3D eikonal equation is a partial differential equation for the calculation of first-arrival traveltimes and has been widely applied in many scopes such as ray tracing,source localization,reflection migration,seismic m...3D eikonal equation is a partial differential equation for the calculation of first-arrival traveltimes and has been widely applied in many scopes such as ray tracing,source localization,reflection migration,seismic monitoring and tomographic imaging.In recent years,many advanced methods have been developed to solve the 3D eikonal equation in heterogeneous media.However,there are still challenges for the stable and accurate calculation of first-arrival traveltimes in 3D strongly inhomogeneous media.In this paper,we propose an adaptive finite-difference(AFD)method to numerically solve the 3D eikonal equation.The novel method makes full use of the advantages of different local operators characterizing different seismic wave types to calculate factors and traveltimes,and then the most accurate factor and traveltime are adaptively selected for the convergent updating based on the Fermat principle.Combined with global fast sweeping describing seismic waves propagating along eight directions in 3D media,our novel method can achieve the robust calculation of first-arrival traveltimes with high precision at grid points either near source point or far away from source point even in a velocity model with large and sharp contrasts.Several numerical examples show the good performance of the AFD method,which will be beneficial to many scientific applications.展开更多
This work develops a Hermitian C^(2) differential reproducing kernel interpolation meshless(DRKIM)method within the consistent couple stress theory(CCST)framework to study the three-dimensional(3D)microstructuredepend...This work develops a Hermitian C^(2) differential reproducing kernel interpolation meshless(DRKIM)method within the consistent couple stress theory(CCST)framework to study the three-dimensional(3D)microstructuredependent static flexural behavior of a functionally graded(FG)microplate subjected to mechanical loads and placed under full simple supports.In the formulation,we select the transverse stress and displacement components and their first-and second-order derivatives as primary variables.Then,we set up the differential reproducing conditions(DRCs)to obtain the shape functions of the Hermitian C^(2) differential reproducing kernel(DRK)interpolant’s derivatives without using direct differentiation.The interpolant’s shape function is combined with a primitive function that possesses Kronecker delta properties and an enrichment function that constituents DRCs.As a result,the primary variables and their first-and second-order derivatives satisfy the nodal interpolation properties.Subsequently,incorporating ourHermitianC^(2)DRKinterpolant intothe strong formof the3DCCST,we develop a DRKIM method to analyze the FG microplate’s 3D microstructure-dependent static flexural behavior.The Hermitian C^(2) DRKIM method is confirmed to be accurate and fast in its convergence rate by comparing the solutions it produces with the relevant 3D solutions available in the literature.Finally,the impact of essential factors on the transverse stresses,in-plane stresses,displacements,and couple stresses that are induced in the loaded microplate is examined.These factors include the length-to-thickness ratio,the material length-scale parameter,and the inhomogeneity index,which appear to be significant.展开更多
目的探讨(1-3)-β-D葡聚糖联合降钙素原(procalcitonin,PCT)、CD4^(+)T淋巴细胞多指标在艾滋病患者马尔尼菲篮状菌感染早期诊断临床研究。方法回顾性选取我院2020年1月—2022年6月住院的120例艾滋病患者为研究对象。依据实验室结果,将...目的探讨(1-3)-β-D葡聚糖联合降钙素原(procalcitonin,PCT)、CD4^(+)T淋巴细胞多指标在艾滋病患者马尔尼菲篮状菌感染早期诊断临床研究。方法回顾性选取我院2020年1月—2022年6月住院的120例艾滋病患者为研究对象。依据实验室结果,将其分为马尔尼菲篮状菌感染确诊组(血或组织液培育养出马尔尼菲篮状菌),简称A组(62例),及马尔尼菲篮状菌感染临床诊断组[根据临床症状、体征、血常规及(1-3)-β-D葡聚糖、PCT、CD4^(+)T淋巴细胞多指标诊断],简称B组(58例)。检测患者(1-3)-β-D葡聚糖、PCT、CD4^(+)T淋巴细胞的表达水平,采用受试者工作特征(receiver-operating characteristic,ROC)曲线下面积(area under the curve,AUC)评估上述指标联合检测对艾滋病患者感染马尔尼菲篮状菌的诊断效能。结果A组的(1-3)-β-D葡聚糖和PCT水平均高于B组,CD4^(+)T淋巴细胞个数低于B组(P<0.05);(1-3)-β-D葡聚糖、PCT、CD4^(+)T淋巴细胞联合检测的AUC为0.933,(1-3)-β-D葡聚糖单独检测的AUC是0.812,PCT单独检测的AUC为0.883,CD4^(+)T淋巴细胞单独检测的AUC是0.810,(1-3)-β-D葡聚糖、PCT和CD4^(+)T淋巴细胞联合检测的AUC皆优于三项单独检测,表明(1-3)-β-D葡聚糖、PCT和CD4^(+)T淋巴细胞联合检测的诊断价值皆优于单一指标诊断,且联合检测的特异度、约登指数分别为92.43%和0.580,均高于三项单独检测。结论(1-3)-β-D葡聚糖联合PCT和CD4^(+)T淋巴细胞多指标对艾滋病马尔尼菲篮状菌感染具有非常高的临床诊断价值,能够帮助医生分析出高危风险患者,及时制定治疗方案,同时也承担预后效果的判断依据,对治疗艾滋病马尔尼菲篮状菌感染具有非常重要的研究价值。展开更多
Most of local feature descriptors assume that the scene is planar. In the real scene, the captured images come from the 3-D world. 3-D corner as a novel invariant feature is important for the image matching and the ob...Most of local feature descriptors assume that the scene is planar. In the real scene, the captured images come from the 3-D world. 3-D corner as a novel invariant feature is important for the image matching and the object detection, while automatically discriminating 3-D corners from ordinary corners is difficult. A novel method for 3-D corner detection is proposed based on the image graph grammar, and it can detect the 3-D features of corners to some extent. Experimental results show that the method is valid and the 3-D corner is useful for image matching.展开更多
3-D geological modeling plays an increasingly important role in Petroleum Geology, Mining Geology and Engineering Geology. The complexity of geological conditions requires different modeling methods in different situa...3-D geological modeling plays an increasingly important role in Petroleum Geology, Mining Geology and Engineering Geology. The complexity of geological conditions requires different modeling methods in different situations. This paper summarizes the general concept of geological modeling; compares the characteristics of borehole-based modeling, cross-section based modeling and multi- source interactive modeling; analyses key techniques in 3-D geological modeling; and highlights the main difficulties and directions of future studies.展开更多
A 3-D digital core describes the pore space microstructure of rocks. An X-ray micro CT scan is the most accurate and direct but costly method to obtain a 3-D digital core. In this study, we propose a hybrid method whi...A 3-D digital core describes the pore space microstructure of rocks. An X-ray micro CT scan is the most accurate and direct but costly method to obtain a 3-D digital core. In this study, we propose a hybrid method which combines sedimentation simulation and simulated annealing (SA) method to generate 3-D digital cores based on 2-D images of rocks. The method starts with the sedimentation simulation to build a 3-D digital core, which is the initial configuration for the SA method. We update the initial digital core using the SA method to match the auto-correlation function of the 2-D rock image and eventually build the final 3-D digital core. Compared with the typical SA method, the hybrid method has significantly reduced the computation time. Local porosity theory is applied to quantitatively compare the reconstructed 3-D digital cores with the X-ray micro CT 3-D images. The results indicate that the 3-D digital cores reconstructed by the hybrid method have homogeneity and geometric connectivity similar to those of the X-ray micro CT image. The formation factors and permeabilities of the reconstructed 3-D digital cores are estimated using the finite element method (FEM) and lattice Boltzmann method (LBM), respectively. The simulated results are in good agreement with the experimental measurements. Comparison of the simulation results suggests that the digital cores reconstructed by the hybrid method more closely reflect the true transport properties than the typical SA method alone.展开更多
Nanocrystal of upconversion (UC) phosphor Ho^3+, Tm^3+ , and Yb^3+ co-doped NaYF4 was prepared by the hydrothermal method in the presence of the complexing agent EDTA. Under 980 nm diode laser excitation, the imp...Nanocrystal of upconversion (UC) phosphor Ho^3+, Tm^3+ , and Yb^3+ co-doped NaYF4 was prepared by the hydrothermal method in the presence of the complexing agent EDTA. Under 980 nm diode laser excitation, the impact of different concentrations of Ho^3+ ion on the UC luminescence intensity was discussed. The law of luminescence intensity versus pump power shows that the 474 nm blue emission, 538 nm green emission, and 642 nm red emission are all due to the two-photon process, while the 450 nm blue emission is a three-photon process. The UC mechanism and processes were also analyzed. The sample was characterized by transmission electron microscopy (TEM) and X-ray diffraction (XRD). The result shows that Ho^3+ ,Tm^3+ , and Yb^3+ co-doped NaYF4 prepared by the hydrothermal method exhibits a hexagonal nanocrystal.展开更多
3-D rigid visco-plastic finite element method (FEM) is used in the analysisof metal forming processes, including strip and plate rolling, shape rolling, slab edging, specialstrip rolling. The shifted incomplete Choles...3-D rigid visco-plastic finite element method (FEM) is used in the analysisof metal forming processes, including strip and plate rolling, shape rolling, slab edging, specialstrip rolling. The shifted incomplete Cholesky decomposition of the stiffness matrix with thesolution of the equations for velocity increment by the conjugate gradient method is combined. Thistechnique, termed the shifted ICCG method, is then employed to solve the slab edging problem. Theperformance of this algorithm in terms of the number of iterations, friction variation, shiftedparameter psi and the results of simulation for processing parameters are analysed. Numerical testsand application of this technique verify the efficiency and stability of the shifted ICCG method inthe analysis of slab edging.展开更多
NaTaONcatalysts were synthesized by a hydrothermal(H) and a solid-state(S) methods in this study.The H-and S-NaTaONsamples were characterized by X-ray diffraction(XRD), scanning electron microscopy(SEM), trans...NaTaONcatalysts were synthesized by a hydrothermal(H) and a solid-state(S) methods in this study.The H-and S-NaTaONsamples were characterized by X-ray diffraction(XRD), scanning electron microscopy(SEM), transmission electron microscopy(TEM), UV–visible(UV–vis) diffuse reflectance spectroscopy, and photoluminescence(PL) spectroscopy. The XRD patterns of the H-and S-samples showed peaks indexed to the pure phase of perovskite NaTaOand minor peaks assignable to TaNat various synthesis temperatures. Substitution of oxygen by nitrogen ions causes the light absorption of the H-and S-NaTaONsamples to be extended to the 600–650 nm region, thus making the samples visible-light active. The NaTaONsamples exhibited photocatalytic activity for Hand Oevolution from aqueous methanol and silver nitrate solutions under visible-light irradiation. The UV–vis and PL spectra of the Hand S-catalysts revealed the presence of cationic vacancies and reduced metallic species, which acted as recombination centers. These results demonstrated that the preparation method plays a critical role in the formation of defect states, thereby governing the photocatalytic activity of the NaTaONcatalysts.展开更多
Equivalent staggered-grid(ESG) as a new family of schemes has been utilized in seismic modeling,imaging,and inversion.Traditionally,the Taylor series expansion is often applied to calculate finite-difference(FD) coeff...Equivalent staggered-grid(ESG) as a new family of schemes has been utilized in seismic modeling,imaging,and inversion.Traditionally,the Taylor series expansion is often applied to calculate finite-difference(FD) coefficients on spatial derivatives,but the simulation results suffer serious numerical dispersion on a large frequency zone.We develop an optimized equivalent staggered-grid(OESG) FD method that can simultaneously suppress temporal and spatial dispersion for solving the second-order system of the 3 D elastic wave equation.On the one hand,we consider the coupling relations between wave speeds and spatial derivatives in the elastic wave equation and give three sets of FD coefficients with respect to the P-wave,S-wave,and converted-wave(C-wave) terms.On the other hand,a novel plane wave solution for the 3 D elastic wave equation is derived from the matrix decomposition method to construct the time-space dispersion relations.FD coefficients of the OESG method can be acquired by solving the new dispersion equations based on the Newton iteration method.Finally,we construct a new objective function to analyze P-wave,S-wave,and C-wave dispersion concerning frequencies.The dispersion analyses show that the presented method produces less modeling errors than the traditional ESG method.The synthetic examples demonstrate the effectiveness and superiority of the presented method.展开更多
The technique of phase measuring profilometry using a single phase step method is proposed.This method can automatically obtain phase value at each pixel by using a discret cosine transform algorithm.The method is abl...The technique of phase measuring profilometry using a single phase step method is proposed.This method can automatically obtain phase value at each pixel by using a discret cosine transform algorithm.The method is able to automatically recognize any position between depression and elevation on an object surface.Theoretical analysis and experimental verification are presented.展开更多
Lie group analysis method is applied to the extended(3+1)-dimensional Kadomtsev–Petviashvili–Boussinesq equation and the corresponding similarity reduction equations are obtained with various infinitesimal generator...Lie group analysis method is applied to the extended(3+1)-dimensional Kadomtsev–Petviashvili–Boussinesq equation and the corresponding similarity reduction equations are obtained with various infinitesimal generators.By selecting suitable arbitrary functions in the similarity reduction solutions,we obtain abundant invariant solutions,including the trigonometric solution,the kink-lump interaction solution,the interaction solution between lump wave and triangular periodic wave,the two-kink solution,the lump solution,the interaction between a lump and two-kink and the periodic lump solution in different planes.These exact solutions are also given graphically to show the detailed structures of this high dimensional integrable system.展开更多
yb3+/Dy3+ co-doped A1203 nanopowders have been prepared by the non-aqueous sol-gel method and their up- conversion photoluminescence spectra are measured under excitation by a 980-nm semiconductor laser. The results...yb3+/Dy3+ co-doped A1203 nanopowders have been prepared by the non-aqueous sol-gel method and their up- conversion photoluminescence spectra are measured under excitation by a 980-nm semiconductor laser. The results show that there are comparatively abundant spectra of up-conversion emissions centered at 378, 408, 527 and 543, and 663 nm, corresponding to 4C9/2→ 6H13/2, 4C9/2→ 6Hll/2, 4115/2 → 6H13/2, and 4F9/2 →6Hll/2 transitions of Dy3+, respectively. Two-photon and three-photon processes are involved in ultraviolet, violet, green, and red up-conversion emissions. The energy transition between Yb3+ and Dy3+ is discussed.展开更多
A generalized variable-coefficient algebraic method is appfied to construct several new families of exact solutions of physical interest for (3+1)-dimensional Kadomtsev-Petviashvilli (KP) equation. Among them, th...A generalized variable-coefficient algebraic method is appfied to construct several new families of exact solutions of physical interest for (3+1)-dimensional Kadomtsev-Petviashvilli (KP) equation. Among them, the Jacobi elliptic periodic solutions exactly degenerate to the soliton solutions at a certain limit condition. Compared with the existing tanh method, the extended tanh method, the Jacobi elliptic function method, and the algebraic method, the proposed method gives new and more general solutions.展开更多
To achieve full-surface strain measurement of variable curvature objects,a 360°3D digital image correlation(DIC)system is proposed.The measurement system consists of four double-camera systems,which capture the o...To achieve full-surface strain measurement of variable curvature objects,a 360°3D digital image correlation(DIC)system is proposed.The measurement system consists of four double-camera systems,which capture the object’s entire surface from multiple angles,enabling comprehensive full-surface measurement.To increase the stitching quality,a hierarchical coordinate matching method is proposed.Initially,a 3D rigid body calibration auxiliary block is employed to track motion trajectory,which enables preliminary matching of four 3D-DIC sub-systems.Subsequently,secondary precise matching is performed based on feature points on the test specimen’s surface.Through the hierarchical coordinate matching method,the local 3D coordinate systems of each double-camera system are unified into a global coordinate system,achieving 3D surface reconstruction of the variable curvature cylindrical shell,and error analysis is conducted on the results.Furthermore,axial compression buckling experiment is conducted to measure the displacement and strain fields on the cylindrical shell’s surface.The experimental results are compared with the finite element analysis,validating the accuracy and effectiveness of the proposed multi-camera 3D-DIC measuring system.展开更多
Y2O3:Eu3+ phosphors co-doped with different metal cations (Li+, Na+, K+, Mg2+, Ca2+) are prepared by the gel- combustion method with Y2O3:Eu3+, and R(NO3)x (R = Li, Na, K, Mg, Ca) serving as raw materi...Y2O3:Eu3+ phosphors co-doped with different metal cations (Li+, Na+, K+, Mg2+, Ca2+) are prepared by the gel- combustion method with Y2O3:Eu3+, and R(NO3)x (R = Li, Na, K, Mg, Ca) serving as raw materials and glycine as fuel, calcined at 1000 ℃ for 2 h. The synthesized Y203 :Eu3+ phosphors doped with different metal cations and doping ratios are characterized by x-ray diffractometry (XRD), fluorescence and phosphorescent spectrophotometer. The co-doping metal cations are advantageous to the development of Y203:Eu3+ lattice. All the samples can emit red light peaked at 611 nm under 254-nm excited. The luminescence intensities of co-doping samples are increased because the cations increase the electron transition probability of Eu3+ from 5D0 level to 7F level. The fluorescence lifetime of Eu3+ (SD0 --+7F2) is increased by doping metal cations.展开更多
La-doped and undoped xBiIn03-(1 - x)PbTi03 (BI-PT) thin films are deposited on (101)SrRuO3/(lOO)Pt/(lO0) MgO substrates by the rf-magnetron sputtering method. The structures of the films are characterized by...La-doped and undoped xBiIn03-(1 - x)PbTi03 (BI-PT) thin films are deposited on (101)SrRuO3/(lOO)Pt/(lO0) MgO substrates by the rf-magnetron sputtering method. The structures of the films are characterized by XRD and SEM, and the results indicate that the thin films are grown with mainly (100) oriented and columnar structures. The ferroelectricity and piezoelectricity of the BI-PT films are also measured, and the measured results illustrate that both performances are effectively improved by the La-doping with suitable concentrations. These results will open up wide potential applications of the films in electronic devices.展开更多
Fe-based carbon materials are widely considered promising to replace Pt/C as next-generation electrocatalysts towards oxygen reduction reaction (ORR). However, the preparation of Fe-based carbon materials is still car...Fe-based carbon materials are widely considered promising to replace Pt/C as next-generation electrocatalysts towards oxygen reduction reaction (ORR). However, the preparation of Fe-based carbon materials is still carried out by conventional heating method (CHM). Herein, a novel microwave-assisted carbon bath method (MW-CBM) was proposed, which only took 35 min to synthesize Fe/Fe3C nanoparticles encapsulated in N-doped carbon layers derived from Prussian blue (PB). The catalyst contained large specific surface area and mesoporous structure, abundant Fe-Nx and C–N active sites, unique core-shell structure. Due to the synergistic effects of these features, the as-prepared Fe/Fe3C@NC-2 displayed outstanding ORR activity with onset potential of 0.98 VRHE and halfwave potential of 0.87 VRHE, which were more positive than 20 wt.% Pt/C (0.93 VRHE and 0.82 VRHE). Besides, Fe/Fe3C@NC-2 gave a better stability and methanol tolerance than Pt/C towards ORR in alkaline media, too.展开更多
基金The authors thank the funds supported by the China National Nuclear Corporation under Grants Nos.WUQNYC2101 and WUHTLM2101-04National Natural Science Foundation of China(42074132,42274154).
文摘3D eikonal equation is a partial differential equation for the calculation of first-arrival traveltimes and has been widely applied in many scopes such as ray tracing,source localization,reflection migration,seismic monitoring and tomographic imaging.In recent years,many advanced methods have been developed to solve the 3D eikonal equation in heterogeneous media.However,there are still challenges for the stable and accurate calculation of first-arrival traveltimes in 3D strongly inhomogeneous media.In this paper,we propose an adaptive finite-difference(AFD)method to numerically solve the 3D eikonal equation.The novel method makes full use of the advantages of different local operators characterizing different seismic wave types to calculate factors and traveltimes,and then the most accurate factor and traveltime are adaptively selected for the convergent updating based on the Fermat principle.Combined with global fast sweeping describing seismic waves propagating along eight directions in 3D media,our novel method can achieve the robust calculation of first-arrival traveltimes with high precision at grid points either near source point or far away from source point even in a velocity model with large and sharp contrasts.Several numerical examples show the good performance of the AFD method,which will be beneficial to many scientific applications.
基金supported by a grant from the National Science and Technology Council of the Republic of China(Grant Number:MOST 112-2221-E-006-048-MY2).
文摘This work develops a Hermitian C^(2) differential reproducing kernel interpolation meshless(DRKIM)method within the consistent couple stress theory(CCST)framework to study the three-dimensional(3D)microstructuredependent static flexural behavior of a functionally graded(FG)microplate subjected to mechanical loads and placed under full simple supports.In the formulation,we select the transverse stress and displacement components and their first-and second-order derivatives as primary variables.Then,we set up the differential reproducing conditions(DRCs)to obtain the shape functions of the Hermitian C^(2) differential reproducing kernel(DRK)interpolant’s derivatives without using direct differentiation.The interpolant’s shape function is combined with a primitive function that possesses Kronecker delta properties and an enrichment function that constituents DRCs.As a result,the primary variables and their first-and second-order derivatives satisfy the nodal interpolation properties.Subsequently,incorporating ourHermitianC^(2)DRKinterpolant intothe strong formof the3DCCST,we develop a DRKIM method to analyze the FG microplate’s 3D microstructure-dependent static flexural behavior.The Hermitian C^(2) DRKIM method is confirmed to be accurate and fast in its convergence rate by comparing the solutions it produces with the relevant 3D solutions available in the literature.Finally,the impact of essential factors on the transverse stresses,in-plane stresses,displacements,and couple stresses that are induced in the loaded microplate is examined.These factors include the length-to-thickness ratio,the material length-scale parameter,and the inhomogeneity index,which appear to be significant.
文摘目的探讨(1-3)-β-D葡聚糖联合降钙素原(procalcitonin,PCT)、CD4^(+)T淋巴细胞多指标在艾滋病患者马尔尼菲篮状菌感染早期诊断临床研究。方法回顾性选取我院2020年1月—2022年6月住院的120例艾滋病患者为研究对象。依据实验室结果,将其分为马尔尼菲篮状菌感染确诊组(血或组织液培育养出马尔尼菲篮状菌),简称A组(62例),及马尔尼菲篮状菌感染临床诊断组[根据临床症状、体征、血常规及(1-3)-β-D葡聚糖、PCT、CD4^(+)T淋巴细胞多指标诊断],简称B组(58例)。检测患者(1-3)-β-D葡聚糖、PCT、CD4^(+)T淋巴细胞的表达水平,采用受试者工作特征(receiver-operating characteristic,ROC)曲线下面积(area under the curve,AUC)评估上述指标联合检测对艾滋病患者感染马尔尼菲篮状菌的诊断效能。结果A组的(1-3)-β-D葡聚糖和PCT水平均高于B组,CD4^(+)T淋巴细胞个数低于B组(P<0.05);(1-3)-β-D葡聚糖、PCT、CD4^(+)T淋巴细胞联合检测的AUC为0.933,(1-3)-β-D葡聚糖单独检测的AUC是0.812,PCT单独检测的AUC为0.883,CD4^(+)T淋巴细胞单独检测的AUC是0.810,(1-3)-β-D葡聚糖、PCT和CD4^(+)T淋巴细胞联合检测的AUC皆优于三项单独检测,表明(1-3)-β-D葡聚糖、PCT和CD4^(+)T淋巴细胞联合检测的诊断价值皆优于单一指标诊断,且联合检测的特异度、约登指数分别为92.43%和0.580,均高于三项单独检测。结论(1-3)-β-D葡聚糖联合PCT和CD4^(+)T淋巴细胞多指标对艾滋病马尔尼菲篮状菌感染具有非常高的临床诊断价值,能够帮助医生分析出高危风险患者,及时制定治疗方案,同时也承担预后效果的判断依据,对治疗艾滋病马尔尼菲篮状菌感染具有非常重要的研究价值。
文摘Most of local feature descriptors assume that the scene is planar. In the real scene, the captured images come from the 3-D world. 3-D corner as a novel invariant feature is important for the image matching and the object detection, while automatically discriminating 3-D corners from ordinary corners is difficult. A novel method for 3-D corner detection is proposed based on the image graph grammar, and it can detect the 3-D features of corners to some extent. Experimental results show that the method is valid and the 3-D corner is useful for image matching.
文摘3-D geological modeling plays an increasingly important role in Petroleum Geology, Mining Geology and Engineering Geology. The complexity of geological conditions requires different modeling methods in different situations. This paper summarizes the general concept of geological modeling; compares the characteristics of borehole-based modeling, cross-section based modeling and multi- source interactive modeling; analyses key techniques in 3-D geological modeling; and highlights the main difficulties and directions of future studies.
基金sponsored by NSFC(Grant No.40574030)CNPC Research Project(Grant No.06A30102)
文摘A 3-D digital core describes the pore space microstructure of rocks. An X-ray micro CT scan is the most accurate and direct but costly method to obtain a 3-D digital core. In this study, we propose a hybrid method which combines sedimentation simulation and simulated annealing (SA) method to generate 3-D digital cores based on 2-D images of rocks. The method starts with the sedimentation simulation to build a 3-D digital core, which is the initial configuration for the SA method. We update the initial digital core using the SA method to match the auto-correlation function of the 2-D rock image and eventually build the final 3-D digital core. Compared with the typical SA method, the hybrid method has significantly reduced the computation time. Local porosity theory is applied to quantitatively compare the reconstructed 3-D digital cores with the X-ray micro CT 3-D images. The results indicate that the 3-D digital cores reconstructed by the hybrid method have homogeneity and geometric connectivity similar to those of the X-ray micro CT image. The formation factors and permeabilities of the reconstructed 3-D digital cores are estimated using the finite element method (FEM) and lattice Boltzmann method (LBM), respectively. The simulated results are in good agreement with the experimental measurements. Comparison of the simulation results suggests that the digital cores reconstructed by the hybrid method more closely reflect the true transport properties than the typical SA method alone.
基金Project supported bythe Key Laboratory of Rare Earth Chemistry and Physics ,ChangchunInstitute of Applied Chemistry ,Chinese Academy of Sciences (R020202K)
文摘Nanocrystal of upconversion (UC) phosphor Ho^3+, Tm^3+ , and Yb^3+ co-doped NaYF4 was prepared by the hydrothermal method in the presence of the complexing agent EDTA. Under 980 nm diode laser excitation, the impact of different concentrations of Ho^3+ ion on the UC luminescence intensity was discussed. The law of luminescence intensity versus pump power shows that the 474 nm blue emission, 538 nm green emission, and 642 nm red emission are all due to the two-photon process, while the 450 nm blue emission is a three-photon process. The UC mechanism and processes were also analyzed. The sample was characterized by transmission electron microscopy (TEM) and X-ray diffraction (XRD). The result shows that Ho^3+ ,Tm^3+ , and Yb^3+ co-doped NaYF4 prepared by the hydrothermal method exhibits a hexagonal nanocrystal.
基金supported by Huo Yingdong Young Teachers Foundation,Ministry of State Education of ChinaNational Natural Science Foundation of China(No.59904003).
文摘3-D rigid visco-plastic finite element method (FEM) is used in the analysisof metal forming processes, including strip and plate rolling, shape rolling, slab edging, specialstrip rolling. The shifted incomplete Cholesky decomposition of the stiffness matrix with thesolution of the equations for velocity increment by the conjugate gradient method is combined. Thistechnique, termed the shifted ICCG method, is then employed to solve the slab edging problem. Theperformance of this algorithm in terms of the number of iterations, friction variation, shiftedparameter psi and the results of simulation for processing parameters are analysed. Numerical testsand application of this technique verify the efficiency and stability of the shifted ICCG method inthe analysis of slab edging.
基金the financial support from the Ministry of Science and Technology,Taiwan(MOST 104-2218-E-033-006-MY2)
文摘NaTaONcatalysts were synthesized by a hydrothermal(H) and a solid-state(S) methods in this study.The H-and S-NaTaONsamples were characterized by X-ray diffraction(XRD), scanning electron microscopy(SEM), transmission electron microscopy(TEM), UV–visible(UV–vis) diffuse reflectance spectroscopy, and photoluminescence(PL) spectroscopy. The XRD patterns of the H-and S-samples showed peaks indexed to the pure phase of perovskite NaTaOand minor peaks assignable to TaNat various synthesis temperatures. Substitution of oxygen by nitrogen ions causes the light absorption of the H-and S-NaTaONsamples to be extended to the 600–650 nm region, thus making the samples visible-light active. The NaTaONsamples exhibited photocatalytic activity for Hand Oevolution from aqueous methanol and silver nitrate solutions under visible-light irradiation. The UV–vis and PL spectra of the Hand S-catalysts revealed the presence of cationic vacancies and reduced metallic species, which acted as recombination centers. These results demonstrated that the preparation method plays a critical role in the formation of defect states, thereby governing the photocatalytic activity of the NaTaONcatalysts.
文摘Equivalent staggered-grid(ESG) as a new family of schemes has been utilized in seismic modeling,imaging,and inversion.Traditionally,the Taylor series expansion is often applied to calculate finite-difference(FD) coefficients on spatial derivatives,but the simulation results suffer serious numerical dispersion on a large frequency zone.We develop an optimized equivalent staggered-grid(OESG) FD method that can simultaneously suppress temporal and spatial dispersion for solving the second-order system of the 3 D elastic wave equation.On the one hand,we consider the coupling relations between wave speeds and spatial derivatives in the elastic wave equation and give three sets of FD coefficients with respect to the P-wave,S-wave,and converted-wave(C-wave) terms.On the other hand,a novel plane wave solution for the 3 D elastic wave equation is derived from the matrix decomposition method to construct the time-space dispersion relations.FD coefficients of the OESG method can be acquired by solving the new dispersion equations based on the Newton iteration method.Finally,we construct a new objective function to analyze P-wave,S-wave,and C-wave dispersion concerning frequencies.The dispersion analyses show that the presented method produces less modeling errors than the traditional ESG method.The synthetic examples demonstrate the effectiveness and superiority of the presented method.
文摘The technique of phase measuring profilometry using a single phase step method is proposed.This method can automatically obtain phase value at each pixel by using a discret cosine transform algorithm.The method is able to automatically recognize any position between depression and elevation on an object surface.Theoretical analysis and experimental verification are presented.
文摘Lie group analysis method is applied to the extended(3+1)-dimensional Kadomtsev–Petviashvili–Boussinesq equation and the corresponding similarity reduction equations are obtained with various infinitesimal generators.By selecting suitable arbitrary functions in the similarity reduction solutions,we obtain abundant invariant solutions,including the trigonometric solution,the kink-lump interaction solution,the interaction solution between lump wave and triangular periodic wave,the two-kink solution,the lump solution,the interaction between a lump and two-kink and the periodic lump solution in different planes.These exact solutions are also given graphically to show the detailed structures of this high dimensional integrable system.
基金Project supported by the National Natural Science Foundation of China (Grant No. 11004092) and the Scientific Research Fund of Education Department of Liaoning Province, China (Grant No. 2009A417).
文摘yb3+/Dy3+ co-doped A1203 nanopowders have been prepared by the non-aqueous sol-gel method and their up- conversion photoluminescence spectra are measured under excitation by a 980-nm semiconductor laser. The results show that there are comparatively abundant spectra of up-conversion emissions centered at 378, 408, 527 and 543, and 663 nm, corresponding to 4C9/2→ 6H13/2, 4C9/2→ 6Hll/2, 4115/2 → 6H13/2, and 4F9/2 →6Hll/2 transitions of Dy3+, respectively. Two-photon and three-photon processes are involved in ultraviolet, violet, green, and red up-conversion emissions. The energy transition between Yb3+ and Dy3+ is discussed.
文摘A generalized variable-coefficient algebraic method is appfied to construct several new families of exact solutions of physical interest for (3+1)-dimensional Kadomtsev-Petviashvilli (KP) equation. Among them, the Jacobi elliptic periodic solutions exactly degenerate to the soliton solutions at a certain limit condition. Compared with the existing tanh method, the extended tanh method, the Jacobi elliptic function method, and the algebraic method, the proposed method gives new and more general solutions.
基金funded by the National Natural Science Foundations of China(Nos.12272176,U2037603).
文摘To achieve full-surface strain measurement of variable curvature objects,a 360°3D digital image correlation(DIC)system is proposed.The measurement system consists of four double-camera systems,which capture the object’s entire surface from multiple angles,enabling comprehensive full-surface measurement.To increase the stitching quality,a hierarchical coordinate matching method is proposed.Initially,a 3D rigid body calibration auxiliary block is employed to track motion trajectory,which enables preliminary matching of four 3D-DIC sub-systems.Subsequently,secondary precise matching is performed based on feature points on the test specimen’s surface.Through the hierarchical coordinate matching method,the local 3D coordinate systems of each double-camera system are unified into a global coordinate system,achieving 3D surface reconstruction of the variable curvature cylindrical shell,and error analysis is conducted on the results.Furthermore,axial compression buckling experiment is conducted to measure the displacement and strain fields on the cylindrical shell’s surface.The experimental results are compared with the finite element analysis,validating the accuracy and effectiveness of the proposed multi-camera 3D-DIC measuring system.
文摘Y2O3:Eu3+ phosphors co-doped with different metal cations (Li+, Na+, K+, Mg2+, Ca2+) are prepared by the gel- combustion method with Y2O3:Eu3+, and R(NO3)x (R = Li, Na, K, Mg, Ca) serving as raw materials and glycine as fuel, calcined at 1000 ℃ for 2 h. The synthesized Y203 :Eu3+ phosphors doped with different metal cations and doping ratios are characterized by x-ray diffractometry (XRD), fluorescence and phosphorescent spectrophotometer. The co-doping metal cations are advantageous to the development of Y203:Eu3+ lattice. All the samples can emit red light peaked at 611 nm under 254-nm excited. The luminescence intensities of co-doping samples are increased because the cations increase the electron transition probability of Eu3+ from 5D0 level to 7F level. The fluorescence lifetime of Eu3+ (SD0 --+7F2) is increased by doping metal cations.
基金Supported by the National Natural Science Foundation of China under Grant Nos 11174142 and 11304160he National Basic Research Program of China under Grant No 2012CB921504the Special Fund for Public Interest of China under Grant No201510068
文摘La-doped and undoped xBiIn03-(1 - x)PbTi03 (BI-PT) thin films are deposited on (101)SrRuO3/(lOO)Pt/(lO0) MgO substrates by the rf-magnetron sputtering method. The structures of the films are characterized by XRD and SEM, and the results indicate that the thin films are grown with mainly (100) oriented and columnar structures. The ferroelectricity and piezoelectricity of the BI-PT films are also measured, and the measured results illustrate that both performances are effectively improved by the La-doping with suitable concentrations. These results will open up wide potential applications of the films in electronic devices.
基金supported by the National Natural Science Foundation of China (U1303291)the Program for Changjiang Scholars and Innovative Research Team in University (No. IRT_15R46)
文摘Fe-based carbon materials are widely considered promising to replace Pt/C as next-generation electrocatalysts towards oxygen reduction reaction (ORR). However, the preparation of Fe-based carbon materials is still carried out by conventional heating method (CHM). Herein, a novel microwave-assisted carbon bath method (MW-CBM) was proposed, which only took 35 min to synthesize Fe/Fe3C nanoparticles encapsulated in N-doped carbon layers derived from Prussian blue (PB). The catalyst contained large specific surface area and mesoporous structure, abundant Fe-Nx and C–N active sites, unique core-shell structure. Due to the synergistic effects of these features, the as-prepared Fe/Fe3C@NC-2 displayed outstanding ORR activity with onset potential of 0.98 VRHE and halfwave potential of 0.87 VRHE, which were more positive than 20 wt.% Pt/C (0.93 VRHE and 0.82 VRHE). Besides, Fe/Fe3C@NC-2 gave a better stability and methanol tolerance than Pt/C towards ORR in alkaline media, too.