Characterization and Analysis of Inconel 718 Alloy Ground at Different Speeds

Inconel 718(IN718)alloy is widely applied to fabricate high temperature resistant or corrosion resistant parts due to its excellent mechanical performance.However,the machining of IN718 alloy is difficult as it may cause serious tool wear and poor surface quality(SQ)of the workpiece.In this work,grinding experiments on IN718 alloy at different speeds were conducted by using a CBN grinding wheel.The relationship between grinding speed,SQ and subsurface damage(SSD)was well studied.With increasing grinding speed,surface roughness decreased,and SQ was greatly improved.Meanwhile,the microhardness of the grinding surface declined as the grinding speed increased.The SSD depth was almost unchanged when the grinding speed was lower than 15 m/s,then it decreased with higher grinding speeds.It was attributed to the mechanical-thermal synergistic effect in the grinding process.The results indicated that increasing grinding speed can effectively improve the SQ and reduce the SSD of IN718 alloy.The conclusion in the work may also provide insight into processing other hard-to-machining materials.

Effect of two-step solid solution on microstructure andδphase precipitation of Inconel 718 alloy

Inconel 718 is the most popular nickel-based superalloy and is extensively used in aerospace,automotive,and energy indus-tries owing to its extraordinary thermomechanical properties.The effects of different two-step solid solution treatments on microstructure andδphase precipitation of Inconel 718 alloy were studied,and the transformation mechanism fromγ″metastable phase toδphase was clarified.The precipitates were statistically analyzed by X-ray diffractometry.The results show that theδphase content firstly increased,and then decreased with the temperature of the second-step solid solution.The changes in microstructure andδphase were studied by scanning electron microscopy and transmission electron microscopy.An intragranularδphase formed in Inconel 718 alloy at the second-[100]_(δ)[011]γ step solid solution temperature of 925℃,and its orientation relationship withγmatrix was determined as//and(010)_(δ)//(111)γ.Furthermore,the Vickers hardness of different heat treatment samples was measured,and the sample treated by second-step solid solution at 1010℃ reached the maximum hardness of HV 446.84.

Effects of P and B addition on as-cast microstructure and homogenization parameter of Inconel 718 alloy

The effects of phosphorus and boron addition on the as-cast microstructure and homogenization parameters of Inconel 718 were studied. The results indicate that the addition of phosphorus and boron promotes the formation of blocky Laves phase. Due to the strong segregation behavior of boron in the final residual liquid, a low melting B-bearing phase enriched in Nb, Mo and Cr is observed. According to the differential scanning calorimeter results and electron probe micro-analysis characterization, the solidification sequence of Inconel 718 with phosphorus and boron addition in best combination is determined as L→L＋γ→L＋γ＋MC→L＋γ＋MC＋Laves→γ＋MC＋Laves＋MC＋Laves＋B-bearing phase. Accordingly, the homogenization temperature is recommended to be adjusted at least 40°C lower than that of standard Inconel 718 due to the existence of low melting B-bearing phase.

Microstructural characterization of Inconel 718 alloy after pulsed laser surface treatment at different powers

An annealed Inconel 718 alloy was surface-treated by pulsed laser at three different powers（100, 50 and 25 W）. Microstructural changes induced by the laser treatments were characterized by use of electron backscatter diffraction and electron channeling contrast imaging techniques. Results show that both annealing twins and strengthening precipitates profusely existing in the as-received specimen are dissolved at elevated temperatures during the laser irradiation. Meanwhile, in the melting zone（MZ）, densities of low angle boundaries（LABs） are greatly increased with a large number of Laves phases preferentially distributed along such LABs. For different specimens, widths and depths of their MZs are found to be gradually reduced with decreasing the laser powers. Orientation analyses reveal that the columnar grains in the MZ of the 100 W specimen could inherit orientations existing in the matrix while lower laser powers promote the formation of more nuclei with scattered orientations to grow to be granular grains in the MZ. Hardness tests reveal that the MZs of all laser-treated specimens are softer than the matrix probably due to both precipitate dissolution and grain coarsening.

CONSTITUTIVE RELATIONSHIP OF IN718 ALLOY FOR THERMOVISCOPLASTIC AND MICROSTRUCTURE EVOLUTION COUPLED ANALYSIS

The interaction between thermomechanical parameters and microstructure evolution is so intense that it must be considered during the finite element method （FEM） simulation of the hot plastic working process, for materials that are difficult to deform. Taking the microstructure evolution into account, a novel type of constitutive relationship has been put forward for the IN718 alloy. The microstructure evolution model was first established for the dominant microstructure evolution processes. Then the microstructure evolution models and the method to determine the local flow stress of the corresponding microstructure for current thermomechanical parameters and deformation history were presented. Once the local flow stresses of different structures and their volume contributions were defined, the apparent flow stress of the material could be determined as the weighted sum of the local flow stresses and volume contributions. To validate the proposed method, a thermoviscoplastics and microstructure evolution coupled analysis for a forging process of a critical IN718 disk forging was performed. The predicting results were in close agreement with the experimental data.

Influence of magnetically constricted arc traverse speed (MCATS) on tensile properties and microstructural characteristics of welded Inconel 718 alloy sheets

The magnetically constricted arc technique was implemented to mitigate the heat input related metallurgical problems in Gas Tungsten Arc Welding(GTAW)of Inconel 718 alloy particularly Nb segregation and subsequent laves phase evolution in fusion zone.This paper reports the direct effect of magnetically constricted arc traverse speed(MCATS)on bead profile,tensile properties and microstructural evolution of Inconel 718 alloy sheets joined by Gas Tungsten Constricted Arc Welding(GTCAW)process.The mechanism amenable for the microstructural modification and corresponding influence on the tensile properties of joints is investigated both in qualitative and quantitative manner related to the mechanics of arc constriction and pulsing.It is correlated to the solidification conditions during welding.The relationship between MCATS and Arc Constriction Current(ACC)was derived.Its interaction effect on the magnetic arc constriction and joint performance was analysed.Results showed that the joints fabricated using CATS of 70 mm/min exhibited superior tensile properties(98.39% of base metal strength with 31.50% elongation).It is attributed to the grain refinement in fusion zone microstructure leading to the evolution of finer,discrete laves phase in interdendritic areas.

Effect of Carbon on DA718 Alloy with P Addition

Lower content of carbon can further improve the stress rupture life of p-modified DA 718 alloy up to more than 270%. Meanwhile, the ductility of the alloy decreased a little. More boron atoms dissociate due to decreasing carbon content and interact with phosphorus which brings the longer stress rupture life of the alloy. Less carbon may induce more phosphorus segregating in the grain boundary and result in brittleness.

Influence of Different Lubricants on Deformation Behaviour of IN 718 Alloy in Hot Compression Process

The influence of different lubricants on the deformation behaviour of IN 718 alloy was studied. The results show that, with the improvement of lubrication condition, the deformation of the alloy tends to be homogeneous, and the resistance of deformation decreases. Consequently, FR 2 glass lubricant is considered to be an ideal choice when the relationship between stress and strain of IN 718 alloy is measured by means of hot compression experiment.

Orientational growth behavior and mechanism of delta(δ)phase precipitation in cold-rolled Inconel 718 alloy during heat treatment

Due to the important role ofδphase's quantity and morphology in the mechanical and fatigue properties of Inconel 718 alloy and its components,it is necessary to renew insights into the effect of cold deformation on theδphase precipitation,especially on the morphology evolution.Therefore,the nucleation and growth behavior ofδphase in cold-rolled Inconel 718 alloy during aging were investigated.The results show that the precipitation rate and volume fraction ofδphase increase with increasing the cold rolling reduction from 10%to 50%.The volume fraction ofδphase reaches equilibrium after 5 h,remaining at 5.98%,6.52%,and 6.79%under different rolling reductions(10%,30%,and 50%),respectively.The nucleation ofδphase mainly occurs on different sites(grain boundaries,new twin boundaries and old twin boundaries)under 10%rolling reduction,whileδphase mainly nucleates on the new grain boundaries of static recrystallization due to 50%rolling reduction.And the growth ofδphase undergoes a process of alternate orientation growth from spherical(nucleation)→short rod(longitudinal orientation growth)→short rod(radial orientation growth)→dynamic equilib-rium.Under 10%rolling reduction,δphase tends to grow into the matrix,while under 50%rolling reduction,the orientation grows faster and is easily affected by the grain boundary curvature.

Effect of rotation angle on surface morphology, microstructure, and mechanical properties of Inconel 718 alloy fabricated by high power laser powder bed fusion

Rotation angle of the laser scan direction between two adjacent layers is a key controlling parameter during the high-power (≥ 1 kW) laser powder bed fusion (HP-LPBF) process. This study investigates the influences of rotation angles (θ = 0°, 45°, 90°, 105°) on the surface morphology, microstructure, and mechanical properties of Inconel 718 (IN718) alloy produced by HP-LPBF. Results show that adopting low rotation angles (e.g., 0° and 45°) is prone to relatively poor surface finish and lack-of-fusion defects, whereas adopting high rotation angles (e.g., 90° and 105°) induces smaller surface roughness and better relative density. Each case reveals a noticeable edge effect but the maximal heights witness a downward trend with the increase of rotation angle. There are some minor differences in the primary dendrite arm spacing and grain morphology by varying the rotation angles. Moreover, the tensile property is slightly enhanced as the rotation angle increases. The present work suggests that high rotation angles like 90° and 105° would probably be more favorable for the 1 kW HP-LPBF process than rotation angles with relatively low values.

High temperature tensile properties of laser butt-welded plate of Inconel 718 superalloy with ultra-fine grains

For successfully forming multi-sheet cylinder sandwich structure of Inconel 718 superalloy, high temperature tensile properties of laser butt-welded plate of Inconel 718 superalloy were studied. The experiment results show that tensile direction has great effect on elongation of the laser butt-welded plate. Under conditions of transverse direction tension, the maximum elongation reaches 458.56% at 950 °C with strain rate of 3.1-10-4 s-1, in which the strain rate sensitivity value m is 0.352 and the welding seam is not deformed. Under conditions of longitudinal direction tension, the maximum elongation is 178.96% at 965 °C with strain rate of 6.2-10-4 s-1, in which m-value is 0.261, and the welding seam contributes to the deformation with the matrix. The microstructure in as-welded fusion zone is constituted of austenite dendrites and Laves phase precipitated in interdendrites. After longitudinal direction tension, a mixed microstructure with dendrite and equiaxed crystal appears in the welding seam due to dynamic recrystallization. After high temperature deforming, many δ-phase grains are transformed from Laves phase grains but a small part of residual Laves phase grains still exist in the welding seam. The deformation result of multi-sheet cylinder sandwich structure verifies that high temperature plasticity of the laser butt-welded plate can meet the requirement of superplastic forming.

SUPERPLASTICITY AND DIFFUSION BONDING OF IN718 SUPERALLOY

The superplasticity and diffusion bonding of IN718 superalloy were studied in this article. The strain rate sensitivity index m was obtained at different temperatures and various initial strain rates using the tensile speed mutation method; m reached its maximum value 0.53 at an initial strain rate of 1×10^-4s^-1 at 1253K. The diffusion bonding parameters, including the bonding temperature T, pressure p, and time t, affected the mechanism of joints. When the bonded specimen with 25μm thick nickel foil interlayer was tensile at room temperature, the shear fracture of the joints with nickel foil interlayer took place at the IN718 part. Microstructure study was carried out with the bonded samples. The microstructure shows an excellent bonding at the interfaces. The optimum parameters for the diffusion bonding are： T = 1273-1323K, p = 20-30MPa, t = 45-60min.

Microstructure and mechanical properties in the TLP joint of FeCoNiTiAl and Inconel 718 alloys using BNi2 filler

High entropy alloy(HEA) of Fe Co Ni Ti Al and Inconel 718 superalloy were firstly transient liquid phase(TLP) bonded by BNi2 filler due to the diffusion of Si and B in the filler to the base metals. The effects of bonding time on microstructure evolution and mechanical properties of the TLP joints were investigated.Owing to the complete isothermal solidification of the joints bonded for 30 min 120 min at 1100°C,no athermally solidified zones(ASZs) formed by eutectic phases were observed in the welded zone. Thus the TLP joints were only composed by the isothermally solidified zone(ISZ) and two diffusion affected zone(DAZ) adjacent to the dissimilar base metals and the negative effect of the ASZ on joint properties can be avoided. In addition, the increase of the bonding time can also make the Ti B2 borides precipitated in the DAZ near HEA and the brittle borides or carbides in the DAZ near IN718 alloy decrease and reduce the possibility of the stress concentration happened in the joints under loading. Therefore, the highest shear strength(632.1 MPa) of the TLP joints was obtained at 1100°C for 120 min, which was higher than that of the joint bonded for 30 min, 404.2 MPa. Furthermore, the extension of the bonding time made the fracture mechanism of the joint be transformed from the intergranular fracture to the transgranular fracture. However, as the brittle borides in the DAZ near IN718 can not be eliminated completely and refining of grains also happened in such region, all the TLP joints fractured inner the DAZ near IN718 alloy.

Interfacial reaction mechanism of TiBw/Ti6Al4V composites and Inconel 718 alloys by GTAW heat transmission

A good joint of Ti Bw/Ti6Al4V composites and Inconel 718 alloys was obtained by Gas Tungsten Arc Welding(GTAW) heat transmission. The interfacial reaction mechanism of joint was investigated and analyzed in details. Owing to the heat input applied on the surface of Ti Bw/Ti6Al4V composites, a solid-state reaction layer appeared at the interface of Ti Bw/Ti6Al4 V composites to Inconel 718 alloys. The thickness of the reaction layer was obviously increased with increasing heat input.Developing of reaction layer mainly depended on the diffusion of elements of Ti and Ni through the interface during welding to form solid solutions and intermetallic compounds(IMCs). The reaction layer can be divided into Ti-rich zone(layer 2) and Nirich zone(layer 1). In Ni-rich zone, relatively coarse dendrites were the predominant, however, more brittle IMCs like Ti2Ni were found in the Ti-rich zone. Micro hardness of reaction layer was much higher than that of base metal. While a slight decrease of hardness was found between Ti-rich zone and Ni-rich zone due to the formation of TiNi.

Effects of Carbon Content on Mechanical Properties of Inconel 718 Alloy

For improving the service performance of Inconel 718 alloy, especially used as a corrosion-resistant alloy for special environment, the microstructure and mechanical property of different carbon-containing Inconel 718 alloys were investigated by the Thermo-Calc software and experiments. The experimental results indicated that the mor- phology, distribution and types of carbides mainly existing in the form of MC＇were hardly influenced by solution treatment at 1050 ℃ for 1 h. The precipitation amount and particle size of carbides decreased with the decrease of carbon content, which was the main reason resulting in the increase of ductility and toughness. In addition, moving dislocation could be restrained by the precipitation of carbides. Therefore, the strength could benefit from the precip- itation strengthening of carbides when the precipitation of γ′/γ″ phase was not influenced by the precipitation of carbides.

Effects of current path on structure and segregation during electroslag remelting process of Inconel 718 alloy with same power input

Current-conductive mold was recently developed to extend electroslag remelting(ESR)functions to overcome some solidification defects by changing the current path.The macrostructures,microstructures,macrosegregation,and microsegregation of the Inconel 718 ingots produced by the custom laboratory-scale ESR furnace under different current paths(the classical ESR and the single power,and two circuits ESR process with current-conductive mold(ESR-STCCM))with the same power input were compared and investigated.The results indicate that when the ingot was produced during ESR and ESR-STCCM processes,at the same power input,the pool depth was 104 and 90 mm,respectively.A flatter and shallower molten pool was obtained during ESR-STCCM process.Moreover,compared with a classical ESR ingot,the cooling rate of the centerline of ESR-STCCM ingot was increased from 12.7 to 16.7 K min^(−1).The increased cooling rates caused by decreased melting rate and thinner slag skin reduced the growth angle of columnar crystal to the vertical axis and the secondary dendrite arm spacing.Furthermore,the macrosegregation and microsegregation of segregation elements for ESR-STCCM process were dramatically reduced compared with ESR process.The average volume fraction of Laves phase was reduced from 7.39%to 6.14%,and the segregation of Nb in Laves phase was significantly reduced.

Effect of Heat Treatment on the Microstructure and Mechanical Properties of the Modified 718 Alloy

M718 alloy with an extra high Mo content of 7.50 wt% which reduced Nb addition and increased A1 and Ti additionswithin the composition specifications of 718 alloy has been designed to increase the service temperature of 718 alloy. Andthe effect of the heat treatment on the microstructure and mechanical properties of M718 alloy has been investigated in thisstudy. The results showed that Laves phase precipitated on the grain boundaries of M718 alloy instead of 6-Ni3Nb phase in718 alloy, and γ″ and γ′ phases precipitated in the matrix of M718 alloy as that in 718 alloy. Increasing the solutiontemperature from 960 to 1050 ℃ noticeably reduced the intergranular precipitation of Laves phase. The precipitation ofLaves phase was appropriate at 1020 ℃ for improving the grain boundary cohesion. Increasing the two-stage agingtemperatures markedly increased the sizes of γ″ and γ′ phases. As a result, the strength of M718 alloy increased.

Effect of Precipitation on the Microhardness Distribution of Diode Laser Epitaxially Deposited IN718 Alloy Coating

The microhardness distribution of the diode laser epitaxially deposited IN718 alloy coating was investigated. The Laves concentration in different regions of the coating was measured by binarization processing. The strengthening phase of the coating was characterized by transmission electron microscopy （TEM）. The results showed that the microhardness increased along the depth of the coating. Part of Laves dissolved into austenitic matrix during the successive laser deposition, A little amount of strengthening phase was precipitated in the bottom region of the coating. It was attributed to the heat effect from the thermal cycle of successive deposition on the microstructure in the bottom region of the epitaxially deposited coating.

Introduction of a New Method for Regulating Laves Phases in Inconel 718 Superalloy during a Laser-Repairing Process

The morphology,size,and distribution of Laves phases have important influences on the mechanical properties of laser-repaired Inconel 718(IN718)superalloy.Due to the deterioration of the substrate zone,the Laves phase in the laser cladding zone of IN718 superalloy cannot be optimized by a hightemperature solution treatment.In this study,an in situ laser heat-treatment method was proposed to regulate the morphology and size of the Laves phase in the laser cladding zone of IN718 superalloy without impacting the substrate zone.In the in situ laser heat-treatment process,a laser was used to heat previously deposited layers with optimized manufacturing parameters.A thermocouple and an infrared camera were used to analyze thermal cycles and real-time temperature fields,respectively.Microstructures and micro-segregations were observed by optical microscopy,scanning electron microscopy,and electron probe microanalysis.It was found that the in situ laser heat treatment effectively changed the morphology and size of the Laves phase,which was transformed from a continuous striplike shape to a discrete granular shape.The effective temperature range and duration were the two main factors influencing the Laves phase during the in situ laser heat-treatment process.The effective temperature range was determined by the laser linear energy density,and the peak temperature increased with the increase of the linear energy density.In addition,the temperature amplitude could be reduced by simultaneously increasing the laser power and the scanning velocity.Finally,a flow diagram was developed based on the in situ laser heat-treatment process,and the deposition of a single-walled sample with fine and granular Laves phases was detected.

Phase-field simulation of lack-of-fusion defect and grain growth during laser powder bed fusion of Inconel 718

The anisotropy of the structure and properties caused by the strong epitaxial growth of grains during laser powder bed fusion(L-PBF)significantly affects the mechanical performance of Inconel 718 alloy components such as turbine disks.The defects(lack-of-fusion Lo F)in components processed via L-PBF are detrimental to the strength of the alloy.The purpose of this study is to investigate the effect of laser scanning parameters on the epitaxial grain growth and LoF formation in order to obtain the parameter space in which the microstructure is refined and LoF defect is suppressed.The temperature field of the molten pool and the epitaxial grain growth are simulated using a multiscale model combining the finite element method with the phase-field method.The LoF model is proposed to predict the formation of LoF defects resulting from insufficient melting during L-PBF.Defect mitigation and grain-structure control during L-PBF can be realized simultaneously in the model.The simulation shows the input laser energy density for the as-deposited structure with fine grains and without LoF defects varied from 55.0–62.5 J·mm^(-3)when the interlayer rotation angle was 0°–90°.The optimized process parameters(laser power of 280 W,scanning speed of 1160 mm·s^(-1),and rotation angle of 67°)were computationally screened.In these conditions,the average grain size was 7.0μm,and the ultimate tensile strength and yield strength at room temperature were(1111±3)MPa and(820±7)MPa,respectively,which is 8.8%and10.5%higher than those of reported.The results indicating the proposed multiscale computational approach for predicting grain growth and Lo F defects could allow simultaneous grain-structure control and defect mitigation during L-PBF.