The effects of magnetic field annealing on the properties of Fe48Co52 alloy nanowire arrays with various interwire distances （Di=30-60 nm） and wire diameters （Dw=22-46 nm） were investigated in detail. It was found...The effects of magnetic field annealing on the properties of Fe48Co52 alloy nanowire arrays with various interwire distances （Di=30-60 nm） and wire diameters （Dw=22-46 nm） were investigated in detail. It was found that the array＇s best annealing temperature and crys- talline structure did not show any apparent dependence on the treatment of applying a 3 kOe magnetic field along the wire during the annealing process. For arrays with small Dw or with large Di, the treatment of magnetic field annealing also had no obvious influence on their magnetic performances. However, such a magnetic field annealing constrained the shift of the easy magnetization direction and improved the coercivity and the squareness obviously for arrays with large Dw or with small Di. The difference in the intensity of the effective anisotropic field within the arrays was believed to be responsible for this different variation of the array＇s magnetic properties after magnetic field annealing.展开更多
In this paper,the sensors array technique is applied to the quality detection of aluminum alloy spot welding.The sensors array has three forms,i.e.,linear magnetic sensors array,annular magnetic sensors array and cros...In this paper,the sensors array technique is applied to the quality detection of aluminum alloy spot welding.The sensors array has three forms,i.e.,linear magnetic sensors array,annular magnetic sensors array and cross magnetic sensors array.An algorithm based on principal component analysis is proposed to extract the signal eigenvalues.The three types of magnetic sensors array are used in the experiment of monitoring the signal.After the eigenvalues are extracted,they are used to build a relationship with ...展开更多
Spot welding is affected by many factors and is difficult to monitor the nugget information with single sensor. In this paper, a new monitor system based on sensors array technique was developed for spot welding quali...Spot welding is affected by many factors and is difficult to monitor the nugget information with single sensor. In this paper, a new monitor system based on sensors array technique was developed for spot welding quality detection. The key part in the system is cross magnetic sensor array. It is composed of six magnetic sensors. An improved algorithm was proposed to extract the signal eigenvalue, which was based on principle component analysis. The results show that in the case of the 60 mm experiment, cross magnetic sensor array works well. And when the eigenvalues range of the cross magnetic sensor array is 0. 090 1 - 0. 098 2, the spots quality is good. The analysis of the eigenvalues of the cross magnetic sensor array allows us to determine whether the spot qualty is good or bad.展开更多
The mean hyper fine field at the Fe nuclei in amorphous alloys Fe80-xTxB20(T=Co,Ni,Mn,V,Ti) by fitting the Moessbauer spectra is displayed. The behaviors of both the hyperfine field and the atomic magnetic moment in t...The mean hyper fine field at the Fe nuclei in amorphous alloys Fe80-xTxB20(T=Co,Ni,Mn,V,Ti) by fitting the Moessbauer spectra is displayed. The behaviors of both the hyperfine field and the atomic magnetic moment in these amorphous alloys and the relation between both the properties are discussed.展开更多
The crystallization, microstructure, and soft magnetic properties of Fe52Co34Hf7B6Cul alloy are studied. Amorphous Fe52Co34Hf7B6Cul alloys are first treated by a pulsed magnetic field with a medium frequency, and then...The crystallization, microstructure, and soft magnetic properties of Fe52Co34Hf7B6Cul alloy are studied. Amorphous Fe52Co34Hf7B6Cul alloys are first treated by a pulsed magnetic field with a medium frequency, and then annealed at 100 ℃-400 ℃ for 30 min in a vacuum. The rise in temperature during the treatment by a pulsed magnetic field is measured by a non-contact infrared thermometer. The soft magnetic properties of specimens are measured by a vibrating sample magnetometer （VSM）. The microstructure changes of specimens are observed by a MSssbauer spectroscopy and transmission electron microscope （TEM）. The results show the medium-frequency pulsating magnetic field will pro- mote nanocrystallization of the amorphous alloy with a lower temperature rise. The nanocrystalline phase is （α-Fe（Co） with bcc crystal structure, and the grain size is about 10 nm. After vacuum annealing at 100 ℃ for 30 min, scattering nanocrystalline phases become more uniform, the coercive force and the saturation magnetization of the specimens are 41.98 A/m and 185.15 emu/g.展开更多
The corrosion behavior and microstructure of Fe78Si9B13 glassy alloy in NaOH and NaCl solutions under a 0.02-T magnetic field were investigated through electrochemical testing and scanning electron microscopy （SEM）....The corrosion behavior and microstructure of Fe78Si9B13 glassy alloy in NaOH and NaCl solutions under a 0.02-T magnetic field were investigated through electrochemical testing and scanning electron microscopy （SEM）. The current-density prepeak （PP） in the anodic polarization curves in low-concentration NaOH solutions （classified as type I） tends to disappear when the NaOH concentration is increased to 0.4 mol/L and the magnetic field is applied. Under the magnetic field, the height of the second current-density peak is increased in low-concentration NaOH solutions （type I） but decreased in high-concentration NaOH solutions （type Ⅱ）. The non-monotonic effect of the magnetic field was similarly observed in the case of polarization curves of samples measured in NaCl solutions, Ring-like corroded patterns and round pits are easily formed under the magnetic field in NaOH and NaC1 solutions. These experimental results were discussed in terms of the magnetohydrodynamic （MHD） effect.展开更多
We present results of an experimental study of magnetoresistance (MR) in insulating NbSi amorphous alloys sample showing Variable Range Hopping (VRH) conductivity. The MR is found to be negative in a wide range of low...We present results of an experimental study of magnetoresistance (MR) in insulating NbSi amorphous alloys sample showing Variable Range Hopping (VRH) conductivity. The MR is found to be negative in a wide range of low temperature (4.2-20 K) and in the range of moderate magnetic fields (0-4 T). We made tentative analysis using three theoretical models which are the model of quantum interference, the model of Zeeman effect and the model of localized magnetic展开更多
The measurement system is the main equipment of the project.Based on the characteristic of experiment system,a sensor array is designed,and used to continually acquire the global magnetic field.A scientific scheme is ...The measurement system is the main equipment of the project.Based on the characteristic of experiment system,a sensor array is designed,and used to continually acquire the global magnetic field.A scientific scheme is developed to get the signal processing and temperature compensation for nondirective weak magnetic field.The software of sampling control system is given,which is complied using C language in Labwindows/CVI.Taking computer as main engine,the system can acquire the nondirective weak magnetic field automatically and continuously use the sensor array,the change of magnetic field can be shown in real-time and intuitively.展开更多
Fe-based amorphous alloys with high saturation magnetic flux density(B_(s))are increasingly attractive from both scientific and technological points of view,however,they usually suffer from the trade-off between magne...Fe-based amorphous alloys with high saturation magnetic flux density(B_(s))are increasingly attractive from both scientific and technological points of view,however,they usually suffer from the trade-off between magnetization and softness.In this work,we explore the soft magnetic properties(SMPs),magnetic and atomic structures,and defect activation during creep deformation of as-quenched and annealed Fe_(82.65-x)Co_(x)Si_(2)B_(14)Cu_(1.35)(x=0-20)amorphous alloys(AAs).Improved magnetic softness-magnetization synergy has been realized in all these alloys by field annealing.Particularly,superb SMPs with superhigh B_(s) of 1.86 T,low coercivity of 1.2 A/m and high effective permeability of 16300 are obtained in the Fe_(66.65)Co_(16)Si_(2)B_(14)Cu_(1.35) AA.The locally regularized arrangement of domains,homogenized structure with less structural/magnetic defects and suppressed crystal-like ordering by field annealing contribute synergistically to the superb SMPs.Besides,the relaxation time spectra obtained from creep deformation indicate less liquid-like and solid-like defects activated in the field-annealed AA,which is correlated with the structural homogenization and superb SMPs.This work provides new and comprehensive insight into the interplay among external field,heterogeneous structure,SMPs and defect activation of Fe-based AAs,and offers a promising pathway for softening amorphous alloys with high Bs.展开更多
Annealing temperatures and applied magnetic fields are two important parameters for the performance modification of magnetic alloys.This article investigated the effect of different annealing temperatures on crystalli...Annealing temperatures and applied magnetic fields are two important parameters for the performance modification of magnetic alloys.This article investigated the effect of different annealing temperatures on crystallization condition,magnetic properties and thermal stability of the amorphous magnetic alloy Co_(36)Fe_(36)Si_(4.8)B1_(9.2)Nb_(4)(at%).Results indicate that the annealing temperature can significantly affect the size and content of precipitated nanocrystals in the amorphous alloy,and the precipitation of nanocrystalline phases can result in the distinct change of magnetic properties and Curie temperature.When the annealing was performed at 595 ℃ for 30 min under an applied transverse external magnetic field of 9550.0A·m^(-1),the amorphous alloy shows excellent soft magnetic properties with the saturation magnetization of alloy reaching 110.00 mA·m^(2)·g^(-1),the residual magnetic induction intensity of 4 × 10^(-6) T and the coercivity as low as57.3 A·m^(-1).Furthermore,the Curie temperature of the field-annealed samples can reach up to 440 0C,approximately 58℃ higher than that of the as-quenched species.展开更多
高速非晶合金永磁电机设计受电磁、机械、温升的制约,因此高速非晶合金永磁电机的设计是一个多物理场综合设计的过程。针对高速非晶合金永磁电机设计受多物理场制约的问题,基于多物理场的分析方法,分析了非晶合金材料对高速永磁电机电...高速非晶合金永磁电机设计受电磁、机械、温升的制约,因此高速非晶合金永磁电机的设计是一个多物理场综合设计的过程。针对高速非晶合金永磁电机设计受多物理场制约的问题,基于多物理场的分析方法,分析了非晶合金材料对高速永磁电机电磁性能的影响;研究了内置式永磁转子在高速运行状态下的应力分布,并分析了轴承支撑刚度对转子系统临界转速的影响;针对高速非晶合金永磁电机损耗分布特点研究了其温度场的分布。基于提出的多物理场综合设计方法,设计并制造了一台额定功率15 k W、最高转速30 000 r/min的高速内置式非晶合金永磁电机,并对样机进行了试验,验证了仿真分析与设计方法的可行性,为高速非晶合金永磁电机的设计提供参考。展开更多
基金ACKNOWLEDGMENTS This work was supported by the National Nature Science Foundation of China （No.50171033）, the National Key Project of Fundamental Research of China （No.2005CB623605）, and the Scientific Research Foundation for the Doctor of Hefei University of Technology （No.035032）.
文摘The effects of magnetic field annealing on the properties of Fe48Co52 alloy nanowire arrays with various interwire distances （Di=30-60 nm） and wire diameters （Dw=22-46 nm） were investigated in detail. It was found that the array＇s best annealing temperature and crys- talline structure did not show any apparent dependence on the treatment of applying a 3 kOe magnetic field along the wire during the annealing process. For arrays with small Dw or with large Di, the treatment of magnetic field annealing also had no obvious influence on their magnetic performances. However, such a magnetic field annealing constrained the shift of the easy magnetization direction and improved the coercivity and the squareness obviously for arrays with large Dw or with small Di. The difference in the intensity of the effective anisotropic field within the arrays was believed to be responsible for this different variation of the array＇s magnetic properties after magnetic field annealing.
基金Supported by National High Technology Research and Development Program ("863" Program) of China (No.2008AA04Z136)National Natural Science Foundation of China(No.50975197)+1 种基金Cooperation Project in Industry,Education and Research of Guangdong Province and Ministry of Education of China(No.2007A090302105)Tianjin Research Program of Application and Advanced Technology (No.09JCZDJC24000)
文摘In this paper,the sensors array technique is applied to the quality detection of aluminum alloy spot welding.The sensors array has three forms,i.e.,linear magnetic sensors array,annular magnetic sensors array and cross magnetic sensors array.An algorithm based on principal component analysis is proposed to extract the signal eigenvalues.The three types of magnetic sensors array are used in the experiment of monitoring the signal.After the eigenvalues are extracted,they are used to build a relationship with ...
基金This work was supported by Project of National 863 High Technology of China （ No. 2008AA04Z136 ）, Project supported by the National Natural Science Foundation of China（ No. 50975197）.
文摘Spot welding is affected by many factors and is difficult to monitor the nugget information with single sensor. In this paper, a new monitor system based on sensors array technique was developed for spot welding quality detection. The key part in the system is cross magnetic sensor array. It is composed of six magnetic sensors. An improved algorithm was proposed to extract the signal eigenvalue, which was based on principle component analysis. The results show that in the case of the 60 mm experiment, cross magnetic sensor array works well. And when the eigenvalues range of the cross magnetic sensor array is 0. 090 1 - 0. 098 2, the spots quality is good. The analysis of the eigenvalues of the cross magnetic sensor array allows us to determine whether the spot qualty is good or bad.
文摘The mean hyper fine field at the Fe nuclei in amorphous alloys Fe80-xTxB20(T=Co,Ni,Mn,V,Ti) by fitting the Moessbauer spectra is displayed. The behaviors of both the hyperfine field and the atomic magnetic moment in these amorphous alloys and the relation between both the properties are discussed.
基金Project supported by the National Natural Science Foundation of China(Grant No.50771025)
文摘The crystallization, microstructure, and soft magnetic properties of Fe52Co34Hf7B6Cul alloy are studied. Amorphous Fe52Co34Hf7B6Cul alloys are first treated by a pulsed magnetic field with a medium frequency, and then annealed at 100 ℃-400 ℃ for 30 min in a vacuum. The rise in temperature during the treatment by a pulsed magnetic field is measured by a non-contact infrared thermometer. The soft magnetic properties of specimens are measured by a vibrating sample magnetometer （VSM）. The microstructure changes of specimens are observed by a MSssbauer spectroscopy and transmission electron microscope （TEM）. The results show the medium-frequency pulsating magnetic field will pro- mote nanocrystallization of the amorphous alloy with a lower temperature rise. The nanocrystalline phase is （α-Fe（Co） with bcc crystal structure, and the grain size is about 10 nm. After vacuum annealing at 100 ℃ for 30 min, scattering nanocrystalline phases become more uniform, the coercive force and the saturation magnetization of the specimens are 41.98 A/m and 185.15 emu/g.
基金financially supported by the National Natural Science Foundation of China(No.51171091)the Excellent Youth Project of Shandong Natural Science Foundation(No.JQ201012)the Major State Basic Research Development Program of China(No.2012CB825702)
文摘The corrosion behavior and microstructure of Fe78Si9B13 glassy alloy in NaOH and NaCl solutions under a 0.02-T magnetic field were investigated through electrochemical testing and scanning electron microscopy （SEM）. The current-density prepeak （PP） in the anodic polarization curves in low-concentration NaOH solutions （classified as type I） tends to disappear when the NaOH concentration is increased to 0.4 mol/L and the magnetic field is applied. Under the magnetic field, the height of the second current-density peak is increased in low-concentration NaOH solutions （type I） but decreased in high-concentration NaOH solutions （type Ⅱ）. The non-monotonic effect of the magnetic field was similarly observed in the case of polarization curves of samples measured in NaCl solutions, Ring-like corroded patterns and round pits are easily formed under the magnetic field in NaOH and NaC1 solutions. These experimental results were discussed in terms of the magnetohydrodynamic （MHD） effect.
文摘We present results of an experimental study of magnetoresistance (MR) in insulating NbSi amorphous alloys sample showing Variable Range Hopping (VRH) conductivity. The MR is found to be negative in a wide range of low temperature (4.2-20 K) and in the range of moderate magnetic fields (0-4 T). We made tentative analysis using three theoretical models which are the model of quantum interference, the model of Zeeman effect and the model of localized magnetic
基金Project(10672191)supported by the National Natural Science Foundation of ChinaProject(06JJ2059)supported by the Provincial Natural Science Foundation of Hunan,ChinaProject(KF0607) supported by the Key Laboratory of Low Dimensional Materials and Application Technology (Xiangtan University),Ministry of Education,China
文摘The measurement system is the main equipment of the project.Based on the characteristic of experiment system,a sensor array is designed,and used to continually acquire the global magnetic field.A scientific scheme is developed to get the signal processing and temperature compensation for nondirective weak magnetic field.The software of sampling control system is given,which is complied using C language in Labwindows/CVI.Taking computer as main engine,the system can acquire the nondirective weak magnetic field automatically and continuously use the sensor array,the change of magnetic field can be shown in real-time and intuitively.
基金financially supported by the National Natural Science Foundation of China(Nos.51631003 and 51971061)。
文摘Fe-based amorphous alloys with high saturation magnetic flux density(B_(s))are increasingly attractive from both scientific and technological points of view,however,they usually suffer from the trade-off between magnetization and softness.In this work,we explore the soft magnetic properties(SMPs),magnetic and atomic structures,and defect activation during creep deformation of as-quenched and annealed Fe_(82.65-x)Co_(x)Si_(2)B_(14)Cu_(1.35)(x=0-20)amorphous alloys(AAs).Improved magnetic softness-magnetization synergy has been realized in all these alloys by field annealing.Particularly,superb SMPs with superhigh B_(s) of 1.86 T,low coercivity of 1.2 A/m and high effective permeability of 16300 are obtained in the Fe_(66.65)Co_(16)Si_(2)B_(14)Cu_(1.35) AA.The locally regularized arrangement of domains,homogenized structure with less structural/magnetic defects and suppressed crystal-like ordering by field annealing contribute synergistically to the superb SMPs.Besides,the relaxation time spectra obtained from creep deformation indicate less liquid-like and solid-like defects activated in the field-annealed AA,which is correlated with the structural homogenization and superb SMPs.This work provides new and comprehensive insight into the interplay among external field,heterogeneous structure,SMPs and defect activation of Fe-based AAs,and offers a promising pathway for softening amorphous alloys with high Bs.
基金financially supported by National S&T Major Project of China (No.2018ZX10301201)the National Natural Science Foundation of China (No.51371018)the Fundamental Research Funds for the Central Universities (No. FRF-BR-14-001B)。
文摘Annealing temperatures and applied magnetic fields are two important parameters for the performance modification of magnetic alloys.This article investigated the effect of different annealing temperatures on crystallization condition,magnetic properties and thermal stability of the amorphous magnetic alloy Co_(36)Fe_(36)Si_(4.8)B1_(9.2)Nb_(4)(at%).Results indicate that the annealing temperature can significantly affect the size and content of precipitated nanocrystals in the amorphous alloy,and the precipitation of nanocrystalline phases can result in the distinct change of magnetic properties and Curie temperature.When the annealing was performed at 595 ℃ for 30 min under an applied transverse external magnetic field of 9550.0A·m^(-1),the amorphous alloy shows excellent soft magnetic properties with the saturation magnetization of alloy reaching 110.00 mA·m^(2)·g^(-1),the residual magnetic induction intensity of 4 × 10^(-6) T and the coercivity as low as57.3 A·m^(-1).Furthermore,the Curie temperature of the field-annealed samples can reach up to 440 0C,approximately 58℃ higher than that of the as-quenched species.
文摘高速非晶合金永磁电机设计受电磁、机械、温升的制约,因此高速非晶合金永磁电机的设计是一个多物理场综合设计的过程。针对高速非晶合金永磁电机设计受多物理场制约的问题,基于多物理场的分析方法,分析了非晶合金材料对高速永磁电机电磁性能的影响;研究了内置式永磁转子在高速运行状态下的应力分布,并分析了轴承支撑刚度对转子系统临界转速的影响;针对高速非晶合金永磁电机损耗分布特点研究了其温度场的分布。基于提出的多物理场综合设计方法,设计并制造了一台额定功率15 k W、最高转速30 000 r/min的高速内置式非晶合金永磁电机,并对样机进行了试验,验证了仿真分析与设计方法的可行性,为高速非晶合金永磁电机的设计提供参考。
