The analytical electron microscopy has been used to characterize the morphology,structure and composition of the nanostructured material of Sn- Bi alloy prepared by a modified electrohydrodynamic technique. The electr...The analytical electron microscopy has been used to characterize the morphology,structure and composition of the nanostructured material of Sn- Bi alloy prepared by a modified electrohydrodynamic technique. The electron diffraction pattern and the corresponding contrast image for the discrete particles with a diameter smaller than 4 nm have been obtained.It is shown that the nanocrystalline Sn-Bi alloy particles comprise a single crystal of Bi-containing β-Sn solid solution or of Sn-containing Bi solid solution. A direct preparation procedure of the samples during the electrohydrodynamic rapid solidification process has been developed for electron microscopic observation.展开更多
Relaxor ferroelectrics have different properties from that of the normal ferroelectrics,such as dielectric properties with diffuse phase transition and frequency dispersion,specific heat,birefringence,elastic constan...Relaxor ferroelectrics have different properties from that of the normal ferroelectrics,such as dielectric properties with diffuse phase transition and frequency dispersion,specific heat,birefringence,elastic constants and Raman scattering,etc.It is considered that the different properties are related with the polar nanoregions in relaxors.In this work we briefly introduce how we use the high spatial resolution analytical electron microscopy and high resolution electron microscopy methods to investigate the polar nanoregion in Pb(Mg_(1/3)Nb_(2/3))O_(3)(PMN),Pb(Mg_(1/3)Nb_(2/3))O_(3)PbTiO_(3)(PMNPT)and Ba(Ti_(1-x)Sn_(x))O_(3)(BTSn).The main experimental results110 are as mentioned in next three parts.展开更多
To explore ways to improve the accuracy of quantitative analysis of samples in the micrometer to nanometer range of magnitudes,we adopted analytical transmission electron microscopy(AEM/EDS)for qualitative and quantit...To explore ways to improve the accuracy of quantitative analysis of samples in the micrometer to nanometer range of magnitudes,we adopted analytical transmission electron microscopy(AEM/EDS)for qualitative and quantitative analysis of pyrite materials.Additionally,the k factor of pyrite is calculated experimentally.To develop an appropriate non-standard quantitative analysis model for pyrite materials,the experimentally calculated k factor is compared with that estimated from the non-standard quantitative analytical model of the instrument software.The experimental findings demonstrate that the EDS attached to a TEM can be employed for precise quantitative analysis of micro-and nanoscale regions of pyrite materials.Furthermore,it serves as a reference for improving the results of the EDS quantitative analysis of other sulfides.展开更多
文摘The analytical electron microscopy has been used to characterize the morphology,structure and composition of the nanostructured material of Sn- Bi alloy prepared by a modified electrohydrodynamic technique. The electron diffraction pattern and the corresponding contrast image for the discrete particles with a diameter smaller than 4 nm have been obtained.It is shown that the nanocrystalline Sn-Bi alloy particles comprise a single crystal of Bi-containing β-Sn solid solution or of Sn-containing Bi solid solution. A direct preparation procedure of the samples during the electrohydrodynamic rapid solidification process has been developed for electron microscopic observation.
文摘Relaxor ferroelectrics have different properties from that of the normal ferroelectrics,such as dielectric properties with diffuse phase transition and frequency dispersion,specific heat,birefringence,elastic constants and Raman scattering,etc.It is considered that the different properties are related with the polar nanoregions in relaxors.In this work we briefly introduce how we use the high spatial resolution analytical electron microscopy and high resolution electron microscopy methods to investigate the polar nanoregion in Pb(Mg_(1/3)Nb_(2/3))O_(3)(PMN),Pb(Mg_(1/3)Nb_(2/3))O_(3)PbTiO_(3)(PMNPT)and Ba(Ti_(1-x)Sn_(x))O_(3)(BTSn).The main experimental results110 are as mentioned in next three parts.
基金Funded by the International Science&Technology Cooperation Program of Hubei Province of China(No.2022EHB024)。
文摘To explore ways to improve the accuracy of quantitative analysis of samples in the micrometer to nanometer range of magnitudes,we adopted analytical transmission electron microscopy(AEM/EDS)for qualitative and quantitative analysis of pyrite materials.Additionally,the k factor of pyrite is calculated experimentally.To develop an appropriate non-standard quantitative analysis model for pyrite materials,the experimentally calculated k factor is compared with that estimated from the non-standard quantitative analytical model of the instrument software.The experimental findings demonstrate that the EDS attached to a TEM can be employed for precise quantitative analysis of micro-and nanoscale regions of pyrite materials.Furthermore,it serves as a reference for improving the results of the EDS quantitative analysis of other sulfides.
