The loading tests of Fe 3Al under tensile impact have been carried out by a self designed rotating circular disk tensile impact apparatus. An experimental study of Fe 3Al in the strain rate range from 80 s -1 to 1 200...The loading tests of Fe 3Al under tensile impact have been carried out by a self designed rotating circular disk tensile impact apparatus. An experimental study of Fe 3Al in the strain rate range from 80 s -1 to 1 200 s -1 was performed and the complete stress strain curves under tensile impact were obtained. On the basis of the experimental results, it is believed that Fe 3Al obviously exists dynamic ductility and effect of strain rate hardening. The yield strength, ultimate strength and failure strain increase with increasing strain rate. Based on the linear least squares fit, the relationship between the yield strength, ultimate strength, failure strain and strain rate under tensile impact was obtained. At the same time, one dimensional macro constitutive equation for Fe 3Al under tensile impact according to the elastic viscoplastic constitutive theory was derived.展开更多
The influence of cooling rate and Fe-containing phases on Sr-modification of Si phases in hypoeutectic Al-Si alloys, a problem with great industrial importance, was investigated. The microstructures of samples were ex...The influence of cooling rate and Fe-containing phases on Sr-modification of Si phases in hypoeutectic Al-Si alloys, a problem with great industrial importance, was investigated. The microstructures of samples were examined using scanning electron microscopy(SEM) with energy-dispersive X-ray spectroscopy(EDX). A new method of electron probe microanalysis(EPMA) map scanning was used to analyze the Sr distribution, which gave quantitative results covering more Si particles. EPMA map scanning, together with SEM with EDX, was also used in analyzing the distribution of Fe phases. Results show that Fe-containing phase was related to the unmodified Si particles in samples with partial modification failure and the plate-like Si phases in samples without modification failure. Such a relationship was further confirmed by the microstructure observation.In conclusion, a partial failure of Sr-modification can be caused by both slow cooling rate and Fe-containing phases.展开更多
Al-20Si-5Fe melt was rapidly solidified into particles and ribbons and then consolidated to near full density by hot pressing at 400℃/250 MPa/1 h. According to the eutectic-growth and dendritic-growth velocity models...Al-20Si-5Fe melt was rapidly solidified into particles and ribbons and then consolidated to near full density by hot pressing at 400℃/250 MPa/1 h. According to the eutectic-growth and dendritic-growth velocity models, the solidification front velocity and the amount of undercooling were estimated for the particles with different sizes. Values of 0.43-1.2 cm/s and 15-28 K were obtained. The secondary dendrite arm spacing revealed a cooling rate of 6 × 10^5 K/s for the particles with an average size of 20 μm. Solidification models for the ribbons yielded a cooling rate of 5 × 10^7 K/s. As a result of the higher cooling rate, the melt-spun ribbons exhibited considerable microstructural refinement and modification. The size of the primary silicon decreased from approximately 1μm to 30 nm while the formation of iron-containing intermetallic compounds was suppressed. Supersaturation of the aluminum matrix in an amount of-7 at.% Si was noticed from the XRD patterns During the hot consolidation process, coarsening of the primary silicon particles and precipitation of β-Al5FeSi phase were observed. Evaluation of the compressive strength and hardness of the alloy indicated an improvement in mechanical properties due to the microstructural modification.展开更多
A self adjusting model was presented on the basis of the effect of temperature gradient on eutectic growth and a curved solid/liquid interface. Finite differential method was adopted to solve the model. The average la...A self adjusting model was presented on the basis of the effect of temperature gradient on eutectic growth and a curved solid/liquid interface. Finite differential method was adopted to solve the model. The average lamellar spacing of the Al Al 3Fe eutectic alloy and the content fields ahead of the solidifying interface under different growth rates were calculated. Directional solidification experiments were carried out in order to prove the modification of the modeling. The experimental results are in relatively good agreement with the calculations.展开更多
The 3D morphologies and growth mechanisms of proeutectic FeAl_(3) at the Al/Fe interface under different cooling rates were studied by synchrotron X-ray tomography.With increasing cooling rate,FeAl_(3) crystals develo...The 3D morphologies and growth mechanisms of proeutectic FeAl_(3) at the Al/Fe interface under different cooling rates were studied by synchrotron X-ray tomography.With increasing cooling rate,FeAl_(3) crystals developed from faceted polygonal prism,plates with flat surface,thin ribbon-like with periodic undulating surface to non-faceted rods with radial dendrites in cross section,indicating a gradual interface growth mode transition from two-dimensional layer growth to continuous growth.At a higher cooling rate,twinning mechanism plays a leading role in the formation and growth of FeAl_(3).A link between the morphologies,twinning and crystallographic structure was established based on quantitative analyses on the 3D structures.展开更多
文摘The loading tests of Fe 3Al under tensile impact have been carried out by a self designed rotating circular disk tensile impact apparatus. An experimental study of Fe 3Al in the strain rate range from 80 s -1 to 1 200 s -1 was performed and the complete stress strain curves under tensile impact were obtained. On the basis of the experimental results, it is believed that Fe 3Al obviously exists dynamic ductility and effect of strain rate hardening. The yield strength, ultimate strength and failure strain increase with increasing strain rate. Based on the linear least squares fit, the relationship between the yield strength, ultimate strength, failure strain and strain rate under tensile impact was obtained. At the same time, one dimensional macro constitutive equation for Fe 3Al under tensile impact according to the elastic viscoplastic constitutive theory was derived.
基金supported by the International Science & Technology Cooperation Program of China(No.2015DFR50470)
文摘The influence of cooling rate and Fe-containing phases on Sr-modification of Si phases in hypoeutectic Al-Si alloys, a problem with great industrial importance, was investigated. The microstructures of samples were examined using scanning electron microscopy(SEM) with energy-dispersive X-ray spectroscopy(EDX). A new method of electron probe microanalysis(EPMA) map scanning was used to analyze the Sr distribution, which gave quantitative results covering more Si particles. EPMA map scanning, together with SEM with EDX, was also used in analyzing the distribution of Fe phases. Results show that Fe-containing phase was related to the unmodified Si particles in samples with partial modification failure and the plate-like Si phases in samples without modification failure. Such a relationship was further confirmed by the microstructure observation.In conclusion, a partial failure of Sr-modification can be caused by both slow cooling rate and Fe-containing phases.
基金The authors wish to sincerely acknowledge the High Technology Industries Center, Iranian Ministry of Mines and Metals for financial support of the research work.
文摘Al-20Si-5Fe melt was rapidly solidified into particles and ribbons and then consolidated to near full density by hot pressing at 400℃/250 MPa/1 h. According to the eutectic-growth and dendritic-growth velocity models, the solidification front velocity and the amount of undercooling were estimated for the particles with different sizes. Values of 0.43-1.2 cm/s and 15-28 K were obtained. The secondary dendrite arm spacing revealed a cooling rate of 6 × 10^5 K/s for the particles with an average size of 20 μm. Solidification models for the ribbons yielded a cooling rate of 5 × 10^7 K/s. As a result of the higher cooling rate, the melt-spun ribbons exhibited considerable microstructural refinement and modification. The size of the primary silicon decreased from approximately 1μm to 30 nm while the formation of iron-containing intermetallic compounds was suppressed. Supersaturation of the aluminum matrix in an amount of-7 at.% Si was noticed from the XRD patterns During the hot consolidation process, coarsening of the primary silicon particles and precipitation of β-Al5FeSi phase were observed. Evaluation of the compressive strength and hardness of the alloy indicated an improvement in mechanical properties due to the microstructural modification.
文摘A self adjusting model was presented on the basis of the effect of temperature gradient on eutectic growth and a curved solid/liquid interface. Finite differential method was adopted to solve the model. The average lamellar spacing of the Al Al 3Fe eutectic alloy and the content fields ahead of the solidifying interface under different growth rates were calculated. Directional solidification experiments were carried out in order to prove the modification of the modeling. The experimental results are in relatively good agreement with the calculations.
基金supported by the National Natural Science Foundation of China-Excellent Young Scholars(No.51922068)National Natural Science Foundation of China(Nos.51821001,51904186,and 51904187)。
文摘The 3D morphologies and growth mechanisms of proeutectic FeAl_(3) at the Al/Fe interface under different cooling rates were studied by synchrotron X-ray tomography.With increasing cooling rate,FeAl_(3) crystals developed from faceted polygonal prism,plates with flat surface,thin ribbon-like with periodic undulating surface to non-faceted rods with radial dendrites in cross section,indicating a gradual interface growth mode transition from two-dimensional layer growth to continuous growth.At a higher cooling rate,twinning mechanism plays a leading role in the formation and growth of FeAl_(3).A link between the morphologies,twinning and crystallographic structure was established based on quantitative analyses on the 3D structures.