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重熔对Al-Ti-La中间合金中Ti_(2)Al_(20)La相的影响
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作者 丁万武 田旭东 +4 位作者 陈建超 安家志 余海存 魏振鹏 杨成亮 《有色金属工程》 CAS 北大核心 2024年第8期56-66,共11页
通过扫描电镜、X射线衍射和电子探针等分析研究了重熔过程中不同保温时间和温度对Al-Ti-La中间合金中Ti_(2)Al_(20)La相的含量、形态尺寸和稳定性的影响。结果表明:在750℃下,随着保温时间的延长,Ti_(2)Al_(20)La相的溶解度逐渐增大,含... 通过扫描电镜、X射线衍射和电子探针等分析研究了重熔过程中不同保温时间和温度对Al-Ti-La中间合金中Ti_(2)Al_(20)La相的含量、形态尺寸和稳定性的影响。结果表明:在750℃下,随着保温时间的延长,Ti_(2)Al_(20)La相的溶解度逐渐增大,含量由未处理的20.776%下降至13.72%,形态由块状演变为圆整和细小的片状,长宽比由2.33下降至1.52;在1000℃下,保温15 min后溶解度较大,含量降低至4.5%,形态演变为尖锐的长条状,长宽比上升至2.55;溶解产生的La原子与Al在晶界处形成La-Al金属间化合物(IMC),Ti原子在基体中的分布密度随保温时间的延长和保温温度的升高而增高,以游离态均匀分布在基体中。 展开更多
关键词 Al-ti-La合金 ti_(2)Al_(20)La 重熔 保温时间
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显微组织对近α钛合金BT-20疲劳裂纹扩展的影响 被引量:2
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作者 郭庆清 王佳亮 +1 位作者 吴永红 姜永正 《东北大学学报(自然科学版)》 EI CAS CSCD 北大核心 2017年第3期345-349,共5页
通过显微镜及电子背散射衍射试验对近α钛合金BT-20的篮网、双态和魏氏组织微观结构及晶粒尺寸进行测定,并采用拉伸与疲劳裂纹扩展试验进行力学性能以及裂纹扩展研究,讨论微观组织对裂纹扩展速率、路径和断口形貌的影响.结果表明,双态... 通过显微镜及电子背散射衍射试验对近α钛合金BT-20的篮网、双态和魏氏组织微观结构及晶粒尺寸进行测定,并采用拉伸与疲劳裂纹扩展试验进行力学性能以及裂纹扩展研究,讨论微观组织对裂纹扩展速率、路径和断口形貌的影响.结果表明,双态组织的强度和延伸率最好,魏氏组织最差;双态组织的断口为解理断裂,裂纹碰到大尺寸初生α晶粒时发生穿晶失效,形态呈直线状,从而具有较高的扩展速率;篮网和魏氏组织的断口形式为沿相界断裂,裂纹扩展路径在通过α晶粒集束边界时改变方向,路径呈曲线状,扩展速率相对较低,从而具有较好的耐裂纹性能. 展开更多
关键词 bt-20 近Α钛合金 疲劳裂纹扩展 显微组织 断口形貌
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Homogeneity of microstructure and Vickers hardness in cold closed-die forged spur-bevel gear of 20Cr Mn Ti alloy 被引量:2
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作者 董丽颖 兰箭 庄武豪 《Journal of Central South University》 SCIE EI CAS CSCD 2015年第5期1595-1605,共11页
Cold closed-die forging is a suitable process to produce spur-bevel gears due to its advantages, such as saving materials and time, reducing costs, increasing die life and improving the quality of the product. The hom... Cold closed-die forging is a suitable process to produce spur-bevel gears due to its advantages, such as saving materials and time, reducing costs, increasing die life and improving the quality of the product. The homogeneity of microstructure of cold closed-die forged gears can highly affect their service performance. The homogeneity of microstructure and Vickers hardness in cold closed-die forged gear of 20 Cr Mn Ti alloy is comprehensively studied by using optical microscopy and Vickers hardness tester. The results show that the distribution homogeneity of the aspect ratio of grain and Vickers hardness is the same. In the circumferential direction of the gear tooth, the distribution of the aspect ratio of grain and Vickers hardness is inhomogeneous and they gradually decrease from the surface to the center of the tooth. In the radial direction, the distribution of the aspect ratio of grain and Vickers hardness is inhomogeneous on the surface of the gear tooth; while it is relatively homogeneous in the center of the gear tooth. In the axial direction of the gear tooth, the distribution of the aspect ratio of grain and Vickers hardness is relatively homogeneous from the small-end to the large-end of the gear tooth. 展开更多
关键词 cold closed-die forging 20Cr Mn ti alloy MICROSTRUCTURE Vickers hardness
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稀土磷复合变质剂对Al-20%Si合金的细化处理研究 被引量:1
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作者 林益雄 王连登 +4 位作者 杜安栋 王沁峰 王火生 张拓 黄街华 《铸造》 CAS 北大核心 2020年第10期1065-1071,共7页
采用EPMA、XRD与DSC等分析手段,对制得的AlTiCREP(含2%P)进行物相分析,研究不同P(以AlTiCREP形式加入)添加量、熔体处理温度及保温时间对Al-20%Si初生硅的变质效果的影响,并探讨其细化机理。结果表明:制得的AlTiCREP中间合金含有TiAl3、... 采用EPMA、XRD与DSC等分析手段,对制得的AlTiCREP(含2%P)进行物相分析,研究不同P(以AlTiCREP形式加入)添加量、熔体处理温度及保温时间对Al-20%Si初生硅的变质效果的影响,并探讨其细化机理。结果表明:制得的AlTiCREP中间合金含有TiAl3、TiC、AlP及稀土复合相;经AlTiCREP中间合金变质的初生硅颗粒明显细化且较圆整。添加0.03%AlTiCREP的变质效果最佳,初生Si尺寸细化至26.40μm,相对AlTiCRE细化的晶粒尺寸减小了10.8%,这归因于变质剂中的TiC在硅的作用下易于反应形成的Al4C3。该相可作为AlP的基底,在细化过程形成的Al4C3·AlP为初晶硅提供更多的形核质点,提高了AlP变质效果。最佳熔体处理温度为800℃,细化时效长达120 min。 展开更多
关键词 Al-ti-C-RE-P 热力学分析 AL-20%SI合金 变质处理 初晶硅
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Effect of Gd on microstructure and refinement performance of Al-5Ti-B alloy 被引量:2
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作者 Dong-song Yin Ning Zhang +1 位作者 Ke-ju Chen Yun-long Zhang 《China Foundry》 SCIE CAS 2021年第3期223-228,共6页
Al-5Ti-B and Al-5Ti-B-Gd master alloy refiners were fabricated by fluorine salt casting method.The microstructure and phase constitution of the master alloys were investigated by scanning electron microscopy (SEM),tra... Al-5Ti-B and Al-5Ti-B-Gd master alloy refiners were fabricated by fluorine salt casting method.The microstructure and phase constitution of the master alloys were investigated by scanning electron microscopy (SEM),transmission electron microscopy (TEM) and X-ray diffraction (XRD).The results show that Al-Ti-B alloy refiner consists of Al_(3)Ti phase and TiB2 phase.After Gd is introduced into the intermediate alloy,Ti_(2)Al_(20)Gd phase appears in the alloy,the size of Al_(3)Ti is significantly reduced,and Ti-Al-Gd phase is found in the edge of Al_(3)Ti phase.At the same time,some independent Ti-Al-Gd phases appear in local areas,which are Ti_(2)Al_(20)Gd phase determined by micro-area electron diffraction analysis.Analysis and calculation results of the high-resolution images of the Ti_(2)Al_(20)Gd/Al structure show that there is no other compound at the junction between the Ti_(2)Al_(20)Gd phase and Al,and Ti_(2)Al_(20)Gd phase has a great difference in atomic space with the α-Al,which cannot be directly used as heterogeneous nucleus.But,after being decomposed in the aluminum melt,the Ti_(2)Al_(20)Gd phase can promote the refinement effect of the refiner.In the Al-Ti-B-Gd master alloy,there are many dispersed Al_(3)Ti particles with a size of less than 1 μm,which can promote the Al-5Ti-B refining effect. 展开更多
关键词 Al-5ti-B alloy refiner Al_(3)ti rare earth Gd ti_(2)Al_(20)Gd
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