Semi-quantitative electron probe microanalysis （EPMA） mapping, scanning electron microscopy （SEM） and transmission electron microscopy （TEM） were employed to study the effect of one-step and two-step treatments ...Semi-quantitative electron probe microanalysis （EPMA） mapping, scanning electron microscopy （SEM） and transmission electron microscopy （TEM） were employed to study the effect of one-step and two-step treatments on the Zr distribution and Al3Zr dispersoid characteristics in as-cast commercial AA7150 aluminum alloy. It is shown that the Zr concentration in the dendrite centre regions is higher than that near the dendrite edges in the as-cast condition, and that homogenization at 460 °C for 20 h is insufficient to remove these concentration gradients. After homogenizing at 460-480 °C, a high number density of larger dispersoids can be observed in dendrite centre regions but not near dendrite edges. Furthermore, the dispersoid size increases with increasing the temperature during both one-step and two-step homogenization treatments.展开更多
以纳米ZrO 、微米Al O 为原料,采用无压烧结方式制备了ZTA 复相陶瓷。结果表明:nano-ZrO 的 2 2 3 2加入有利于制备细晶ZTA 复相陶瓷。此外,nano-ZrO 的加入对 Al O 陶瓷的显微结构也产生影响,ZrO ...以纳米ZrO 、微米Al O 为原料,采用无压烧结方式制备了ZTA 复相陶瓷。结果表明:nano-ZrO 的 2 2 3 2加入有利于制备细晶ZTA 复相陶瓷。此外,nano-ZrO 的加入对 Al O 陶瓷的显微结构也产生影响,ZrO 颗粒以 2 2 3 2“晶内型”和晶界型两种形式存在。合理的配方组成及制备工艺有利于 Z r O 以四方亚稳相存在。Z r O 含量为 2 23 0 w t % 时,其四方相含量可达 6 9 %,有利于应力诱导相变增韧,该 Z T A 复相陶瓷的抗弯强度、断裂韧性分别达到 604MPa、6.87MPa·m1/2。展开更多
文摘Semi-quantitative electron probe microanalysis （EPMA） mapping, scanning electron microscopy （SEM） and transmission electron microscopy （TEM） were employed to study the effect of one-step and two-step treatments on the Zr distribution and Al3Zr dispersoid characteristics in as-cast commercial AA7150 aluminum alloy. It is shown that the Zr concentration in the dendrite centre regions is higher than that near the dendrite edges in the as-cast condition, and that homogenization at 460 °C for 20 h is insufficient to remove these concentration gradients. After homogenizing at 460-480 °C, a high number density of larger dispersoids can be observed in dendrite centre regions but not near dendrite edges. Furthermore, the dispersoid size increases with increasing the temperature during both one-step and two-step homogenization treatments.
文摘以纳米ZrO 、微米Al O 为原料,采用无压烧结方式制备了ZTA 复相陶瓷。结果表明:nano-ZrO 的 2 2 3 2加入有利于制备细晶ZTA 复相陶瓷。此外,nano-ZrO 的加入对 Al O 陶瓷的显微结构也产生影响,ZrO 颗粒以 2 2 3 2“晶内型”和晶界型两种形式存在。合理的配方组成及制备工艺有利于 Z r O 以四方亚稳相存在。Z r O 含量为 2 23 0 w t % 时,其四方相含量可达 6 9 %,有利于应力诱导相变增韧,该 Z T A 复相陶瓷的抗弯强度、断裂韧性分别达到 604MPa、6.87MPa·m1/2。
