建立了全自动石墨消解-火焰原子吸收法,对安徽省耕地质量调查中青阳地区农田土壤的锌进行了样品消解和分析检测,土壤消解体系采用1.5 m L HNO3-4.5 mL HCl-3 mL HF-1 m L HClO4进行,通过设定的消解程序完成对土壤样品消解后在火焰原子...建立了全自动石墨消解-火焰原子吸收法,对安徽省耕地质量调查中青阳地区农田土壤的锌进行了样品消解和分析检测,土壤消解体系采用1.5 m L HNO3-4.5 mL HCl-3 mL HF-1 m L HClO4进行,通过设定的消解程序完成对土壤样品消解后在火焰原子吸收分光光度计上对Zn的测定,通过对土壤标准物质GBW 07385、GBW 07387、GBW 07388的测定,结果表明,其测定结果平均值与认定值相吻合,精密度符合要求。将优化后的测量方法用于青阳地区农田土壤实际样品测定,其结果与平行实验室间测定平均值的对比结果线性相关性极显著,证明了该方案的有效性。展开更多
Electrochemical machining (ECM) is one of the best al ternatives for producing complex shapes in advanced materials used in aircraft a nd aerospace industries. However, the reduction of the stray material removal co n...Electrochemical machining (ECM) is one of the best al ternatives for producing complex shapes in advanced materials used in aircraft a nd aerospace industries. However, the reduction of the stray material removal co ntinues to be major challenges for industries in addressing accuracy improvement . This study presents a method of improving machining accuracy in ECM by using a dual pole tool with a metallic bush outside the insulated coating of a cathode tool. The bush is connected with anode and so the electric field at the side gap area is substantially weakened. The modeling and simulation indicate that the p ositive bush brings down the current density at the side gap area of the machine d hole and hence reduces the stray material removal there. It has been experimen tally observed that the machining accuracy and the process stability are signifi cantly improved.展开更多
文摘建立了全自动石墨消解-火焰原子吸收法,对安徽省耕地质量调查中青阳地区农田土壤的锌进行了样品消解和分析检测,土壤消解体系采用1.5 m L HNO3-4.5 mL HCl-3 mL HF-1 m L HClO4进行,通过设定的消解程序完成对土壤样品消解后在火焰原子吸收分光光度计上对Zn的测定,通过对土壤标准物质GBW 07385、GBW 07387、GBW 07388的测定,结果表明,其测定结果平均值与认定值相吻合,精密度符合要求。将优化后的测量方法用于青阳地区农田土壤实际样品测定,其结果与平行实验室间测定平均值的对比结果线性相关性极显著,证明了该方案的有效性。
文摘Electrochemical machining (ECM) is one of the best al ternatives for producing complex shapes in advanced materials used in aircraft a nd aerospace industries. However, the reduction of the stray material removal co ntinues to be major challenges for industries in addressing accuracy improvement . This study presents a method of improving machining accuracy in ECM by using a dual pole tool with a metallic bush outside the insulated coating of a cathode tool. The bush is connected with anode and so the electric field at the side gap area is substantially weakened. The modeling and simulation indicate that the p ositive bush brings down the current density at the side gap area of the machine d hole and hence reduces the stray material removal there. It has been experimen tally observed that the machining accuracy and the process stability are signifi cantly improved.
