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[Ni(en)_2]_6H_2[(VO)_(12)O_6B_(18)O_(42)]·15H_2O的水热合成和晶体结构 被引量:2
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作者 林志华 张汉辉 +3 位作者 黄长沧 孙瑞卿 杨齐愉 吴小园 《Chinese Journal of Structural Chemistry》 SCIE CAS CSCD 北大核心 2004年第1期83-86,共4页
在水热的条件下合成了1个多聚钒硼酸盐[Ni(en)2]6H2[(VO)12O6B18O42]15H2O,化学式为C24H128B18N24Ni6O75V12(Mr=3111.62),用单晶X射线衍射方法测定了它的结构,该晶体属三方晶系,R-3空间群,晶胞参数为a=13.942(2)?=96.476(2),V=2653.9(5)... 在水热的条件下合成了1个多聚钒硼酸盐[Ni(en)2]6H2[(VO)12O6B18O42]15H2O,化学式为C24H128B18N24Ni6O75V12(Mr=3111.62),用单晶X射线衍射方法测定了它的结构,该晶体属三方晶系,R-3空间群,晶胞参数为a=13.942(2)?=96.476(2),V=2653.9(5)?,Z=1,Dc=1.947g/cm3,=21.55cm-1,F(000)=1574,2108个可观察衍射点(I>2(I)),最终结构精修到偏离因子R=0.0594,wR=0.1398,S=1.009。在该化合物的结构中,18员环的B18O42通过18个B(3-O)V键被2个V6O15簇夹在中间,6个[Ni(en)2]基团分别通过2个Ni(3-O)B与B18O42环相连。 展开更多
关键词 [Ni(en)2]6H2[(VO)12O6B18O42].15H2O 水热法 合成 晶体结构 多聚钒硼酸盐 金属-氧簇化合物
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纤维蛋白原Bβ15-42肽对大鼠肾脏缺血再灌注损伤凋亡及相关蛋白的影响 被引量:1
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作者 黄跃琼 张紫婷 +2 位作者 仇文芳 贾珺丹 乔玉峰 《中国中西医结合肾病杂志》 2022年第12期1043-1046,I0009,共5页
目的:观察纤维蛋白原Bβ_(1)5-42肽(fibrinogen-derived peptide Bβ_(1)5-42,FgBβ_(1)5-42)对大鼠肾脏缺血再灌注损伤(ischemia-reperfusion injury,IRI)凋亡及相关蛋白的影响。方法:将24只SD大鼠随机分成假手术组(Sham组)、肾脏缺血... 目的:观察纤维蛋白原Bβ_(1)5-42肽(fibrinogen-derived peptide Bβ_(1)5-42,FgBβ_(1)5-42)对大鼠肾脏缺血再灌注损伤(ischemia-reperfusion injury,IRI)凋亡及相关蛋白的影响。方法:将24只SD大鼠随机分成假手术组(Sham组)、肾脏缺血再灌注模型组(I/R组)、FgBβ_(1)5-42肽治疗组(Fg+I/R组),每组8只。Sham组:分离肾动脉后关闭腹腔;I/R组:采用双侧肾动脉夹闭的方法制作肾脏IRI模型;Fg+I/R组:于肾脏缺血30 min后立即尾静脉注射FgBβ_(1)5-42肽3.6 mg/kg。采用血肌酐测定试剂盒和尿素氮测定试剂盒分别检测血清中肌酐(Scr)和尿素氮(BUN)水平;HE染色观察肾组织病理变化,并半定量分析肾组织病理损伤程度;TUNEL凋亡试剂盒检测肾组织细胞凋亡;Western blot检测肾组织Bcl-2、Caspase-3、Bax蛋白表达。结果:与Sham组比较,I/R组Scr、BUN增加(P<0.05);肾小管上皮细胞水肿、肾小管管腔变小、刷状缘消失、部分上皮细胞脱落,间质可见炎症细胞浸润,肾损伤评分高(P<0.05);肾组织细胞凋亡率增加(P<0.05);Caspase-3、Bax蛋白表达增加、Bcl-2蛋白表达减少(P<0.05)。与I/R组比较,Fg+I/R组Scr、BUN降低(P<0.05);肾组织病理学变化减轻,损伤评分降低(P<0.05);Caspase-3、Bax蛋白表达减少,Bcl-2蛋白表达增加(P<0.05)。结论:FgBβ_(1)5-42肽可能通过抑制细胞凋亡参与肾脏IRI保护作用。 展开更多
关键词 纤维蛋白原Bβ15-42肽 凋亡 肾脏 缺血再灌注
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Certain oscillatory integrals on unit square and their applications 被引量:6
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作者 FAN DaShan WU HuoXiong 《Science China Mathematics》 SCIE 2008年第10期1895-1903,共9页
Let Q 2 = [0, 1]2 be the unit square in two dimension Euclidean space ?2. We study the L p boundedness properties of the oscillatory integral operators T α,β defined on the set S(?3) of Schwartz test functions f by ... Let Q 2 = [0, 1]2 be the unit square in two dimension Euclidean space ?2. We study the L p boundedness properties of the oscillatory integral operators T α,β defined on the set S(?3) of Schwartz test functions f by $$ \mathcal{T}_{\alpha ,\beta } f(x,y,z) = \int_{Q^2 } {f(x - t,y - s,z - t^k s^j )e^{ - it^{ - \beta _1 } s^{ - \beta 2} } t^{ - 1 - \alpha _1 } s^{ - 1 - \alpha _2 } dtds} , $$ where β1 > α1 ? 0, β2 > α2 ? 0 and (k, j) ∈ ?2. As applications, we obtain some L p boundedness results of rough singular integral operators on the product spaces. 展开更多
关键词 oscillatory integral singular integral rough kernel unit square product space 42B10 42b15 42B20
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Boundedness for commutators of Bochner-Riesz operators below a critical index 被引量:3
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作者 Shan-zhen LU Xia XIA 《Science China Mathematics》 SCIE 2007年第6期801-813,共13页
In this paper, the authors obtain a necessary and sufficient condition for the LP bound-edness of commutators generated by Bochner-Riesz operators below a critical index and Lipschitz functions in two dimensional case... In this paper, the authors obtain a necessary and sufficient condition for the LP bound-edness of commutators generated by Bochner-Riesz operators below a critical index and Lipschitz functions in two dimensional case. The authors also discuss a similar problem for higher dimensions. 展开更多
关键词 COMMUTATOR Bochner-Riesz operators Lipschitz functions 42b15
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Multipliers and Herz type spaces 被引量:2
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作者 LU ShanZhen School of Mathematical Sciences, Beijing Normal University, Beijing 100875, China 《Science China Mathematics》 SCIE 2008年第10期1919-1936,共18页
Hrmander condition for boundedness of multiplier operators will be replaced by a weaker condition described by certain weighted or non-weighted Herz spaces. Some results on boundedness of multiplier operators are then... Hrmander condition for boundedness of multiplier operators will be replaced by a weaker condition described by certain weighted or non-weighted Herz spaces. Some results on boundedness of multiplier operators are then established. As direct corollaries of main theorems in this paper, several celebrated results on boundedness of multiplier operators will be improved or deduced. 展开更多
关键词 MULTIPLIER Herz space Herz type Hardy space 42b15 42B30 42B35
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Jackson-type and Bernstein-type inequalities for multipliers on Herz-type Hardy spaces
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作者 XIE LinSen LAN JiaCheng +1 位作者 LAN SenHua YAN DunYan 《Science China Mathematics》 SCIE 2009年第3期481-492,共12页
We establish Jackson-type and Bernstein-type inequalities for multipliers on Herz-type Hardy spaces. These inequalities can be applied to some important operators in Fourier analysis, such as the Bochner-Riesz multipl... We establish Jackson-type and Bernstein-type inequalities for multipliers on Herz-type Hardy spaces. These inequalities can be applied to some important operators in Fourier analysis, such as the Bochner-Riesz multiplier over the critical index, the generalized Bochner-Riesz mean and the generalized Able-Poisson operator. 展开更多
关键词 Herz-type Hardy space multiplier Jackson-type inequality Bernstein-type inequality 42b15 42B20
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