Effect of sintering temperature on microstructure and properties of 3D printing polysilazane reinforced Al_(2)O_(3)core

Ceramic cores are the key intermediate components of hollow blades for aero-engine.Conventional processes,such as hot-press molding and gel film casting,face difficulties in fabricating complex-structured ceramic cores due to the complexity of moulds and long process cycles.Stereolithography 3D printing provides a new idea for the fabrication of complex-structured ceramic cores.The effect of sintering temperature on open porosity,bulk density,weight loss rate,shrinkage rate,flexural strength and microstructure of the Al_(2)O_(3)-based ceramic core doped with 10vol.%polysilazane(PSZ)was studied.The sintering mechanism of PSZ-reinforced ceramic cores was analyzed.Results show that the optimum sintering temperature of PSZ-reinforced ceramic cores is 1,450°C.At this temperature,the open porosity of the ceramic core is 36.60%,bulk density is 2.33 g·cm^(-3),weight loss rate is 22.11%,shrinkage rate along the X,Y,Z directions is 5.72%,5.01%,9.61%,respectively;the flexural strength is 28.794 MPa at 25°C and 13.649 MPa at 1,500°C.Properties of 3D printing PSZ-reinforced ceramic cores can meet the casting requirement of superalloy hollow blades,which is expected to promote the industrial application of 3D printing complex structure ceramic cores.

High-Performance and Flexible Co-Planar Integrated Microsystem of Carbon-Based All-Solid-State Micro-Supercapacitor and Real-Time Temperature Sensor

With the rapid development of flexible and portable microelectronics,the extreme demand for miniaturized,mechanically flexible,and integrated microsystems are strongly stimulated.Here,biomass-derived carbons(BDCs)are prepared by KOH activation using Qamgur precursor,exhibiting three-dimensional(3D)hierarchical porous structure.Benefiting from unobstructed 3D hierarchical porous structure,BDCs provide an excellent specific capacitance of 433 F g^(-1)and prominent cyclability without capacitance degradation after 50000 cycles at 50 A g^(-1).Furthermore,BDC-based planar micro-supercapacitors(MSCs)without metal collector,prepared by mask-assisted coating,exhibit outstanding areal-specific capacitance of 84 mF cm^(-2)and areal energy density of 10.6μWh cm^(-2),exceeding most of the previous carbon-based MSCs.Impressively,the MSCs disclose extraordinary flexibility with capacitance retention of almost 100%under extreme bending state.More importantly,a flexible planar integrated system composed of the MSC and temperature sensor is assembled to efficiently monitor the temperature variation,providing a feasible route for flexible MSC-based functional micro-devices.

3D Eddy Current and Temperature Field Analysis of Large Hydro-generators in Leading Phase Operations

As a common practice,a large hydro-generator will operate in leading phase conditions to absorb the reactive power of the power grid.However,the accurate and precise prediction of the leading phase operation capacity of a large hydro-generator has always been a formidable challenge to engineers and academicians because it is extremely hard to compute the eddy currents and losses as well as the local overheating in the pressure plate and finger.To address this problem,a full three dimensional(3D)finite element model and method of the coupled eddy current and temperature fields in the end region of a large hydro-generator are developed.The equivalent medium parameters used in the computations are comprehensively discussed.Moreover,some numerically based solution methodologies for accurate computation of the field and armature currents under different leading phase conditions are proposed.Numerical results on the coupled eddy current and temperature fields in the end regions of a 250 MW hydro-generator confirm positively the feasibility of the present work.

Visualization of 3-D temperature distribution in a 300 MW twin-furnace coal-fired boiler

Until now, it has been difficult to obtain on-line three-dimensional (3-D) temperature distribution information which can reflect the overall combustion condition in the furnace of a coal-fired power plant boiler. A combustion monitoring system is introduced which can solve the problem efficiently. Through this system, the 3-D temperature distribution in a coal-fired boiler furnace can be obtained using a novel flame image processing technique. Briefly, we first outline the visualization principle. Then, the hardware and software design of the system in a 300 MW twin-furnace coal-fired boiler are introduced in detail. The visualization of the 3-D temperature distribution in the twin-furnace boiler is realized with an industrial computer and the Distributed Control System (DCS) of the boiler. The practical operation of the system shows that it can provide valuable combustion information of a furnace and is useful for the combustion diagnosis and adjustment in coal-fired power plants.

Study on the Influence of Piloti on Mean Radiant Temperature in Residential Blocks by 3-D Unsteady State Heat Balance Radiation Calculation

Piloti is commonly used in tropical and subtropical climate zones to get high wind velocity and create shadowed areas in order to optimize the living environment of residential blocks,but there are few studies to reveal the influence of piloti on the radiant environment of residential blocks systematically. Taking the city of Guangzhou as an example,using 3-D Unsteady State Heat Balance Radiation Calculation Method,this paper shows that the mean radiant temperature( MRT) under piloti area increases with the increase of piloti ratio,and especially when piloti ratio is equal to 100%,the MRT increase trend becomes sharp. The MRT of exposed area decreases with the increase of piloti ratio,especially when piloti ratio reaches 100%,the decrease trend of MRT becomes sharp,which offers the reference for the study on piloti design in subtropical climate zones and further research on living environment by CFD simulation in residential blocks.

Reconstruction of Temperature Field in 3-D, Absorbing, Emitting, and Anisotropically Scattering Medium

The soft measurement technology of flame temperature field is an efficient method to learn the combustion status in furnace. Generally, it reconstructs the temperature field in furnace through the image of flame, which is a process to solve radiative inverse problem. In this paper, the flame of pulverized coal is considered as 3-D, absorbing, emitting, and anisotropically scattering non-gray medium. Through the study on inverse problem of radiative heat transfer, the temperature field in this kind of medium has been reconstructed. The mechanism of 3-D radiative heat transfer in a rectangular media, which is 2 m×3 m× 5 m and full of CO2, N2 and carbon particles, is studied with Monte Carlo method. The 3-D temperature field in this rectangular space is reconstructed and the influence of particles density profile is discussed.

Assimilation of FY-3D MWTS-Ⅱ Radiance with 3D Precipitation Detection and the Impacts on Typhoon Forecasts

Precipitation detection is an essential step in radiance assimilation because the uncertainties in precipitation would affect the radiative transfer calculation and observation errors.The traditional precipitation detection method for microwave only detects clouds and precipitation horizontally,without considering the three-dimensional distribution of clouds.Extending precipitation detection from 2D to 3D is expected to bring more useful information to the data assimilation without using the all-sky approach.In this study,the 3D precipitation detection method is adopted to assimilate Microwave Temperature Sounder-2(MWTS-Ⅱ)onboard the Fengyun-3D,which can dynamically detect the channels above precipitating clouds by considering the near-real-time cloud parameters.Cycling data assimilation and forecasting experiments for Typhoons Lekima(2019)and Mitag(2019)are carried out.Compared with the control experiment,the quantity of assimilated data with the 3D precipitation detection increases by approximately 23%.The quality of the additional MWTS-Ⅱradiance data is close to the clear-sky data.The case studies show that the average root-mean-square errors(RMSE)of prognostic variables are reduced by 1.7%in the upper troposphere,leading to an average reduction of4.53%in typhoon track forecasts.The detailed diagnoses of Typhoon Lekima(2019)further show that the additional MWTS-Ⅱradiances brought by the 3D precipitation detection facilitate portraying a more reasonable circulation situation,thus providing more precise structures.This paper preliminarily proves that 3D precipitation detection has potential added value for increasing satellite data utilization and improving typhoon forecasts.

Optimal Design Strategies of Femur Tumor Hyperthermia Based on Finite Element Analysis of Temperature Field

A 3D femoral model was built to obtain the three-dimensional temperature distribution of femur and its surrounding tissues and provide references for clinical applications. According to the relationship between gray-value and material properties,the model was assigned with various materials to make sure that it is more similar to the real femur in geometry and physical properties. 3D temperature distribution is obtained by using finite element analysis software ANSYS 11. 0 on the basis of heat conduction theory,Laplace equation,Pennes bio-heat transfer equation,thermo physical parameters of bone tissues,the boundary condition,and initial conditions. Taken the asymmetry of the 3D distribution of temperature into account,it is necessary to adopt the heating method with multiple heat sources. This method can ensure that the temperature fields match well with the tumor tissues and kill the tumor cells efficiently under the condition of protecting the normal tissues from damage. The analysis results supply important guidance for determining the needle position and the needle number and controlling the intensity of heating.

RESEARCH ON INFLUENCE OF TEMPERATURE ON A PRECISION FORGING PROCESS OF BLADE WITH A TENON

The blade precision forging process is a forming process with high temperature and large plastic deformation. Interaction of deformation and heat conduction leads to large uneven distribution of temperature. The unevenness of temperature distribution has a great effect on mechanical properties and the microstracture of materials. So it is necessary to consider the influence of temperature on the precision forging process of blades. Taking a blade with a tenon into consideration, a 3D mechanical model in precision forging is built up. The distribution laws of temperature field and the influence of the temperature on the equivalem stress in the process are obtained by using 3-D coupled thermo-mechanical FEM code developed by the authors Theresuits obtained illustrate that the influence of the temperature field on the blade forging process is considerable. The achievements of predicting microstructure and mechanical properties for forged blades is significant.

Temperature Field Reconstruction in High-Temperature Gas by Using the Colored Background Oriented Schlieren Method

A 3D temperature field reconstruction method using the colored background oriented schlieren(CBOS)method is proposed to address image blurring due to the different refractive index of the multi-wavelength light and significant errors produced when the traditional background oriented schlieren(BOS)method is applied to high-temperature gas.First,the traditional method is employed to reconstruct the non-uniform 3D temperature field.Second,the CBOS method is applied to correct the distortion.Then,by analyzing the correlation coefficient among different color points of the colored background pattern,the non-uniform temperature field is reconstructed much more accurately.Finally,the experimental results are verified by applying the Runge-Kutta ray-tracing method and the thermocouple contact measurement method.The maximum average temperature error of the CBOS-reconstructed temperature field is 12.92°C,compared with the thermocouples.Therefore,an accurate three-dimensional reconstruction of the temperature field can be achieved by the proposed method effectively.

Steady State Temperature Study on RF LDMOS with Structure Modification

This paper is devoted to temperature analysis on power RF LDMOS with different feature parameters of die thickness, pitch S length and finger width. The significance of these three parameters is determined from temperature comparison obtained by 3D Silvaco-Atlas device simulator. The first three simulations focus on temperature variation with the three factors at different output power density respectively. The results indicate that both the thinner die thickness and the broaden pitch S length have distinct advantages over the shorter finger width. The device, at the same time, exhibits higher temperature at a larger output power density. Simulations are further carried out on structure with combination of different pitch s length and die thickness at a large 1W/mm output power density and the temperature reduction reaches as high as 55%.

基于Deform-3D的准干式深孔钻削有限元分析

采用Deform-3D有限元分析软件对准干式BTA单刃内排屑深孔钻钻削做了仿真研究。应用Deform-3D软件设置模拟参数为干式钻削,在不同的切削用量情况下对切削力的大小、刀具磨损以及切削温度场进行了仿真分析,讨论了断屑的发生位置以及分屑的形成过程,为准干式深孔加工的切削参数和刀具参数进一步的优化提供了依据。

基于3D有限元法的圆柱形永磁体与高温超导体悬浮特性的数字仿真

在场冷和零场冷两种条件下对圆柱形永磁体与高温超导块材之间的悬浮特性进行测量和分析。提出一种基于H-法的三维有限元模型用于动态分析永磁体相对高温超导块材运动时的悬浮特性。在此模型中,高温超导体的E-J电磁特性采用幂指数模型表示,有限元非线性方程组采用超松弛迭代的解法。相对于其他有限元模型,本模型具有在相同维度下变量少、计算速度快及易收敛等特点。通过仿真曲线与实验曲线的比较,验证了模型的有效性。

基于DEFORM-3D的钛合金钻削温度场研究

为研究麻花钻的钻削参数对钛合金钻削温度的影响规律,采用DEFORM-3D软件对钛合金的钻削加工进行有限元仿真分析,建立钻削温度场模型,应用正交试验设计分析钻头直径、钻削速度和进给量三个钻削参数对钻削温度场的分布及温度的影响。通过极差分析,以图表直观反映各因素对钻削温度的影响程度,并获得最优钻削参数组合。仿真结果表明:钻削速度对于钻削温度的影响最为明显,进给量次之,钻头直径影响最小。

(E)-(5-(4-(二苯基胺)苯乙烯基)二噻吩并[2,3-b∶3′,2′-d]噻吩基)-2-亚甲基丙二腈的聚集态发光现象的研究

本文报道了对一种电子给体-受体化合物(E)-(5-(4-(二苯基胺)苯乙烯基)二噻吩并[2,3-b∶3′,2′-d]噻吩基)-2-亚甲基丙二腈(TPA-DCST)的合成与光谱学行为的研究。化合物TPA-DCST的分子结构中含有强电子给体(三苯胺)与强电子受体(二氰基乙烯)两个部分,并由二噻吩并[2,3-b∶3′,2′-d]噻吩作为共轭桥将电子给体与受体相连接。在合成方面,采用Wittig反应将三苯胺通过双键与二噻吩并[2,3-b∶3′,2′-d]噻吩相连接、醛基化,并与并二腈经Knoevenagel缩合反应合成目标产物。产物通过了核磁氢谱、碳谱、红外以及高分辨率质谱的确认。光谱方面,主要考察了该化合物的吸收与荧光行为。其最大吸收峰位在412nm左右,归属于π-π*跃迁。在非极性溶剂正己烷中表现出来自分子间聚集而形成的聚集态荧光(550nm),并通过了单分子在CTAB胶束([c]=1.02×10-2 mol/L)的发光(460nm)试验得到验证。溶剂效应表明,该化合物没有出现典型的ICT态的发光现象,其原因在于电子给体与受体相连的共轭桥单元,即二噻吩并[2,3-b∶3′,2′-d]噻吩不具有有效的共轭效应。浓度效应与温度效应进一步表明TPA-DCST分子易于产生分子间聚集态的发光。在THF-H_2O二元溶剂体系中呈现典型的聚集诱导(AIE)发光现象,发光峰位为692nm。随着TPA-DCST分子间的聚集程度的增加,聚集态的荧光出现大范围的红移,直至固体发光红移到710nm。TPA-DCST分子的聚集因素可能来自于疏脂作用、偶极-偶极相互作用等。

3D-C／SiC复合材料的高温疲劳性能

采用应力比为0.1和0.5,频率为60和20Hz的正弦波从室温至1500℃,在10-4Pa真空中对3D-C/SiC复合材料进行拉—拉疲劳实验;获得其在应力比0.1频率60Hz条件下室温、1100、1300和1500℃的疲劳曲线,以及应力比0.1频率20Hz和应力比0.5频率20Hz条件下1500℃的疲劳曲线。结果表明,若取循环基数为106周,应力比0.1频率60Hz条件下,3D-C/SiC复合材料在室温、1100、1300和1500℃的疲劳极限分别为235、350、285和240MPa,约为其拉伸强度的87%、97%、94%和90%;疲劳极限与比例极限和拉伸强度随温度有相似的变化规律,即随温度升高而增加,在1100℃达到最大值,尔后随温度增加而下降;但是S—Nf曲线的斜率的变化规律恰好与此相反。应力比的增加和频率的降低,均使复合材料1500℃的疲劳极限有所减小。

工艺参数对激光3D智能打印效果的分析研究

为了摆脱激光3D智能打印中数据复杂、3D物体表面曲率不利于计算等情况,并从多个角度稳定提升激光3D智能打印效果,需从工艺参数入手进行分析与研究,因此,提出一种激光3D智能打印工艺参数分析方法,主要进行分层厚度与覆膜工艺参数对打印效果的函数与实例分析。所提方法利用四叉树进行激光3D点云数据的处理与存储,通过切割四叉树来建立点云数据重心与分层厚度的关系图例,从四叉树切割误差入手进行最佳分层厚度的迭代求解。方法还讨论了覆膜工艺参数以及激光功率、3D扫描速率等对打印效果的影响,并给出各项工艺参数的最佳取值范围。实验结果表明,在所提方法给定的工艺参数支持下,激光3D智能打印工作的复杂度小、产品活化能高,具备很好的打印效果。

3D打印钛合金钻削性能试验研究

钛合金由于其比强度高、比刚度高、耐高温等特性,而广泛应用于航空航天领域。3D打印钛合金(激光烧结成型)由于加工制造的特殊性,使得其与常用的锻造钛合金拥有不同的组织和力学性能。本文通过钻削试验,探究了不同切削参数(转速、进给量)对切削力和切削温度的影响,为钻削3D打印钛合金提供了合理的加工参数。实验发现:钻孔加工过程中主轴转速在800-1200r/min左右,进给量保持在0.06-0.09mm/r左右比较合适。另外,钻削3D打印钛合金时,刀具磨损形式为:前刀面主要产生涂层剥落和粘结磨损,后刀面产生磨粒磨损。

Modeling and simulation of 3D thermal stresses of large-sized castings in solidification processes

When heavy machines and large scaled receiver system of communication equipment are manufactured, it always needs to produce large-sized steel castings, aluminum castings and etc. Some defects of hot cracking by thermal stress often appear during solidification process as these castings are produced, which results in failure of castings. Therefore predicting the effects of technological parameters for production of castings on the thermal stress during solidification process becomes an important means. In this paper, the mathematical models have been established and numerical calculation of temperature fields by using finite difference method (FDM) and then thermal stress fields by using finite element method (FEM) during solidification process of castings have been carried out. The technological parameters of production have been optimized by the results of calculation and the defects of hot cracking have been eliminated. Modeling and simulation of 3D thermal stress during solidification processes of large-sized castings provided a scientific basis, which promoted further development of advanced manufacturing technique.

基于Deform-3D的细长杆切削加工仿真研究

为了更好地研究细长杆的切削过程,以有限元分析法为基础,借助Deform-3D软件的切削仿真模型和数值模拟分析环境,通过对金属切削过程中切屑的形成及流动进行模拟,获得切削力变化规律,切削热和应力应变的分布情况。仿真结果对实际加工过程中工艺效果的预测提供理论依据。