Bulk metallic glasses（BMGs）have attracted considerable attention in the last few decades particularly triggered by their potential applications as novel structural and/or functional materials,owing to their superior...Bulk metallic glasses（BMGs）have attracted considerable attention in the last few decades particularly triggered by their potential applications as novel structural and/or functional materials,owing to their superior strength,large elastic strain limit and relatively low Young′s modulus etc.compared to their crystalline counterparts.Here,a 3Dreconstruction application to the fractography and the morphology of shear bands was reported for a ductile Zr_（56）Co_（28）Al_（16）（at.%）BMG through a Phenom series desktop scanning electron microscope.The results of the 3Dreconstruction and the following contour analysis indicate a typical shear fracture mode for the investigated alloy.It is inferred that the fractography and the morphology of shear bands might be dependent on their composition,structure states,and loading conditions for BMGs.展开更多
93W-4.5Ni-l.5Fe-lCo （W） was prepared by powder metallurgic method, and then dynamic mechanical properties of this material were tested at high temperature by means of high-temperature split Hopkinson pressure bar （...93W-4.5Ni-l.5Fe-lCo （W） was prepared by powder metallurgic method, and then dynamic mechanical properties of this material were tested at high temperature by means of high-temperature split Hopkinson pressure bar （SHPB）. The results show that the material possesses high- dynamic mechanical properties, significant temperature effects, and strain hardening behaviors. Used two-stage light gas gun, the penetration test of 93W projectile was finished. After the completion of the test, through the microstructure observation of the residual 93W projectiles with the aid of scanning electron microscopy （SEM） and transmission electron microscopy （TEM）, it can be found that there are obvious signs of hot melt existing on the surface of the projectile, a lot of adiabatic shear bands inside the projectile, and microcracks exist at the end of adiabatic shear bands. The test results show that adiabatic shear is the main form to cause the projectile failure and it is the emergence of the adiabatic shearing phenomenon that makes 93W display good self-sharpening property in the process of hypervelocity penetration. At the same time, the results of TEM observation show that there are high- density dislocations at the interface between W and Ni-Fe- Co-based alloy inside the 93W.展开更多
基于面心立方固溶体结构和时效强化机理,设计出一种新型高密度合金NiW750。利用SEM,TEM对合金微观组织进行观察,采用分离式Hopkinson压杆实验研究合金在动态压缩条件下的特点,并将此合金与其领域常用材料超高强度钢G50及钨合金93WNiFe...基于面心立方固溶体结构和时效强化机理,设计出一种新型高密度合金NiW750。利用SEM,TEM对合金微观组织进行观察,采用分离式Hopkinson压杆实验研究合金在动态压缩条件下的特点,并将此合金与其领域常用材料超高强度钢G50及钨合金93WNiFe进行对比。结果表明:NiW750合金在3种材料中综合性能最好。在750℃/5h时效后,合金抗拉强度可达1746MPa,冲击韧度( a kU )可达113J/cm^2。在动态加载条件下,材料存在应变率硬化效应,其动态流变应力可达到2250MPa左右。试样在与中心轴线成45°方向形成绝热剪切带,在应变率约5500s -1 条件下,带宽80~150μm,过渡区较宽,避免材料剪切断裂过早出现。展开更多
Preheating is the first step for thermal-mechanical processing of the materials. Several preheating schedules were designed based on industrial manufacturing to explore their effect on the microstructure and mechanica...Preheating is the first step for thermal-mechanical processing of the materials. Several preheating schedules were designed based on industrial manufacturing to explore their effect on the microstructure and mechanical properties of AA2099 Al-Li alloy during the following hot rolling. The results show that the mechanical properties of as-rolled sheets are quite sensitive to preheating. Various types of secondary phases, including δ', T1 and T2 phases, were precipitated during the heating process. The difference among precipitates is the main reason to induce the variation of mechanical properties for as-rolled sheets. A rapid heating rate gave rise to the precipitation of δ' phase, which largely promoted yield stress and ultimate tensile strength in as-rolled sheets. T1 phase was more favorable in the preheating with a holding period at 150–250 °C, which caused a moderated strain hardening behavior. Precipitates formed during preheating induced different slip behaviors in the following deformation. The coexistence of T1 and δ' phase could restrict planar slip, which inhibited the formation of the shear band. The difference in the activity of non-octahedral slips and planar slips determined the strain hardening effect, which should be the reason for the variation of mechanical properties of as-rolled sheets.展开更多
Deformation behavior of a FeCrNi medium entropy alloy(MEA)prepared by powder metallurgy(P/M)method was investigated over a wide range of strain rates.The FeCrNi MEA exhibits high strain-hardening ability,which can be ...Deformation behavior of a FeCrNi medium entropy alloy(MEA)prepared by powder metallurgy(P/M)method was investigated over a wide range of strain rates.The FeCrNi MEA exhibits high strain-hardening ability,which can be attributed to the multiple deformation mechanisms,including dislocation slip,deformation induced stacking fault and mechanical twinning.The shear localization behavior of the FeCrNi MEA was also analyzed by dynamically loading hat-shaped specimens,and the distinct adiabatic shear band cannot be observed until the shear strain reaches~14.5.The microstructures within and outside the shear band exhibit different characteristics:the grains near the shear band are severely elongated and significantly refined by dislocation slip and twinning;inside the shear band,the initial coarse grains completely disappear,and transform into recrystallized ultrafine equiaxed grains by the classical rotational dynamic recrystallization mechanism.Moreover,microvoids preferentially nucleate in the central areas of the shear band where the temperature is very high and the shear stress is highly concentrated.These microvoids will coalesce into microcracks with the increase of strain,which eventually leads to the fracture of the shear band.展开更多
基金supported by National Natural Science Foundation of China(51301078,51461026and51671120)the Specialized Research Fund for the Doctoral Program of Higher Education of China(20135314120002)+1 种基金the Scientific Research Foundation of Department of Education,Yunnan(2017YJS059)the Young Talents Support Program of Faculty of Materials Science and Engineering,Kunming University of Science and Technology(20140102)
文摘Bulk metallic glasses（BMGs）have attracted considerable attention in the last few decades particularly triggered by their potential applications as novel structural and/or functional materials,owing to their superior strength,large elastic strain limit and relatively low Young′s modulus etc.compared to their crystalline counterparts.Here,a 3Dreconstruction application to the fractography and the morphology of shear bands was reported for a ductile Zr_（56）Co_（28）Al_（16）（at.%）BMG through a Phenom series desktop scanning electron microscope.The results of the 3Dreconstruction and the following contour analysis indicate a typical shear fracture mode for the investigated alloy.It is inferred that the fractography and the morphology of shear bands might be dependent on their composition,structure states,and loading conditions for BMGs.
基金financially supported by the Fundamental Research Funds for the Central Universities(Nos.DL12C B05 and 2572014EB04-02)the National Natural Science Foundation of China(Nos.31200434 and 31370566)the China Postdoctoral Science Foundation(No.2013M531007)
文摘93W-4.5Ni-l.5Fe-lCo （W） was prepared by powder metallurgic method, and then dynamic mechanical properties of this material were tested at high temperature by means of high-temperature split Hopkinson pressure bar （SHPB）. The results show that the material possesses high- dynamic mechanical properties, significant temperature effects, and strain hardening behaviors. Used two-stage light gas gun, the penetration test of 93W projectile was finished. After the completion of the test, through the microstructure observation of the residual 93W projectiles with the aid of scanning electron microscopy （SEM） and transmission electron microscopy （TEM）, it can be found that there are obvious signs of hot melt existing on the surface of the projectile, a lot of adiabatic shear bands inside the projectile, and microcracks exist at the end of adiabatic shear bands. The test results show that adiabatic shear is the main form to cause the projectile failure and it is the emergence of the adiabatic shearing phenomenon that makes 93W display good self-sharpening property in the process of hypervelocity penetration. At the same time, the results of TEM observation show that there are high- density dislocations at the interface between W and Ni-Fe- Co-based alloy inside the 93W.
文摘基于面心立方固溶体结构和时效强化机理,设计出一种新型高密度合金NiW750。利用SEM,TEM对合金微观组织进行观察,采用分离式Hopkinson压杆实验研究合金在动态压缩条件下的特点,并将此合金与其领域常用材料超高强度钢G50及钨合金93WNiFe进行对比。结果表明:NiW750合金在3种材料中综合性能最好。在750℃/5h时效后,合金抗拉强度可达1746MPa,冲击韧度( a kU )可达113J/cm^2。在动态加载条件下,材料存在应变率硬化效应,其动态流变应力可达到2250MPa左右。试样在与中心轴线成45°方向形成绝热剪切带,在应变率约5500s -1 条件下,带宽80~150μm,过渡区较宽,避免材料剪切断裂过早出现。
基金financially supported by the National Natural Science Foundation of China (Grant No. 51871038)the Chongqing Key Project of Technology Innovation and Application Development (Grant No. cstc2019jscx-mbdx X0025)the support from the University Innovation Research Group of Chongqing (Grant No. CXQT20023)。
文摘Preheating is the first step for thermal-mechanical processing of the materials. Several preheating schedules were designed based on industrial manufacturing to explore their effect on the microstructure and mechanical properties of AA2099 Al-Li alloy during the following hot rolling. The results show that the mechanical properties of as-rolled sheets are quite sensitive to preheating. Various types of secondary phases, including δ', T1 and T2 phases, were precipitated during the heating process. The difference among precipitates is the main reason to induce the variation of mechanical properties for as-rolled sheets. A rapid heating rate gave rise to the precipitation of δ' phase, which largely promoted yield stress and ultimate tensile strength in as-rolled sheets. T1 phase was more favorable in the preheating with a holding period at 150–250 °C, which caused a moderated strain hardening behavior. Precipitates formed during preheating induced different slip behaviors in the following deformation. The coexistence of T1 and δ' phase could restrict planar slip, which inhibited the formation of the shear band. The difference in the activity of non-octahedral slips and planar slips determined the strain hardening effect, which should be the reason for the variation of mechanical properties of as-rolled sheets.
基金supported by the National Natural Science Foundation of China[Grant numbers 52020105013,51771232]。
文摘Deformation behavior of a FeCrNi medium entropy alloy(MEA)prepared by powder metallurgy(P/M)method was investigated over a wide range of strain rates.The FeCrNi MEA exhibits high strain-hardening ability,which can be attributed to the multiple deformation mechanisms,including dislocation slip,deformation induced stacking fault and mechanical twinning.The shear localization behavior of the FeCrNi MEA was also analyzed by dynamically loading hat-shaped specimens,and the distinct adiabatic shear band cannot be observed until the shear strain reaches~14.5.The microstructures within and outside the shear band exhibit different characteristics:the grains near the shear band are severely elongated and significantly refined by dislocation slip and twinning;inside the shear band,the initial coarse grains completely disappear,and transform into recrystallized ultrafine equiaxed grains by the classical rotational dynamic recrystallization mechanism.Moreover,microvoids preferentially nucleate in the central areas of the shear band where the temperature is very high and the shear stress is highly concentrated.These microvoids will coalesce into microcracks with the increase of strain,which eventually leads to the fracture of the shear band.
