The fatigue behavior of a high strength steel 300 M in the gigacycle regime was investigated. Fully reversed tension - compression fatigue tests at ambient temperature were performed using an ultrasonic fatigue system...The fatigue behavior of a high strength steel 300 M in the gigacycle regime was investigated. Fully reversed tension - compression fatigue tests at ambient temperature were performed using an ultrasonic fatigue system operating at 20 kHz.The staircase test method was employed to obtain accurate values of the mean fatigue strength corresponding to fixed numbers of cycles up to 10~9.These results were compared to the curve which is estimated by the data tested in the mid-long life regime on conventional servo hydraulic test machine at 20 Hz.Results indicate that the fatigue strength determined from ultrasonic fatigue testing is lightly higher than conventional testing in the range of 10~6-10~7 cycles.It is obvious that nucleations of fractures tend to occur below the surface, if fractures happen after more than 10~7 cycles.All the fractured specimens fails from internal SiO_2 inclusions or smaller carbides and carbide clusters.展开更多
The microstructure models were integrated into finite element(FE)code,and a three-dimensional(3D)FE analysis on the entire hot forging processes of 300 M steel large components was performed to predict the distrib...The microstructure models were integrated into finite element(FE)code,and a three-dimensional(3D)FE analysis on the entire hot forging processes of 300 M steel large components was performed to predict the distributions of effective strain,temperature field and austenite grain size.The simulated results show that the finest grains distribute in the maximum effective strain region because large strain induces the occurrence of dynamic recrystallization.However,coarse macro-grains appear in the minimum effective strain region.Then,300 M steel forging test was performed to validate the results of FE simulation,and microstructure observations and quantitative analysis were implemented.The average relative difference between the calculated and experimental austenite grain size is 7.56%,implying that the present microstructure models are reasonable and can be used to analyze the hot forging processes of 300 M steel.展开更多
The ultrahigh strength 300M steel has been commonly used in the manufacture of aircraft landing gear and rotor shaft parts due to its excellent mechanical properties.Creep feed grinding is one of the essential operati...The ultrahigh strength 300M steel has been commonly used in the manufacture of aircraft landing gear and rotor shaft parts due to its excellent mechanical properties.Creep feed grinding is one of the essential operations during the whole component manufacturing processes.In this work,the feasibility of creep feed grinding of 300M steel by using the hard zirconium corundum wheel was theoretically and experimentally evaluated.A variety of responses including grinding forces,temperature fields,specific grinding energy,surface integrity and chip modes were carefully recorded.Besides,the mechanism of ground surface profile generation and the spatial frequency spectrum of the surface profile were tentatively analyzed.It was found that the wheel speed has a relative influence on the grinding forces and temperatures of which the work hardening effect dominates the material removal with lower wheel speed while the thermal softening becomes crucial as the wheel speed exceeds the critical value for the studied 300M steel.Furthermore,a scattered spatial frequency spectrum for the generated surface profile was noticed with lower wheel speed while the spectrum gathers towards the lower frequency values with higher amplitude as the wheel speed increases.The shearing chip and flowing chip dominates the main chip type,indicating the excellent abrasive sharpness during the grinding process.In general,the used zirconium corundum wheel presents feasibility for the creep feed grinding of 300M steel because of the high material removal rate,absence of surface burn,low wheel wear and higher compressive residual stresses.展开更多
The compressive deformation behaviors of 300M high strength steel were investigated over a wide range of temperatures (850- 1200 C) and strain rates (0. 001- 10 s^- 1 ) on a Gleeble-3800 thermo-mechanical simulato...The compressive deformation behaviors of 300M high strength steel were investigated over a wide range of temperatures (850- 1200 C) and strain rates (0. 001- 10 s^- 1 ) on a Gleeble-3800 thermo-mechanical simulator. The measured flow stress was modified by the corrections of the friction and the temperature compensations, which nicely reflect negative effects of the friction and temperature on the flow stress. The corrected stress-strain curves were the dynamic recrystallization type on the conditions of higher deformation temperature and lower strain rate. Flow stress increases with the increase of strain rate at the same deformation temperature and strain. By contrast, flow stress decreases with the increase of temperature at the same strain rate and strain. Dependence of the peak stress on temperature and strain rate for 300M steel is described by means of the conventional hyperbolic sine equation. By re gression analysis, the activation energy (Q) in the whole range of deformation temperature is determined to be 367. 562 kJ/mol. The effects of the temperature and the strain rate on mierostructural evolution are obvious. With the increase of the deformation temperature and the decrease of the strain rate, the original austenite grain sizes of 300M steel increase. At the same time, the corrected flow stress curves more accurately determine the evolution of the microstrueture.展开更多
300 M ultra-high strength steel has been widely used in critical structural components for aviation and aerospace vehicles,owing to its high strength,excellent transverse plasticity,fracture toughness and fatigue resi...300 M ultra-high strength steel has been widely used in critical structural components for aviation and aerospace vehicles,owing to its high strength,excellent transverse plasticity,fracture toughness and fatigue resistance.Herein,low and high power selective laser melting(SLM)of 300 M steel and their microstructural evolution and mechanical properties have been reported.The results show that the optimal energy density range with the highest relative density for SLMed 300 M steel is between 60 and160 J/mm^3.Furthermore,molten pools for deposition exhibit a conduction mode with semi-elliptical shape at a lower laser power of 300~600 W but a keyhole mode with"U"shape at a higher laser power of 800~1900 W.The heterogeneous microstructure of as-built samples is cha racterized by a skin-core structure which is that tempered troostite with the coarse non-equiaxed grains in the molten pool is wrapped by tempered sorbite with the fine equiaxed grains in the heat-affected zone.The skin-core structure of SLMed 300 M steel has the characteristics of hard inside and soft outside.The average microhardness of samples varies from 385 to 341 HV when laser power increases from 300 to 1900 W.Interestingly,ultimate tensile strength(1156-1193 MPa)and yield tensile strength(1085-1145 MPa)of dense samples fabricated at diffe rent laser powers vary marginally.But,the elongation(6.8-9.1%)of SLMed 300 M steel is greatly affected by the laser power.展开更多
The electrochemical corrosion behavior of 300M ultra high strength steel in chloride containing environment was investigated by potentiodynamic polarization technique, electrochemical impedance spectroscopy (EIS) an...The electrochemical corrosion behavior of 300M ultra high strength steel in chloride containing environment was investigated by potentiodynamic polarization technique, electrochemical impedance spectroscopy (EIS) and scanning electron microscopy (SEM). The results show that uniform corrosion occurs on 300M steel during the elec- trochemical measurements because no anodic passivation phenomenon is observed on polarization curves within the measurement range. The tests also show that 300M steel is highly susceptible to chloride containing solution, which is characterized by corrosion current density increasing with the addition of chlorides, and corrosion potential shifting towards positive direction and corrosion resistance decreasing, pos- itively suggesting that chloride ions speed up the corrosion rate of 300M steel. Mean- while corrosion products on the 300M steel surface formed during the salt spray test are too loose and porous to effectively slow down the corrosion rate. Additionally, a schematic structure of uniform corrosion mechanism can explain that 300M steel has better property of stress corrosion cracking (SCC) resistance than stainless steels.展开更多
基金supported by the National Natural Science Foundation of China(50775182)the Scientific Research Foundation for the Returned Overseas Chinese Scholars, State Education Ministry
文摘The fatigue behavior of a high strength steel 300 M in the gigacycle regime was investigated. Fully reversed tension - compression fatigue tests at ambient temperature were performed using an ultrasonic fatigue system operating at 20 kHz.The staircase test method was employed to obtain accurate values of the mean fatigue strength corresponding to fixed numbers of cycles up to 10~9.These results were compared to the curve which is estimated by the data tested in the mid-long life regime on conventional servo hydraulic test machine at 20 Hz.Results indicate that the fatigue strength determined from ultrasonic fatigue testing is lightly higher than conventional testing in the range of 10~6-10~7 cycles.It is obvious that nucleations of fractures tend to occur below the surface, if fractures happen after more than 10~7 cycles.All the fractured specimens fails from internal SiO_2 inclusions or smaller carbides and carbide clusters.
基金Item Sponsored by National Natural Science Foundation of China(51575446)Natural Science Basis Research Plan in Shaanxi Province of China(2016JQ5070)
文摘The microstructure models were integrated into finite element(FE)code,and a three-dimensional(3D)FE analysis on the entire hot forging processes of 300 M steel large components was performed to predict the distributions of effective strain,temperature field and austenite grain size.The simulated results show that the finest grains distribute in the maximum effective strain region because large strain induces the occurrence of dynamic recrystallization.However,coarse macro-grains appear in the minimum effective strain region.Then,300 M steel forging test was performed to validate the results of FE simulation,and microstructure observations and quantitative analysis were implemented.The average relative difference between the calculated and experimental austenite grain size is 7.56%,implying that the present microstructure models are reasonable and can be used to analyze the hot forging processes of 300 M steel.
基金supported by the National Natural Science Foundation of China(U19372708)。
文摘The ultrahigh strength 300M steel has been commonly used in the manufacture of aircraft landing gear and rotor shaft parts due to its excellent mechanical properties.Creep feed grinding is one of the essential operations during the whole component manufacturing processes.In this work,the feasibility of creep feed grinding of 300M steel by using the hard zirconium corundum wheel was theoretically and experimentally evaluated.A variety of responses including grinding forces,temperature fields,specific grinding energy,surface integrity and chip modes were carefully recorded.Besides,the mechanism of ground surface profile generation and the spatial frequency spectrum of the surface profile were tentatively analyzed.It was found that the wheel speed has a relative influence on the grinding forces and temperatures of which the work hardening effect dominates the material removal with lower wheel speed while the thermal softening becomes crucial as the wheel speed exceeds the critical value for the studied 300M steel.Furthermore,a scattered spatial frequency spectrum for the generated surface profile was noticed with lower wheel speed while the spectrum gathers towards the lower frequency values with higher amplitude as the wheel speed increases.The shearing chip and flowing chip dominates the main chip type,indicating the excellent abrasive sharpness during the grinding process.In general,the used zirconium corundum wheel presents feasibility for the creep feed grinding of 300M steel because of the high material removal rate,absence of surface burn,low wheel wear and higher compressive residual stresses.
基金Sponsored by Technology Major Projects of "High-end CNC Machine Tools and Basic Manufacturing Equipment"(2012ZX04010081)Natural Science Research Foundation Program for Distinguished Young Scholars in Higher EducationInstitutions of Hebei Province of China(Y2012034)
文摘The compressive deformation behaviors of 300M high strength steel were investigated over a wide range of temperatures (850- 1200 C) and strain rates (0. 001- 10 s^- 1 ) on a Gleeble-3800 thermo-mechanical simulator. The measured flow stress was modified by the corrections of the friction and the temperature compensations, which nicely reflect negative effects of the friction and temperature on the flow stress. The corrected stress-strain curves were the dynamic recrystallization type on the conditions of higher deformation temperature and lower strain rate. Flow stress increases with the increase of strain rate at the same deformation temperature and strain. By contrast, flow stress decreases with the increase of temperature at the same strain rate and strain. Dependence of the peak stress on temperature and strain rate for 300M steel is described by means of the conventional hyperbolic sine equation. By re gression analysis, the activation energy (Q) in the whole range of deformation temperature is determined to be 367. 562 kJ/mol. The effects of the temperature and the strain rate on mierostructural evolution are obvious. With the increase of the deformation temperature and the decrease of the strain rate, the original austenite grain sizes of 300M steel increase. At the same time, the corrected flow stress curves more accurately determine the evolution of the microstrueture.
基金supported by the Pre-research Fund Project of Ministry of Equipment and Development of China though no.61409230301)the Fundamental Research Funds for the Central Universities through Program no.2019kfy XMPY005 and no.2019kfy XKJC042。
文摘300 M ultra-high strength steel has been widely used in critical structural components for aviation and aerospace vehicles,owing to its high strength,excellent transverse plasticity,fracture toughness and fatigue resistance.Herein,low and high power selective laser melting(SLM)of 300 M steel and their microstructural evolution and mechanical properties have been reported.The results show that the optimal energy density range with the highest relative density for SLMed 300 M steel is between 60 and160 J/mm^3.Furthermore,molten pools for deposition exhibit a conduction mode with semi-elliptical shape at a lower laser power of 300~600 W but a keyhole mode with"U"shape at a higher laser power of 800~1900 W.The heterogeneous microstructure of as-built samples is cha racterized by a skin-core structure which is that tempered troostite with the coarse non-equiaxed grains in the molten pool is wrapped by tempered sorbite with the fine equiaxed grains in the heat-affected zone.The skin-core structure of SLMed 300 M steel has the characteristics of hard inside and soft outside.The average microhardness of samples varies from 385 to 341 HV when laser power increases from 300 to 1900 W.Interestingly,ultimate tensile strength(1156-1193 MPa)and yield tensile strength(1085-1145 MPa)of dense samples fabricated at diffe rent laser powers vary marginally.But,the elongation(6.8-9.1%)of SLMed 300 M steel is greatly affected by the laser power.
基金supported by the Chinese National Science and Technology Infrastructure Platforms Construction Project (Grant No.2005DKA10400)Beijing Science and Technology Project (No.D09030303790901)
文摘The electrochemical corrosion behavior of 300M ultra high strength steel in chloride containing environment was investigated by potentiodynamic polarization technique, electrochemical impedance spectroscopy (EIS) and scanning electron microscopy (SEM). The results show that uniform corrosion occurs on 300M steel during the elec- trochemical measurements because no anodic passivation phenomenon is observed on polarization curves within the measurement range. The tests also show that 300M steel is highly susceptible to chloride containing solution, which is characterized by corrosion current density increasing with the addition of chlorides, and corrosion potential shifting towards positive direction and corrosion resistance decreasing, pos- itively suggesting that chloride ions speed up the corrosion rate of 300M steel. Mean- while corrosion products on the 300M steel surface formed during the salt spray test are too loose and porous to effectively slow down the corrosion rate. Additionally, a schematic structure of uniform corrosion mechanism can explain that 300M steel has better property of stress corrosion cracking (SCC) resistance than stainless steels.