The 6351 wrought aluminum alloy and K2TiF6-CaF2-LiCl components were selected as raw materials to fabricate in situ Al3Ti particulate reinforced aluminum alloy at 720℃via direct melt reaction method with electromagne...The 6351 wrought aluminum alloy and K2TiF6-CaF2-LiCl components were selected as raw materials to fabricate in situ Al3Ti particulate reinforced aluminum alloy at 720℃via direct melt reaction method with electromagnetic stirring(EMS).CaF2 and LiCl acted as fluxes to lower the reaction temperature of the system.It is shown that the electromagnetic stirring and fluxes accelerate the emulsion process of K2TiF6.Optical microscopy,scanning electron microscopy,transmission electron microscopy and energy dispersive spectrum were utilized to analyze the microstructure and components of composites.Compared to composites fabricated without EMS and fluxes,the sizes of endogenetic Al3Ti are refined from 10-15μm to 2-4μm,which are often accompanied with silicon element.The morphology of Al3Ti or Al3TiSi0.22 exhibits triangle,quadrilateral and other clumpy patterns. Because of the Ca elements from CaF2,the sizes of Mg2Si decrease from 8-10μm to 1-2μm due to the formation of Ca2Si.展开更多
In situ TiB2 reinforced 6351 Al alloy composites were subjected to compression testing at strain rates and temperatures ranging from 0.001 to 10 s -1 and from 300 to 550℃,respectively,using Gleeble-1500D system.And t...In situ TiB2 reinforced 6351 Al alloy composites were subjected to compression testing at strain rates and temperatures ranging from 0.001 to 10 s -1 and from 300 to 550℃,respectively,using Gleeble-1500D system.And the associated microstructural transformations and instability phenomena were studied by observations of the optical and transmission electron microscope.The power dissipation efficiency and instability parameter were calculated following the dynamic material model and plotted with the temperature and logarithm of strain rate to obtain processing maps for strains of 0.2,0.4,and 0.6.The processing maps present the instability zones at higher strain rates.The result shows that with increasing strain,the instability zones enlarge.The microstructural examination shows that the interface separates even the particle cracks or aligns along the shear direction of the adiabatic shear band in the instability zones.Two domains of higher efficiencies correspond to dynamic recovery and dynamic recrystallization during the hot deformation.Using the processing maps,the optimum processing parameters of stain rates and temperatures can be chosen for effective hot deformation of TiB2/6351 composites.展开更多
基金Project(2012M511552) supported by China Postdoctoral Science FoundationProject(2009A080205001) supported by the State Key Fundamental Research Program of China
基金Project(2007AA03Z548)supported by the National High-Tech Research and Development Program of ChinaProject(207038)supported by the Key Program of Ministry of Education of China+3 种基金Project(06-D-021)supported by the Talents Peak in Six Key Fields of Jiangsu Province in ChinaProject(07JDG084)supported by the Technical Enablement Foundation for the Super Special Talents of Jiangsu UniversityProject(20071108)supported by the Technical Enablement Foundation of Ministry of Education for the Returned ScholarsProject(20060299006)supported by the PhD Programs Foundation of Ministry of Education of China
文摘The 6351 wrought aluminum alloy and K2TiF6-CaF2-LiCl components were selected as raw materials to fabricate in situ Al3Ti particulate reinforced aluminum alloy at 720℃via direct melt reaction method with electromagnetic stirring(EMS).CaF2 and LiCl acted as fluxes to lower the reaction temperature of the system.It is shown that the electromagnetic stirring and fluxes accelerate the emulsion process of K2TiF6.Optical microscopy,scanning electron microscopy,transmission electron microscopy and energy dispersive spectrum were utilized to analyze the microstructure and components of composites.Compared to composites fabricated without EMS and fluxes,the sizes of endogenetic Al3Ti are refined from 10-15μm to 2-4μm,which are often accompanied with silicon element.The morphology of Al3Ti or Al3TiSi0.22 exhibits triangle,quadrilateral and other clumpy patterns. Because of the Ca elements from CaF2,the sizes of Mg2Si decrease from 8-10μm to 1-2μm due to the formation of Ca2Si.
文摘In situ TiB2 reinforced 6351 Al alloy composites were subjected to compression testing at strain rates and temperatures ranging from 0.001 to 10 s -1 and from 300 to 550℃,respectively,using Gleeble-1500D system.And the associated microstructural transformations and instability phenomena were studied by observations of the optical and transmission electron microscope.The power dissipation efficiency and instability parameter were calculated following the dynamic material model and plotted with the temperature and logarithm of strain rate to obtain processing maps for strains of 0.2,0.4,and 0.6.The processing maps present the instability zones at higher strain rates.The result shows that with increasing strain,the instability zones enlarge.The microstructural examination shows that the interface separates even the particle cracks or aligns along the shear direction of the adiabatic shear band in the instability zones.Two domains of higher efficiencies correspond to dynamic recovery and dynamic recrystallization during the hot deformation.Using the processing maps,the optimum processing parameters of stain rates and temperatures can be chosen for effective hot deformation of TiB2/6351 composites.
