Mechanism of microarc oxidation on AZ91D Mg alloy induced byβ-Mg_(17)Al_(12) phase

This work proposed a strategy of indirectly inducing uniform microarc discharge by controlling the content and distribution ofβ-Mg_(17)Al_(12)phase in AZ91D Mg alloy.Two kinds of nano-particles(ZrO_(2)and TiO_(2))were designed to be added into the substrate of Mg alloy by friction stir processing(FSP).Then,Mg alloy sample designed with different precipitated morphology ofβ-Mg_(17)Al_(12)phase was treated by microarc oxidation(MAO)in Na_(3)PO_(4)/Na2SiO3electrolyte.The characteristics and performance of the MAO coating was analyzed using scanning electron microscopy(SEM),energy dispersive spectrometer(EDS),X-ray diffraction(XRD),X-ray photoelectron spectroscopy(XPS),contact angle meter,and potentiodynamic polarization.It was found that the coarseα-Mg grains in extruded AZ91D Mg alloy were refined by FSP,and theβ-Mg_(17)Al_(12)phase with reticular structure was broken and dispersed.The nano-ZrO_(2)particles were pinned at the grain boundary by FSP,which refined theα-Mg grain and promoted the precipitation ofβ-Mg_(17)Al_(12)phase in grains.It effectively inhibited the“cascade”phenomenon of microarcs,which induced the uniform distribution of discharge pores.The MAO coating on Zr-FSP sample had good wettability and corrosion resistance.However,TiO_(2)particles were hardly detected in the coating on TiFSP sample.

Effect of pre-deformation on precipitation behavior of AZ80 alloy:Comparison of slip-and twinning-dominant deformation

This study investigates the effect of the deformation mode on the precipitation behavior of an extruded Mg-8.0Al-0.5Zn-0.2Mn(AZ80)alloy.The alloy samples are compared after the application of 3.5%tension and 3.5%compression along the extrusion direction to induce slip-dominant and twinning-dominant deformation modes,respectively.The pre-compressed(PC)sample,which contained numerous{10-12}tension twins,has a reduced grain size and a higher internal strain than the pre-tensioned(PT)sample,which is attributed to the inherent internal strain that occurs during the formation and growth of the twins.As a result,the precipitation behavior of the PC sample is accelerated,leading to its short peak aging time of 32 h,which is lower than those of the PT and as-extruded samples(48 and 100 h,respectively).Furthermore,fine continuous precipitates(CPs)rapidly form within the{10-12}twins,contributing to the enhanced hardness.Discontinuous precipitates(DPs),which have a hardness comparable to the CP-containing twinned regions,in the PC sample experience less coarsening during aging than those in the PT sample due to growth inhibition by the{10-12}twins.Ultimately,the{10-12}twins generated under the twinning-dominant deformation condition lead to enhanced precipitation behaviors,including the preferential formation and refinement of CPs and the suppressed coarsening of DPs.Consequently,pre-deformation that occurs{10-12}twinning exhibits more pronounced effects on precipitation acceleration and microstructural modification than slip-inducing pre-deformation.

Effect of addition temperature on dispersion behavior and grain refinement efficiency of MgO introduced into Mg alloy

The effect of addition temperature of MgO particles(MgOp)on their dispersion behavior and the efficiency of grain refinement in AZ31 Mg alloy was investigated.In addition,the grain refinement mechanism was systematically studied by microstructure characterization,thermodynamic calculation,and analysis of solidification curves.The results show that the grain size of AZ31 Mg alloy initially decreases and then increases as the MgOp addition temperature is increased from 720 to 810℃,exhibiting a minimum value of 136μm at 780℃.The improved grain refinement efficiency with increasing MgOp addition temperature can be attributed to the reduced Mg melt viscosity and enhanced wettability between MgOp and Mg melt.Furthermore,a corresponding physical model describing the solidification behavior and grain refinement mechanism was proposed.

Microstructural evolution and mechanical properties of AZ31 Mg alloy fabricated by a novel bifurcation-equal channel angular pressing

In this work,a novel type of short-process deformation technology of Mg alloys,bifurcation-equal channel angular pressing(B-ECAP),was proposed to refine grain and improve the basal texture.The cylindrical billets were first compressed into the die cavity,then sequentially flowed downward through a 90°corner and two 120°shear steps.The total strain of B-ECAP process could reach 3.924 in a single pass.The results of microstructure observation showed that DRX occurred at upsetting process in the die cavity and completed at position D.The grains were refined to 6.3μm at being extruded at 300℃ and grew obviously with the extrusion temperature increase.The shear tress induced by 900 corner and two 120°shear steps resulted in the basal poles of most grains tilted to extrusion direction(ED)by±25°.Compared with the original billets,the extruded sheets exhibited higher yield strengths(YS),which was mainly attributed to the grain refinement.The higher Schmid factor caused by ED-tilt texture resulted in a fracture elongation(FE)more than that of the original bar in ED,while was equivalent to that in transverse direction(TD).As the extrusion temperature increased,the variation of UTS and YS in ED and TD decreased gradually without ductility obviously decrease.

Study of HCP→FCC phase transformation mechanism under different hot compression rates of AZ31 magnesium alloy

At present,there are few studies on the phase transition during the thermocompression plastic deformation of magnesium alloy.In this study,the evolution model of thermal compression plastic of AZ31 magnesium alloy was constructed by molecular dynamics,and the phase transition relationship between HCP and FCC at different thermal compression rates was studied.By combining GLEEBLE thermal compression experiment with transmission electron microscopy experiment,high-resolution transmission electron microscopy images were taken to analyze the transition rules between HCP and FCC during plastic deformation at different thermal compression rates,and the accuracy of molecular dynamics analysis was verified.It is found that the slip of Shockley’s incomplete dislocation produces obvious HCP→FCC phase transition at low strain rate and base plane dislocation at high strain rate,which makes the amorphous phase transition of HCP→OTHER more obvious,which provides theoretical guidance for the formulation of forming mechanism and preparation process of magnesium alloy.

NaF assisted preparation and the improved corrosion resistance of high content ZnO doped plasma electrolytic oxidation coating on AZ31B alloy

In the present research,the NaF assisted plasma electrolytic oxidation(PEO)is designed to fabricate the high-content ZnO nanoparti-cles doped coating on AZ31B alloy.The microstructure,phase constituents and corrosion behavior of the PEO coatings are investigated systematically.The results reveal that the introduction of NaF promotes the formation of MgF2 nanophases in the passivation layer on Mg alloy,decreasing the breakdown voltage and discharge voltage.As a result,the continuous arcing caused by high discharge voltage is alleviated.With the increasing of NaF content,the Zn content in the PEO coating is enhanced and the pore size in the coating is decreased correspondingly.Due to the high-content ZnO doping,the PEO coating protected AZ31B alloy demonstrates the better corrosion resistance.Compared with the bare AZ31B alloy,the high-content ZnO doped PEO coated sample shows an increased corrosion potential from-1.465 V to-1.008 V,a decreased corrosion current density from 3.043×10^(-5) A·cm^(-2) to 3.960×10^(-8) A·cm^(-2) and an increased charge transfer resistance from 1.213×10^(2) ohm·cm^(2) to 2.598×10^(5) ohm·cm^(2).Besides,the high-content ZnO doped PEO coated sample also has the excellent corrosion resistance in salt solution,exhibiting no obvious corrosion after more than 2000 h neutral salt spraying and 28 days’immersion testing.The improved corrosion resistance can be ascribed to the relative uniform distribution of ZnO in PEO coating which can transform to Zn(OH)2 and form a continuous protective layer along the corrosion interface.

Experimental and simulation research on hollow AZ31 magnesium alloy three-channel joint by hot extrusion forming with sand mandrel

Magnesium alloy is one of the lightest metal structural materials.The weight is further reduced through the hollow structure.However,the hollow structure is easily damaged during processing.In order to maintain the hollow structure and to transfer the stresses during the high temperature deformation,the sand mandrel is proposed.In this paper,the hollow AZ31 magnesium alloy three-channel joint is studied by hot extrusion forming.Sand as one of solid granule medium is used to fill the hollow magnesium alloy.The extrusion temperatures are 230℃ and 300℃,respectively.The process parameters(die angle,temperature,bottom thickness,sidewall thickness,edge-to-middle ratio in bottom,bottom shape)of the hollow magnesium alloy are analyzed based on the results of experiments and the finite element method.The results are shown that the formability of the hollow magnesium alloy will be much better when the ratio of sidewall thickness to the bottom thickness is 1:1.5.Also when edge-to-middle ratio in bottom is about 1:1.5,a better forming product can be received.The best bottom shape in these experiments will be convex based on the forming results.The grain will be refined obviously after the extrusion.Also the microstructures will be shown as streamlines.And these lines will be well agreement with the mold in the corner.

Enhancing fatigue performance of AZ31 magnesium alloy components fabricated by cold metal transfer-based wire arc directed energy deposition through LPB

Cold Metal Transfer-Based Wire Arc Directed Energy Deposition(CMT-WA-DED)presents a promising avenue for the rapid fabrication of components crucial to automotive,shipbuilding,and aerospace industries.However,the susceptibility to fatigue of CMT-WA-DED-produced AZ31 Mg alloy components has impeded their widespread adoption for critical load-bearing applications.In this study,a comprehensive investigation into the fatigue behaviour of WA-DED-fabricated AZ31 Mg alloy has been carried out and compared to commercially available wrought AZ31 alloy.Our findings indicate that the as-deposited parts exhibit a lower fatigue life than wrought Mg alloy,primarily due to poor surface finish,tensile residual stress,porosity,and coarse grain microstructure inherent in the WA-DED process.Low Plasticity Burnishing(LPB)treatment is applied to mitigate these issues,which induce significant plastic deformation on the surface.This treatment resulted in a remarkable improvement of fatigue life by 42%,accompanied by a reduction in surface roughness,grain refinement and enhancement of compressive residual stress levels.Furthermore,during cyclic deformation,WA-DED specimens exhibited higher plasticity and dislocation density compared to both wrought and WA-DED+LPB specimens.A higher fraction of Low Angle Grain Boundaries(LAGBs)in WA-DED specimens contributed to multiple crack initiation sites and convoluted crack paths,ultimately leading to premature failure.In contrast,wrought and WA-DED+LPB specimens displayed a higher percentage of High Angle Grain Boundaries(HAGBs),which hindered dislocation movement and resulted in fewer crack initiation sites and less complex crack paths,thereby extending fatigue life.These findings underscore the effectiveness of LPB as a post-processing technique to enhance the fatigue performance of WA-DED-fabricated AZ31 Mg alloy components.Our study highlights the importance of LPB surface treatment on AZ31 Mg components produced by CMT-WA-DED to remove surface defects,enabling their widespread use in load-bearing applications.

Microstructure and mechanical properties of GTA-based wire arc additive manufactured AZ91D magnesium alloy

Wire arc additive manufacturing offers advantages in producing large metal structures.The current research on GTA-based wire arc additive manufacturing(GTA-WAAM)of magnesium alloys is focused on deformed magnesium alloys,mainly on the Mg-Al alloy system.However,there is little research on GTA-WAAM for casting magnesium alloy.This study investigates the microstructural characteristics and mechanical properties of AZ91D magnesium alloy(AZ91D-Mg)deposited by GTA-WAAM.Single-pass multilayer thin-walled components were successfully fabricated.The results show that equiaxed grains dominate the microstructure of the deposited samples.During the remelting process,the precipitated phases dissolve into the matrix,and they precipitate and grow from the matrix under the thermal effect of the subsequent thermal cycle.The mechanical properties in the vertical and horizontal directions are similar,showing higher overall mechanical properties than the casting parts.The average yield strength is 110.5 MPa,the ultimate tensile strength is 243.6 MPa,and the elongation is 11.7%.The overall hardness distribution in the deposited sample is relatively uniform,and the average microhardness is 59.6 HV_(0.2).

Hot tearing behavior of AZ91D magnesium alloy

Hot tearing is a serious destructive solidification defect of magnesium alloys and other casting metals.Quantitative and controllable measurements on the thermal and the mechanical behavior of an alloy during its solidification process are crucial for the understanding of hot tearing formation.We developed a new experimental method and setup to characterize hot tearing behavior via controlled cooling and active loading to force hot hearing formation on cooling at selected fractions of solid.The experimental setup was fully instrumented so that stress,strain,strain rate,and temperature can be measured in-situ while hot tearing was developing.An AZ91D magnesium alloy,which is prone to hot tearing,was used in this study.Results indicate that when hot hearing occurred,the local temperature,critical stress,and cumulative strain were directly affected by strain rate.Depending on the applied strain rate,hot tearing of the AZ91D magnesium alloy could occur in two solidification stages:one in the dendrite solidification stage(fS∼0.81-0.82)and the other in the eutectic solidification stage(fS∼0.99).AZ91D alloy exhibited distinct mechanical behaviors in these two ranges of fraction solid.

Mechanical Evaluation of AZ80 Magnesium Alloy in Cast Wrought Form

Wrought magnesium alloy AZ80 with a thick section of 20 mm was prepared by squeeze casting (SC) and permanent steel mold casting (PSMC). The porosity measurements of the SC and PSMC depicted that SC AZ80 had a pore content of 0.52%, which was 77% lower than 2.21% of PSMC AZ80 counterpart. The YS, UTS, ef, E and strengthening rate of cast AZ80 were determined by mechanical pulling. The engineering stress versus strain bended lines showed that SC AZ80 had a YS of 84.7 MPa, a UTS of 168.2 MPa, 5.1% in ef, and 25.1 GPa in modulus. But, the YS, UTS and ef of the PSMC AZ80 specimen were only 71.6 MPa, 109.0 MPa, 1.9% and 21.9 GPa. The findings of the mechanical pulling evidently depicted that the YS, UTS, ef and E of SC AZ80 were 18%, 54%, 174% and 15% higher than PSMC counterpart. The computed resilience and toughness suggested that the SC AZ80 exhibited greater resistance to tensile loads during elastic deformation and possessed higher capacity to absorb energy during plastic deformation compared to the PSMC AZ80. At the beginning of permanent change, the strengthening rate of SC AZ80 was 10,341 MPa, which was 9% greater than 9489 MPa of PSMC AZ80. The high mechanical characteristics of SC AZ80 should be primarily attributed to its low porosity level. .

Effect of grain refinement induced by wire and arc additive manufacture (WAAM) on the corrosion behaviors of AZ31 magnesium alloy in NaCl solution

Additive manufacturing(AM)of Mg alloys has become a promising strategy for producing complex structures,but the corrosion performance of AM Mg components remains unexploited.In this study,wire and arc additive manufacturing(WAAM)was employed to produce single AZ31 layer.The results revealed that the WAAM AZ31 was characterized by significant grain refinement with non-textured crystallographic orientation,similar phase composition and stabilized corrosion performance comparing to the cast AZ31.These varied corrosion behaviors were principally ascribed to the size of grain,where cast AZ31 and WAAM AZ31 were featured by micro galvanic corrosion and intergranular corrosion,respectively.

Influence of bimodal non-basal texture on microstructure characteristics,texture evolution and deformation mechanisms of AZ31 magnesium alloy sheet rolled at liquid-nitrogen temperature

Cryogenic rolling experiments have been conducted on the AZ31 magnesium(Mg)alloy sheet with bimodal non-basal texture,which is fabricated via the newly developed equal channel angular rolling and continuous bending process with subsequent annealing(ECAR-CB-A)process.Results demonstrate that this sheet shows no edge cracks until the accumulated thickness reduction reaches about 18.5%,which is about 105.6%larger than that of the sheet with traditional basal texture.Characterization experiments including optical microstructure(OM),X-ray diffractometer(XRD),and electron backscatter diffraction(EBSD)measurements are then performed to explore the microstructure characteristics,texture evolution and deformation mechanisms during cryogenic rolling.Experimental observations confirm the occurrence of abundant{10–12}extension twins(ETs),twin-twin interactions among{10–12}ET variants and{10–12}-{10–12}double twins(DTs).The twinning behaviors as for{10–12}ETs are responsible for the concentration of c-axes of grains towards normal direction(ND)and the formation of transverse direction(TD)-component texture at the beginning of cryogenic rolling.The twinning behaviors with respect to{10–12}-{10–12}DTs are responsible for the disappearance of TD-component texture at the later stage of cryogenic rolling.The involved deformation mechanisms can be summarized as follows:Firstly{10–12}ETs dominate the plastic deformation.Subsequently,dislocation slip,especially basal<a>slip,starts to sustain more plastic strain,while{10–12}ETs occur more frequently and enlarge continuously,resulting in the formation of twin-twin interaction among{10–12}ET variants.With the increasing rolling passes,{10–12}-{10–12}DTs incorporate in the plastic deformation and dislocation slip serves as the major one to sustain plastic strain.The activities of basal<a>slip,{10–12}ETs and{10–12}-{10–12}DTs benefit in accommodating the plastic strain in sheet thickness,which contributes to the improved rolling formability in AZ31 Mg alloy sheet with bimodal non-basal texture during cryogenic rolling.

Corrosion resistance and electrical conductivity of V/Ce conversion coating on magnesium alloy AZ31B

A V/Ce conversion coating was deposited in the surface of AZ31B magnesium alloy in a solution containing vanadate and cerium nitrate.The coating composition and morphology were examined.The conversion coating appears to consist of a thin and cracked coating with a scattering of spherical particles.The corrosion behavior of the substrate and conversion coating was studied by potentiodynamic polarization and electrochemical impedance spectroscopy (EIS).Compared with AZ31B magnesium alloy,the corrosion current density of the conversion coating is decreased by two orders of magnitude.The total impedance of the V/Ce conversion coating rise to 1.6×10^(3)Ω·cm^(2)in contrast with2.2×10^(2)Ω·cm^(2)of the bare AZ31B.In addition,the electrical conductivity of the coating was assessed by conductivity meter and Mott-Schottky measurement.The results reveal a high dependence of the conductivity of the coating on the semiconductor properties of the phase compositions.

Acceleration of aging behavior and improvement of mechanical properties of extruded AZ80 alloy through(10–12) twinning

The effects of pre-existing {10–12} extension twins on the precipitation behavior of an extruded AZ80 material during aging and on its mechanical properties after peak aging are investigated. The material containing {10–12} twins-which are formed by compression before aging(twinned material)-has a finer grain size and higher dislocation density than the extruded material. Although the peak hardnesses of the twinned and extruded materials are almost the same, the time to reach the peak hardness is considerably shorter in the former material than in the latter(4 h and 24 h, respectively). In the twinned material, the high dislocation density of the {10–12} twins promotes continuous precipitation, which results in the formation of numerous fine Mg17Al12precipitates within the twins in the early stage of aging.The formation of these continuous precipitates reduces the driving force for discontinuous precipitation, which consequently suppresses the formation and growth of coarse Mg17Al12precipitates at the grain boundaries. Despite its shorter peak-aging time, the 4 h-peak-aged twinned material shows higher tensile strength and elongation than the 24 h-peak-aged extruded material. These higher mechanical properties of the former material are attributed primarily to the presence of more abundant fine continuous precipitates, which are effective in strengthening the material, and less abundant coarse discontinuous precipitates, which can act as crack initiation sites. These results demonstrate that the introduction of {10–12} twins into wrought Mg–Al-based alloys can accelerate the Mg17Al12precipitation kinetics considerably and improve the strength and ductility of the peak-aged alloys simultaneously.

Molecular dynamics study on the effect of temperature on HCP→FCC phase transition of magnesium alloy

To explore the effect of temperature on the phase transformation of HCP→FCC during compression, the uniaxial compression process of AZ31 magnesium alloy was simulated by the molecular dynamics method, and the changes of crystal structure and dislocation evolution were observed. The effects of temperature on mechanical properties, crystal structure, and dislocation evolution of magnesium alloy during compression were analyzed. It is concluded that some of the Shockley partial dislocation is related to FCC stacking faults. With the help of TEM characterization, the correctness of the correlation between some of the dislocations and FCC stacking faults is verified. Through the combination of simulation and experiment, this paper provides an idea for the in-depth study of the solid-phase transformation of magnesium alloys and provides reference and guidance for the design of magnesium alloys with good plasticity and formability at room temperature.

Fabrication of chitosan/silica hybrid coating on AZ31 Mg alloy for orthopaedic applications

Biocompatible conversion of chitosan and chitosan/silica hybrid coating were prepared to enhance the biocompatibility and corrosion resistance of biodegradable AZ31 Mg alloy. The coatings were optimized and analysed with potentiodynamic polarization, SEM, ATR-IR and XPS studies. Potentiodynamic polarization studies, revealed that the coatings exhibited high corrosion resistance. The surface morphology of the Ch-3/Si coating showed small globular rough structure. The presence of functional groups was confirmed by ATR-IR. For a better understanding of chitosan/silica hybrid coating, the chemical states were examined by XPS studies. The in-vitro bioactivity of the coated samples was evaluated in Earle’s solution, which formed a dense layer of coral-like structure and calcium-deficient apatite with less stoichiometric ratio than the hydroxyapatite. In-vitro cell culture studies exhibited a good cell proliferation rate and the fabricated Ch-3/Si coating was found to be non-hemolytic. The bacterial studies proved that Ch-3/Si coating possessed inherent antibacterial activity.

Edge crack damage analysis of AZ31 magnesium alloy hot-rolled plate improved by vertical roll pre-rolling

In the present study,through vertical roll pre-rolling of AZ31 magnesium alloy hot-rolled plate at room temperature,the effect of different vertical roll pre-rolling reduction on edge crack of the plate during flat rolling was systematically studied.The evolution of microstructure and texture in the edge and middle of the plate after vertical roll pre-rolling,heating and rolling was analyzed by using EBSD technology.The results show that during the vertical roll pre-rolling,{10–12}primary twins and{10–12}-{10–12}secondary twins dominated the edge deformation,while{10–12}primary twins dominated the middle deformation.With the increase of vertical roll pre-rolling reduction,the twin volume fraction of the edge and the middle increased,and the difference between them decreased gradually.After heating,the twin orientation caused by vertical roll pre-rolling was still maintained,and there was a significant difference in grain size between the edge and the middle.When the reduction rate of flat rolling was 30%,cracks have already appeared in the initial plate,while the vertical roll pre-rolled samples showed extremely high rolling performance.When the reduction rate of flat rolling was 50%,the 8PR sample still had no crack initiation.In addition,after flat rolling of 50%,the initial plate showed a strong basal texture,while the maximum pole density of the 8PR plate was small,and the texture distribution was very scattered,showing the characteristics of weak orientation.

Effects of surface roughness on bending properties of rolled AZ31 alloy

This study investigated the effects of mechanical-polishing-induced surface roughness and the direction of polishing lines on the bending properties of a rolled AZ31 alloy.To this end,three-point bending tests were performed on one sample without polishing lines(SS sample)and two samples with polishing lines—one in which the polishing lines were parallel to the rolling direction(RS-RD sample)and the other in which they were parallel to the transverse direction(RS-TD sample).In all three samples,macrocracks were formed in the width direction on the outer surface,where tensile stress was predominantly generated in the longitudinal direction.However,the macrocracks formed in the SS sample were curved because of the merging of uniformly formed fine microcracks,whereas those formed in the RS-TD sample were linear owing to the formation of relatively coarse microcracks along the polishing lines.The bendability of the samples was in the order of SS>RS-RD>RS-TD,and their limiting bending depths were 4.8,4.6,and 4.4 mm,respectively.In the presence of mechanical-polishing-induced surface roughness,polishing lines perpendicular to the direction of the major stress(i.e.,tensile stress along the longitudinal direction)resulted in a greater degree of stress concentration on the outer surface of the bending specimen.This higher stress concentration promoted the formation of undesirable{10–11}contraction and{10–11}–{10–12}double twins—which typically act as crack initiation sites—and thereby facilitated crack generation and propagation.Consequently,the surface roughness caused premature fracture during bending deformation,which,in turn,caused deterioration of the bendability of the rolled Mg alloy.

Effects of aging treatment processes on microstructures and mechanical properties of AZ63 casting magnesium alloy

The effects of three different aging treatment processes,namely single-stage,double-stage,and reverse double-stage aging treatment processes,on the microstructures and mechanical properties of the AZ63(Mg-6Al-3Zn-0.25Mn)casting magnesium alloy were investigated and compared.The results indicate that the microstructures of all the aged alloys under the three treatment processes are mainly composed ofα-Mg,Mg17Al12),and Al4Mn phases,indicating that the double-stage and reverse double-stage aging treatments have no obvious effect on the type of alloy phases.However,as compared with the single-stage and double-stage processes,the reverse double-stage process has a great effect on the quantity of the Mg17Al12phases.After the reverse double-stage aging treatment,which results in a stronger drive for decomposition of the supersaturated solid solution,the number of Mg17Al12phases precipitated in the grains significantly increases.In addition,as compared with the single-stage aged alloy,the tensile properties at room temperature for both the double-stage and reverse double-stage aged alloys are significantly improved.Among them,the reverse double-stage aged alloy achieves the highest tensile strength,yield strength,and elongation of 295 MPa,167 MPa,and 8.6%,respectively.