348)。
文摘An accurate flow stress model was established by considering the parameters of strain rate,strain and temperature as well asβ→a+βphase transformation in order to develop the plastic forming theory of TC18 titanium alloy.Firstly,the phase transition kinetics of TC18 titanium alloy during isothermal and continuous cooling at 1073 and 1273 K was studied by thermodynamic calculation,meanwhile,the relationship of volume fraction of phase transition with temperature and time was obtained.Constitutive models were calculated by investigating flow behaviors under hot compression tests with the strain rates of 0.001-1s^(-1) and temperatures of 973-1223 K in the singleβand a+βregions in TC18 titanium alloy,respectively.By combining the phase transformation dynamic kinetics with constitutive models,an accurate flow stress model was established,providing theoretical basis and data support for the hot forging of TC18 titanium alloy.
基金Project(BK20160869)supported by the Natural Science Foundation of Jiangsu Province,ChinaProject(GY12015009)supported by the Nantong Science and Technology Program,China+1 种基金Project(2015B01314)supported by the Fundamental Research Funds for the Central Universities,ChinaProject(51501039)supported by the National Natural Science Foundation of China
文摘The microstructural evolution of a 18R single phase （S 18） alloy during annealing at 773 K for 100 h was investigated in order to reveal the formation mechanism of 14H phase. The results showed that the as-cast S 18 alloy was composed of 18R phase （its volume fraction exceeds 93%）, W particles and α-Mg phase. The 18R phase in S18 alloy was thermally stable and was not transformed into 14H long period stacking ordered （LPSO） phase during annealing. However, 14H lamellas formed within tiny α-Mg slices, and their average size and volume fraction increased with prolonging annealing time. Moreover, the 14H phase is nucleated within α-Mg independently on the basis of basal stacking faults （SFs）. The broadening growth of 14H lamellas is an interface-controlled process which involves ledges on basal planes, while the lengthening growth is a diffusion-controlled process and is associated with diffusion of solute atoms. The formation mechanism of 14H phase in this alloy could be explained as α-Mg＇→α-Mg＋14H.
文摘A series of single bcc,bcc plus fcc duplex and single fcc microcrystalline coatings of 1Cr18Ni9Ti stainless steel were prepared by using sputtering technique.The resistance against pitting corrosion was studied by measurements of pitting corrosion potentials and electrochemical noise during initiation of corrosion pits.The results show that the sputtered coatings with single bcc phase or single fcc structure are more resistant to pitting corrosion than those with bcc plus fcc duplex phase structure.
文摘used－silical capillary columns containing heptakis（2、3、6－tri－o－pentyl）-β-cyclodextrinand dibenzo-18-crown-6 were prepared．By studying the selectivity of mixed stationary phases forsome solute pairs.as well as comparing with the heptakis（2．3、6-tri-O-pentyl）-β-cyclodextrin and thedibenzo-18-crown-6 used as individual stationary phase、the synergistic effects were observed.These effects were affected by the column temperature．mixed ratio and linear velocity of carrier gas．
文摘Globally,about 70% of cervical cancers are associated with human papillomavirus (HPV)-16 or HPV-18 infection.A meta-analysis of epidemiologic studies in China showed that HPV was present in 98% of cervical cancer samples.The HPV-16/18 AS04-adjuvanted vaccine Cervarix has shown a high level of protection against HPV-16/18 infections and associated cervical lesions.This phase Ⅰ trial (NCT00549900) assessed the safety,tolerability,and immunogenicity of the vaccine in Chinese.Thirty healthy Chinese females,aged 15 to 45 years with a median age of 29.5 years,received three doses of Cervarix in Months 0,1,and 6.Safety was assessed via recording solicited local and systemic symptoms within 7 days and unsolicited symptoms within 30 days after each vaccination.Serious adverse events,new onset of chronic diseases,and other medically significant conditions were recorded throughout this trial.As an exploratory objective,HPV-16/18 antibody titers were determined by enzyme-linked immunosorbent assay in serum samples collected in Months 0 and 7.Pain at the injection site was the most frequently reported local symptom.Two subjects reported medically significant adverse events.Both cases were assessed as unrelated to vaccination by the investigator.In Month 7,100% seroconversion was observed for both anti-HPV-16 and anti-HPV-18 with high geometric mean antibody titers.HPV-16/18 AS04-adjuvanted vaccine,evaluated for the first time in Chinese females,was generally well tolerated and immunogenic,as previously shown in global studies.
文摘The effect of trace amount of active element Si on the wetting and interface characteristics of 1Cr18Ni11Nb/TiO was investigated. Based on the results, a new binder phase for TiO based cermets imitated gold materials was developed, and the related mechanisms were studied. The results indicated that there was small wet-ability of the 1Cr18Ni11Nb alloy on TiO, and the interface binding strength of 1Cr18Ni11Nb/TiO was low. 1.5%Si in 1Cr18Ni11Nb could not only make the alloy wet TiO, but also lead to mutual dissolving near the interface, forming high interface binding strength and matching with the thermal expansion coefficient of TiO.
文摘为了满足对电网谐波治理的要求,提出了一种新颖的双18脉波整流器拓扑结构。首先介绍了其工作原理,然后分析了相移变压器的功能以及消谐原理,推导出进线电源中电流的解析表达式,最后对这种新型的拓扑结构进行了仿真和实验研究。仿真和实验的结果表明,这种双18脉冲整流器不仅能实现36脉波整流的效果,使其满足IEEE Standard 519-1992标准的要求,而且该拓扑结构还可以消除由于制造等原因而造成相移角误差所引起的残留在单个相移变压器中的第5、7等低次谐波。该拓扑结构具有优良的工作性能和良好的工业应用前景。
文摘The synergistic effect is investigated in mixed gas chromatographic stationary phase containing dibenzo-18-crown-6 and resorcarene derivative, with benzene/cyclohexane, halogenated hydrocarbon, aromatics, ketone, phenol, alcohol and aniline derivatives as the sample compound pairs. This separation effect is affected by temperature, mixing ratio of stationary phases and linear velocity of carrier gas.
