The surface composite modification of the 7050 aluminum alloy friction stir-welded joints was performed by shot peening(SP)/multiple rotation rolling(MRR)and MRR/SP,and the fatigue performance of the nugget zone(NZ)wa...The surface composite modification of the 7050 aluminum alloy friction stir-welded joints was performed by shot peening(SP)/multiple rotation rolling(MRR)and MRR/SP,and the fatigue performance of the nugget zone(NZ)was investigated.The results demonstrated that the fatigue life of SP/MRR samples is longer than that of MRR/SP.On the plane 150μm below the surface.The grains with high angle grain boundary account for 71.5%and 34.3%for MRR/SP and SP/MRR samples,respectively.The crack propagation path of the MRR/SP is transgranular and intergranular,and it is intergranular for the MRR/SP.Multitudinous fatigue striations and some voids appeared at the fracture during the stable crack propagation stage.However,fatigue striations for SP/MRR are with smaller spacing,fewer holes,and smaller size under SP/MRR compared with fatigue fracture of MRR/SP.The differences in fatigue properties and fracture characteristics of the NZ are related to the microstructure after the two combined surface modifications.展开更多
The passive film-induced stress and the susceptibility to SCC of 7050 aluminum alloy in 3.5%sodium chloride solution at various pH values were investigated by slow strain rate testing(SSRT) and flowing stress differ...The passive film-induced stress and the susceptibility to SCC of 7050 aluminum alloy in 3.5%sodium chloride solution at various pH values were investigated by slow strain rate testing(SSRT) and flowing stress differential method.The results showed that the passive film-induced stress and the susceptibility to SCC decreased with increasing pH values when pH≤7,while they increased with increasing pH values when pH7.However,the corrosion type was interpreted as exfoliation corrosion when pH=l and 14,and there was no film formed on the surface of the specimens.The whole variation plots of film-induced stress and the SCC susceptibility with pH values were both presented as a valley shape.The symbol and amount of the film-induced stress were related to the compositions of the passive film,which were analyzed using X-ray photoelectron spectroscopy(XPS).展开更多
Extrusion experiments with different filling contents at the temperature of 440 ℃ were conducted for solution treated 7050 aluminum alloy.The microstructure of typical regions with different filler contents were desc...Extrusion experiments with different filling contents at the temperature of 440 ℃ were conducted for solution treated 7050 aluminum alloy.The microstructure of typical regions with different filler contents were described qualitatively and characterized quantitatively by electron backscattered diffraction technique(EBSD) and TEM.Fraction of deformed structure decrease continuously since ε=0.72.Second phase particles distribute dispersively and interact with dislocations when ε=0.66,which delays the occurrence of DRX.As the strain increases,particles dissolve into the matrix,and their number reduces rapidly.The influence of particles on dislocation accumulation is impaired,so dislocations accumulate on the subgrain boundaries continuously,and lead to the transformation of subgrain boundaries into high angle grain boundaries(HAGBs).The continuous dynamic recrystallization(CDRX) occurrs at the strain of 0.81~0.85.At ε=0.92,CDRX convert rapidly with the increase of HAGBs fraction.But the size of CDRX grains is deduced to be minimum 3.3 μm by theoretical analysis,and it is obtained from experimental result that the maximal size of CDRX is 5.3 μm.展开更多
The structure evolutions of ZL109 alloy and 7050 alloy were studied in the processes of preparing raw billets by low super heat casting, remelting the raw billets, semisolid forming and heat treating components. The t...The structure evolutions of ZL109 alloy and 7050 alloy were studied in the processes of preparing raw billets by low super heat casting, remelting the raw billets, semisolid forming and heat treating components. The thin and symmetrical structure was obtained by using low super heat casting process. The eutectic that lied in the raw billet of ZL109 alloy remelted and produced liquid phase in the process of remelting, but to the 7050 alloy, the eutectic of intergranular and the pointedness of grains was remelted to make the grains more uniform and smooth. In the process of semisolid forming, the primary α and the eutectic inside the ZL109 alloy were separated partly and the grains in the 7050 alloy was conglutinated together. After heat treatment, the eutectic α grains of ZL109 traveled to primary α and shaped the white fishing net like organization; the eutectic Si grains assembled into the black massive particles. As to 7050, after heat treatment, α particles recrystallized and thin grains pattern was obtained.展开更多
Thin-walled long stringer made of aluminum alloy 7050-T7451 is prone to deformation during transportation,so a research of residual stress relaxation was launched in this paper.The transport resonance stress of long s...Thin-walled long stringer made of aluminum alloy 7050-T7451 is prone to deformation during transportation,so a research of residual stress relaxation was launched in this paper.The transport resonance stress of long stringer was analyzed based on the power spectral density of road transport acceleration.The residual stress relaxation experiment of aluminum alloy 7050-T7451 under different equivalent stress levels was designed and carried out.According to the amount of residual stress relaxation in the experiment,an analytical model was established with the equivalent stress level coefficient.The deflection range of long stringer was evaluated under different damping ratios.The results show that when the equivalent stress exceeds 0.8σ0.2,the residual stress relaxation of the thin-walled samples occurs.The residual stress relaxation increases linearly with the equivalent stress,which is logarithmically related to the loading cycle.The deformation caused by residual stress relaxation of the long stringer is proportional to the square of the length and the bending moment caused by stress rebalance,and inversely proportional to the moment of inertia of the structure.As the damping ratio decreases from 0.03 to 0.01,the total deflection of the long stringer increases from 0 to above 1.55 mm.展开更多
The microstructure of 7050 AI alloy in T74 condition has been studied by means of transmis- sion electron microscopy and dynamical diffraction simulation.It was found that the alloy studied contains mainly AI3Zr super...The microstructure of 7050 AI alloy in T74 condition has been studied by means of transmis- sion electron microscopy and dynamical diffraction simulation.It was found that the alloy studied contains mainly AI3Zr superlattice phase,η′-phase and Al_7Cu_2Fe constituent phase. The η′-phase has an orthorombic crystal structure with a=0.492 nm,b=0.852 nm and c=0.701 nm.The orientation relationship between the η′-phase and matrix was determined as(101)_m∥(010)_(η′)[111]_m∥[001]_(η′)展开更多
3 mm thick 7050-T7451 aluminum alloy joint was obtained by friction stir welding, and the two-step aging treatment was performed at 121 ℃ × 5 h + 163 ℃× 27 h after welding. Microstructure, hardness profile...3 mm thick 7050-T7451 aluminum alloy joint was obtained by friction stir welding, and the two-step aging treatment was performed at 121 ℃ × 5 h + 163 ℃× 27 h after welding. Microstructure, hardness profiles and stress corrosion sensitivity of the joint were measured and studied. The results indicate that through the two-step aging, the grain size is coarsened, the age-hardening precipitates and PFZ become wider at the same time, which results in the discontinuous grain boundary;the microhardness of the FSW joints decreased, but the heat-affected zone significantly narrowed, which increased the uniformity of the microhardness of the FSW joints;and the two-stage aging effectively reduced the stress corrosion sensitivity of the FSW joints. The joints with aging treatment were not broken after 60 days,however all the joints without aging treatment were broken within 1 day.展开更多
In nanofluid minimum quantity lubrication(NMQL)milling of aviation aluminum alloy,it is the bottleneck problem to adjust the position parameters(target distance,incidence angle,and elevation angle)of the nozzle to imp...In nanofluid minimum quantity lubrication(NMQL)milling of aviation aluminum alloy,it is the bottleneck problem to adjust the position parameters(target distance,incidence angle,and elevation angle)of the nozzle to improve the surface roughness of milling,which has large and uncontrollable errors.In this paper,the influence law of milling cutter speed,helical angle,and cavity shape on the flow field around the milling cutter was studied,and the optimal nozzle profile parameters were obtained.Using 7050 aluminum alloy as the workpiece material,the milling experiment of the NMQL cavity was conducted by utilizing cottonseed oil-based Al2 O3 nanofluid.Results show that the high velocity of the surrounding air flow field and the strong gas barrier could be attributed to high rotating velocities of the milling cutter.The incidence angle of the nozzle was consistent with the helical angle of the milling cutter,the target distance was appropriate at 25–30 mm,and the elevation angle was suitable at 60°–65°.The range and variance analyses of the signal-to-noise ratio of milling force and roughness were performed,and the chip morphology was observed and analyzed.The results show that the optimal combination of nozzle position parameters was the target distance of 30 mm,the incidence angle of 35°,and the elevation angle of 60°.Among these parameters,target distance had the largest impact on cutting performance with a contribution rate of more than 55%,followed by incidence angle and elevation contribution rate.Analysis by orthogonal experiment revealed that the nozzle position parameters were appropriate,and Ra(0.087 lm)was reduced by 30.4%from the maximum value(0.125 lm).Moreover,Rsm(0.05 mm)was minimum,which was 36%lower than that of the seventh group(Rsm=0.078 mm).展开更多
The fatigue behavior of aluminum alloy 7050-T7451 single lap four-bolted joints was studied by high- frequency fatigue test and finite element (FE) methods. The fatigue test results showed that a better enhancement ...The fatigue behavior of aluminum alloy 7050-T7451 single lap four-bolted joints was studied by high- frequency fatigue test and finite element (FE) methods. The fatigue test results showed that a better enhancement of fatigue life was achieved for the joints with highlocked bolts by employing the combinations of cold expansion, interference fit, and clamping force. The fractography revealed that fatigue cracks propagated tortuously; more fatigue micro-cliffs, tearing ridges, lamellar structure were observed, and fatigue striation spacing was simultaneously reduced. The evaluation of residual stress conducted by FE methods confirmed the experimental results and locations of fatigue crack initiation. The extension of fatigue lives can be attributed to the evolution of fatigue damage and effect of beneficial compressive residual stresses around the hole, resulting in the delay of crack initiation, crack deflection, and plasticityinduced crack closure.2017 Published by Elsevier Ltd on behalf of The editorial office of Journal of Materials Science & Technology.展开更多
The stress corrosion cracking(SCC) behavior and mechanism of 7050-T7451 aluminum alloy under wet-dry cyclic conditions were investigated. Slow strain rate tests(SSRTs) and electrochemical tests were used to study the ...The stress corrosion cracking(SCC) behavior and mechanism of 7050-T7451 aluminum alloy under wet-dry cyclic conditions were investigated. Slow strain rate tests(SSRTs) and electrochemical tests were used to study the effects of dry/wet ratio(DWR) and pre-immersion on SCC.Fracture and side surface characterizations were observed by scanning electron microscopy(SEM).The results demonstrate that SCC susceptibility decreases with an increase of the DWR. With an increase of the pre-immersion time, both continuous pre-immersion(CP) and wet-dry cyclic preimmersion(WDP) samples are more sensitive to SCC, and the cracking mode in the SCC fracture region is intergranular. Furthermore, the effect of WDP on SCC is greater than that of CP when the total time immersed in solution before an SSRT is the same with each other. In fact, each single wetdry cycle can be divided into three processes with respect to the change of solution on samples’ surface. Volatilization of water on the surface results in an increase in solute concentration, thus accelerating corrosion.展开更多
Aluminum alloy 7050 is widely used in the aeronautical industries.However,owing to their highly ductile property,chips created during high-speed machining cannot be naturally broken,and long continuous chips are unavo...Aluminum alloy 7050 is widely used in the aeronautical industries.However,owing to their highly ductile property,chips created during high-speed machining cannot be naturally broken,and long continuous chips are unavoidably formed,impacting the machining stability and quality of the parts.Because a smaller cutting allowance is required compared with conventional machining operations,the behavior of the chips during reaming operation may be more complex and different from those determined in previous investigations.Therefore,studying the characteristics of chip formation and hole quality during the reaming process is essential to improve the machinability of aluminum alloy 7050.In this study,three different cooling conditions were applied to reaming aluminum alloy 7050-T7451 with polycrystalline diamond(PCD)reamers.The finite element models(FEMs)were established to simulate the chip formation.The macro-and micro-morphologies of chips under the three cooling conditions were compared to analyze the chip behaviors.The diameter,surface roughness,and micro-morphologies of the reamed holes were also analyzed to evaluate the hole quality.The results showed that the chip morphology was strongly influenced by the cutting parameters and cooling strategies.It was found that the desired chip morphologies satisfactory geometrical accuracy and surface quality during the reaming of aluminum alloy 7050-T7451 could be achieved using internal cooling at a spindle speed of 8000 r/min and a feed rate of 0.0l mm/z.This study also demonstrates the feasibility of an internal cooling strategy for breaking chips when reaming aluminum alloy 7050-T7451,which opens new possibilities for improving the chip-snarling that occurs during hole machining.展开更多
基金supported by the National Natural Science Foundation of China(Grants 51865028)the Gansu Provincial Science and Technology Planning Project(Grant No.20YF8GA056).
文摘The surface composite modification of the 7050 aluminum alloy friction stir-welded joints was performed by shot peening(SP)/multiple rotation rolling(MRR)and MRR/SP,and the fatigue performance of the nugget zone(NZ)was investigated.The results demonstrated that the fatigue life of SP/MRR samples is longer than that of MRR/SP.On the plane 150μm below the surface.The grains with high angle grain boundary account for 71.5%and 34.3%for MRR/SP and SP/MRR samples,respectively.The crack propagation path of the MRR/SP is transgranular and intergranular,and it is intergranular for the MRR/SP.Multitudinous fatigue striations and some voids appeared at the fracture during the stable crack propagation stage.However,fatigue striations for SP/MRR are with smaller spacing,fewer holes,and smaller size under SP/MRR compared with fatigue fracture of MRR/SP.The differences in fatigue properties and fracture characteristics of the NZ are related to the microstructure after the two combined surface modifications.
基金Funded by the National Natural Science Foundation of China(No.51371039)
文摘The passive film-induced stress and the susceptibility to SCC of 7050 aluminum alloy in 3.5%sodium chloride solution at various pH values were investigated by slow strain rate testing(SSRT) and flowing stress differential method.The results showed that the passive film-induced stress and the susceptibility to SCC decreased with increasing pH values when pH≤7,while they increased with increasing pH values when pH7.However,the corrosion type was interpreted as exfoliation corrosion when pH=l and 14,and there was no film formed on the surface of the specimens.The whole variation plots of film-induced stress and the SCC susceptibility with pH values were both presented as a valley shape.The symbol and amount of the film-induced stress were related to the compositions of the passive film,which were analyzed using X-ray photoelectron spectroscopy(XPS).
文摘Extrusion experiments with different filling contents at the temperature of 440 ℃ were conducted for solution treated 7050 aluminum alloy.The microstructure of typical regions with different filler contents were described qualitatively and characterized quantitatively by electron backscattered diffraction technique(EBSD) and TEM.Fraction of deformed structure decrease continuously since ε=0.72.Second phase particles distribute dispersively and interact with dislocations when ε=0.66,which delays the occurrence of DRX.As the strain increases,particles dissolve into the matrix,and their number reduces rapidly.The influence of particles on dislocation accumulation is impaired,so dislocations accumulate on the subgrain boundaries continuously,and lead to the transformation of subgrain boundaries into high angle grain boundaries(HAGBs).The continuous dynamic recrystallization(CDRX) occurrs at the strain of 0.81~0.85.At ε=0.92,CDRX convert rapidly with the increase of HAGBs fraction.But the size of CDRX grains is deduced to be minimum 3.3 μm by theoretical analysis,and it is obtained from experimental result that the maximal size of CDRX is 5.3 μm.
文摘The structure evolutions of ZL109 alloy and 7050 alloy were studied in the processes of preparing raw billets by low super heat casting, remelting the raw billets, semisolid forming and heat treating components. The thin and symmetrical structure was obtained by using low super heat casting process. The eutectic that lied in the raw billet of ZL109 alloy remelted and produced liquid phase in the process of remelting, but to the 7050 alloy, the eutectic of intergranular and the pointedness of grains was remelted to make the grains more uniform and smooth. In the process of semisolid forming, the primary α and the eutectic inside the ZL109 alloy were separated partly and the grains in the 7050 alloy was conglutinated together. After heat treatment, the eutectic α grains of ZL109 traveled to primary α and shaped the white fishing net like organization; the eutectic Si grains assembled into the black massive particles. As to 7050, after heat treatment, α particles recrystallized and thin grains pattern was obtained.
基金Supported by National Natural Science Foundation of China(Grant No.51405226).
文摘Thin-walled long stringer made of aluminum alloy 7050-T7451 is prone to deformation during transportation,so a research of residual stress relaxation was launched in this paper.The transport resonance stress of long stringer was analyzed based on the power spectral density of road transport acceleration.The residual stress relaxation experiment of aluminum alloy 7050-T7451 under different equivalent stress levels was designed and carried out.According to the amount of residual stress relaxation in the experiment,an analytical model was established with the equivalent stress level coefficient.The deflection range of long stringer was evaluated under different damping ratios.The results show that when the equivalent stress exceeds 0.8σ0.2,the residual stress relaxation of the thin-walled samples occurs.The residual stress relaxation increases linearly with the equivalent stress,which is logarithmically related to the loading cycle.The deformation caused by residual stress relaxation of the long stringer is proportional to the square of the length and the bending moment caused by stress rebalance,and inversely proportional to the moment of inertia of the structure.As the damping ratio decreases from 0.03 to 0.01,the total deflection of the long stringer increases from 0 to above 1.55 mm.
文摘The microstructure of 7050 AI alloy in T74 condition has been studied by means of transmis- sion electron microscopy and dynamical diffraction simulation.It was found that the alloy studied contains mainly AI3Zr superlattice phase,η′-phase and Al_7Cu_2Fe constituent phase. The η′-phase has an orthorombic crystal structure with a=0.492 nm,b=0.852 nm and c=0.701 nm.The orientation relationship between the η′-phase and matrix was determined as(101)_m∥(010)_(η′)[111]_m∥[001]_(η′)
基金National Natural Science Foundation of China (51774047)Beijing Great Wall Scholars Training Program(CIT&TCD20170309)。
文摘3 mm thick 7050-T7451 aluminum alloy joint was obtained by friction stir welding, and the two-step aging treatment was performed at 121 ℃ × 5 h + 163 ℃× 27 h after welding. Microstructure, hardness profiles and stress corrosion sensitivity of the joint were measured and studied. The results indicate that through the two-step aging, the grain size is coarsened, the age-hardening precipitates and PFZ become wider at the same time, which results in the discontinuous grain boundary;the microhardness of the FSW joints decreased, but the heat-affected zone significantly narrowed, which increased the uniformity of the microhardness of the FSW joints;and the two-stage aging effectively reduced the stress corrosion sensitivity of the FSW joints. The joints with aging treatment were not broken after 60 days,however all the joints without aging treatment were broken within 1 day.
基金the National Natural Science Foundation of China(Nos.51975305,51806112and 51905289)the Major Research Project of Shandong Province of China(Nos.2019GGX104040 and 2019GSF108236)+2 种基金the Shandong Provincial Natural Science Foundation of China(No.ZR2019PEE008)Major Science and Technology Innovation Engineering Projects of Shandong Province of China(No.2019JZZY020111)Applied Basic Research Youth Project of Qingdao Science and Technology Plan of China(No.19-6-2-63-cg)。
文摘In nanofluid minimum quantity lubrication(NMQL)milling of aviation aluminum alloy,it is the bottleneck problem to adjust the position parameters(target distance,incidence angle,and elevation angle)of the nozzle to improve the surface roughness of milling,which has large and uncontrollable errors.In this paper,the influence law of milling cutter speed,helical angle,and cavity shape on the flow field around the milling cutter was studied,and the optimal nozzle profile parameters were obtained.Using 7050 aluminum alloy as the workpiece material,the milling experiment of the NMQL cavity was conducted by utilizing cottonseed oil-based Al2 O3 nanofluid.Results show that the high velocity of the surrounding air flow field and the strong gas barrier could be attributed to high rotating velocities of the milling cutter.The incidence angle of the nozzle was consistent with the helical angle of the milling cutter,the target distance was appropriate at 25–30 mm,and the elevation angle was suitable at 60°–65°.The range and variance analyses of the signal-to-noise ratio of milling force and roughness were performed,and the chip morphology was observed and analyzed.The results show that the optimal combination of nozzle position parameters was the target distance of 30 mm,the incidence angle of 35°,and the elevation angle of 60°.Among these parameters,target distance had the largest impact on cutting performance with a contribution rate of more than 55%,followed by incidence angle and elevation contribution rate.Analysis by orthogonal experiment revealed that the nozzle position parameters were appropriate,and Ra(0.087 lm)was reduced by 30.4%from the maximum value(0.125 lm).Moreover,Rsm(0.05 mm)was minimum,which was 36%lower than that of the seventh group(Rsm=0.078 mm).
基金supported by Key Research and Development Plan of Shandong Province, China (2017GGX20140)Natural Science Foundation of Shandong Province, China (No. ZR2014JL031)
文摘The fatigue behavior of aluminum alloy 7050-T7451 single lap four-bolted joints was studied by high- frequency fatigue test and finite element (FE) methods. The fatigue test results showed that a better enhancement of fatigue life was achieved for the joints with highlocked bolts by employing the combinations of cold expansion, interference fit, and clamping force. The fractography revealed that fatigue cracks propagated tortuously; more fatigue micro-cliffs, tearing ridges, lamellar structure were observed, and fatigue striation spacing was simultaneously reduced. The evaluation of residual stress conducted by FE methods confirmed the experimental results and locations of fatigue crack initiation. The extension of fatigue lives can be attributed to the evolution of fatigue damage and effect of beneficial compressive residual stresses around the hole, resulting in the delay of crack initiation, crack deflection, and plasticityinduced crack closure.2017 Published by Elsevier Ltd on behalf of The editorial office of Journal of Materials Science & Technology.
基金co-supported by the National Natural Science Foundation of China (No. 51671013)the Beijing Nova Program of China (No. Z161100004916061)
文摘The stress corrosion cracking(SCC) behavior and mechanism of 7050-T7451 aluminum alloy under wet-dry cyclic conditions were investigated. Slow strain rate tests(SSRTs) and electrochemical tests were used to study the effects of dry/wet ratio(DWR) and pre-immersion on SCC.Fracture and side surface characterizations were observed by scanning electron microscopy(SEM).The results demonstrate that SCC susceptibility decreases with an increase of the DWR. With an increase of the pre-immersion time, both continuous pre-immersion(CP) and wet-dry cyclic preimmersion(WDP) samples are more sensitive to SCC, and the cracking mode in the SCC fracture region is intergranular. Furthermore, the effect of WDP on SCC is greater than that of CP when the total time immersed in solution before an SSRT is the same with each other. In fact, each single wetdry cycle can be divided into three processes with respect to the change of solution on samples’ surface. Volatilization of water on the surface results in an increase in solute concentration, thus accelerating corrosion.
文摘Aluminum alloy 7050 is widely used in the aeronautical industries.However,owing to their highly ductile property,chips created during high-speed machining cannot be naturally broken,and long continuous chips are unavoidably formed,impacting the machining stability and quality of the parts.Because a smaller cutting allowance is required compared with conventional machining operations,the behavior of the chips during reaming operation may be more complex and different from those determined in previous investigations.Therefore,studying the characteristics of chip formation and hole quality during the reaming process is essential to improve the machinability of aluminum alloy 7050.In this study,three different cooling conditions were applied to reaming aluminum alloy 7050-T7451 with polycrystalline diamond(PCD)reamers.The finite element models(FEMs)were established to simulate the chip formation.The macro-and micro-morphologies of chips under the three cooling conditions were compared to analyze the chip behaviors.The diameter,surface roughness,and micro-morphologies of the reamed holes were also analyzed to evaluate the hole quality.The results showed that the chip morphology was strongly influenced by the cutting parameters and cooling strategies.It was found that the desired chip morphologies satisfactory geometrical accuracy and surface quality during the reaming of aluminum alloy 7050-T7451 could be achieved using internal cooling at a spindle speed of 8000 r/min and a feed rate of 0.0l mm/z.This study also demonstrates the feasibility of an internal cooling strategy for breaking chips when reaming aluminum alloy 7050-T7451,which opens new possibilities for improving the chip-snarling that occurs during hole machining.