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Insights into in-situ imbibition behavior of fracturing fluid in propped shale fractures based on nuclear magnetic resonance:A case study from Longmaxi Formation shale,Sichuan Basin,China
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作者 Jing-Jing Guo Kai-Xiang Di +4 位作者 Lie-Hui Zhang Yu-Long Zhao Hui-Ying Tang Rui-Han Zhang Ye Tian 《Petroleum Science》 SCIE EI CAS CSCD 2024年第1期410-429,共20页
Shale gas is an important component of unconventional oil and gas resources.Studying the imbibition behavior is helpful to optimize flowback parameters and enhance gas recovery.Recent imbibition studies have focused o... Shale gas is an important component of unconventional oil and gas resources.Studying the imbibition behavior is helpful to optimize flowback parameters and enhance gas recovery.Recent imbibition studies have focused on shale matrix,and the pressure conditions discussed were mostly atmospheric.The initial imbibition behavior begins from propped fractures to matrix,but there are few studies working on explaining the imbibition behavior in propped fractures or the phenomenon of many shale wells exhibit higher productivity after a“soaking”period.Therefore,propped fracture samples were designed for imbibition and migration experiments.In order to accurately study the mechanism and main influencing factors of fracturing fluid imbibition and migration in propped and unpropped shale fractures under high temperature and high pressure,a series of experiments based on nuclear magnetic resonance(NMR)were carried out.Results showed that NMR T_(2) spectra of all samples exhibited a bimodal distribution.The final imbibition volume of fracturing fluid was positively related to pressure and fracture width.The imbibition effect of fracturing fluid was more evident in matrix pores under high pressure.In the migration during soaking stage,the fracturing fluid gradually migrated from large pores to small pores and gradually displaced the shale gas from the matrix,thus allowing the water blocking in propped fractures to self-unlock to some extent.Gas permeability decreased in the imbibition stage,while it recovered in the migration stage to some extent. 展开更多
关键词 Forced imbibition Migration SOAKING NMR T_(2)spectra Propped fracture Permeability recovery
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Exploring pore-scale production characteristics of oil shale after CO_(2) huff‘n’puff in fractured shale with varied permeability
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作者 Tianhan Xu Jian Wang +3 位作者 Yuhao Lu Danling Wang Li Yu Ye Tian 《International Journal of Coal Science & Technology》 EI CAS CSCD 2024年第1期194-203,共10页
Recent studies have indicated that the injection of carbon dioxide(CO_(2))can lead to increased oil recovery in fractured shale reservoirs following natural depletion.Despite advancements in understanding mass exchang... Recent studies have indicated that the injection of carbon dioxide(CO_(2))can lead to increased oil recovery in fractured shale reservoirs following natural depletion.Despite advancements in understanding mass exchange processes in subsurface formations,there remains a knowledge gap concerning the disparities in these processes between the matrix and fractures at the pore scale in formations with varying permeability.This study aims to experimentally investigate the CO_(2) diffusion behaviors and in situ oil recovery through a CO_(2) huff‘n’puff process in the Jimsar shale oil reservoir.To achieve this,we designed three matrix-fracture models with different permeabilities(0.074 mD,0.170 mD,and 0.466 mD)and experimented at 30 MPa and 91°C.The oil concentration in both the matrix and fracture was monitored using a low-field nuclear magnetic resonance(LF-NMR)technique to quantify in situ oil recovery and elucidate mass-exchange behaviors.The results showed that after three cycles of CO_(2) huff‘n’puff,the total recovery degree increased from 30.28%to 34.95%as the matrix permeability of the core samples increased from 0.074 to 0.466 mD,indicating a positive correlation between CO_(2) extraction efficiency and matrix permeability.Under similar fracture conditions,the increase in matrix permeability further promoted CO_(2) extraction efficiency during CO_(2) huff‘n’puff.Specifically,the increase in matrix permeability of the core had the greatest effect on the extraction of the first-cycle injection in large pores,which increased from 16.42%to 36.64%.The findings from our research provide valuable insights into the CO_(2) huff‘n’puff effects in different pore sizes following fracturing under varying permeability conditions,shedding light on the mechanisms of CO_(2)-enhanced oil recovery in fractured shale oil reservoirs. 展开更多
关键词 Shale reservoir Hydraulic fracturing CO_(2)huff‘n’puff NMR Production characteristics
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Investigation of influence factors on CO_(2) flowback characteristics and optimization of flowback parameters during CO_(2) dry fracturing in tight gas reservoirs
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作者 Xiao-Mei Zhou Lei Li +4 位作者 Yong-Quan Sun Ran Liu Ying-Chun Guo Yong-Mao Hao Yu-Liang Su 《Petroleum Science》 SCIE EI CAS CSCD 2023年第6期3553-3566,共14页
CO_(2) dry fracturing is a promising alternative method to water fracturing in tight gas reservoirs,especially in water-scarce areas such as the Loess Plateau.The CO_(2) flowback efficiency is a critical factor that a... CO_(2) dry fracturing is a promising alternative method to water fracturing in tight gas reservoirs,especially in water-scarce areas such as the Loess Plateau.The CO_(2) flowback efficiency is a critical factor that affects the final gas production effect.However,there have been few studies focusing on the flowback characteristics after CO_(2) dry fracturing.In this study,an extensive core-to-field scale study was conducted to investigate CO_(2) flowback characteristics and CH_(4) production behavior.Firstly,to investigate the impact of core properties and production conditions on CO_(2) flowback,a series of laboratory experiments at the core scale were conducted.Then,the key factors affecting the flowback were analyzed using the grey correlation method based on field data.Finally,taking the construction parameters of Well S60 as an example,a dual-permeability model was used to characterize the different seepage fields in the matrix and fracture for tight gas reservoirs.The production parameters after CO_(2) dry fracturing were then optimized.Experimental results demonstrate that CO_(2) dry fracturing is more effective than slickwater fracturing,with a 9.2%increase in CH_(4) recovery.The increase in core permeability plays a positive role in improving CH_(4) production and CO_(2) flowback.The soaking process is mainly affected by CO_(2) diffusion,and the soaking time should be controlled within 12 h.Increasing the flowback pressure gradient results in a significant increase in both CH_(4) recovery and CO_(2) flowback efficiency.While,an increase in CO_(2) injection is not conducive to CH_(4) production and CO_(2) flowback.Based on the experimental and field data,the important factors affecting flowback and production were comprehensively and effectively discussed.The results show that permeability is the most important factor,followed by porosity and effective thickness.Considering flowback efficiency and the influence of proppant reflux,the injection volume should be the minimum volume that meets the requirements for generating fractures.The soaking time should be short which is 1 day in this study,and the optimal bottom hole flowback pressure should be set at 10 MPa.This study aims to improve the understanding of CO_(2) dry fracturing in tight gas reservoirs and provide valuable insights for optimizing the process parameters. 展开更多
关键词 CO_(2)fracturing Tight gas reservoir fracturing fluid flowback Parameter optimization
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The enhancement of performance and imbibition effect of slickwater-based fracturing fluid by using MoS_(2)nanosheets
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作者 Hang Xu Yuan Li +6 位作者 Guo-Lin Yu Sa-Sa Yang Bo-Jun Li Fu-Jian Zhou Er-Dong Yao Hao Bai Zhi-Yu Liu 《Petroleum Science》 SCIE EI CAS CSCD 2023年第4期2187-2201,共15页
Slickwater-based fracturing fluid has recently garnered significant attention as the major fluid for volumetric fracturing;however,lots of challenges and limitations such as low viscosity,poor salt tolerance,and possi... Slickwater-based fracturing fluid has recently garnered significant attention as the major fluid for volumetric fracturing;however,lots of challenges and limitations such as low viscosity,poor salt tolerance,and possible formation damage hinder the application of the conventional simple slickwater-based fracturing fluid.In addition,nanomaterials have proven to be potential solutions or improvements to a number of challenges associated with the slickwater.In this paper,molybdenum disulfide(MoS_(2))nanosheets were chemically synthesized by hydrothermal method and applied to improve the performance of conventional slickwater-based fracturing fluid.Firstly,the microstructure characteristics and crystal type of the MoS_(2)nanosheets were analyzed by SEM,EDS,TEM,XPS,and Raman spectroscopy techniques.Then,a series of evaluation experiments were carried out to compare the performance of MoS_(2)nanosheet-modified slickwater with the conventional slickwater,including rheology,drag reduction,and sand suspension.Finally,the enhanced imbibition capacity and potential mechanism of the nanosheet-modified slickwater were systematically investigated.The results showed that the self-synthesized MoS_(2)nanosheets displayed a distinct ultrathin flake-like morphology and a lateral size in the range of tens of nanometers.In the nano-composites,each MoS_(2)nanosheet plays the role of cross-linking point,so as to make the spatial structure of the entire system more compact.Moreover,nanosheet-modified slickwater demonstrates more excellent properties in rheology,drag reduction,and sand suspension.The nanosheet-modified slickwater has a higher apparent viscosity after shearing 120 min under 90℃ and 170 s^(−1).The maximum drag reduction rate achieved 76.3%at 20℃,and the sand settling time of proppants with different mesh in the nano-composites was prolonged.Spontaneous imbibition experiments showed that the gel-breaking fluid of nanosheet-modified slickwater exhibited excellent capability of oil-detaching,and increase the oil recovery to∼35.43%.By observing and analyzing the interfacial behavior of MoS_(2)nanosheets under stimulated reservoir conditions,it was found that the presence of an interfacial tension gradient and the formation of a climbing film may play an essential role in the spontaneous imbibition mechanism.This work innovatively uses two-dimensional MoS_(2)nanosheets to modify regular slickwater and confirms the feasibility of flake-like nanomaterials to improve the performance of slickwater.The study also reveals the underlying mechanism of enhanced imbibition efficiency of the nano-composites. 展开更多
关键词 Slickwater-based fracturing fluid MoS_(2)nanosheet Performance evaluation spontaneous imbibition Climbing film
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基于热障涂层的La_(2)Zr_(2)O_(7)材料改性研究进展 被引量:1
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作者 张晓东 王昊 +2 位作者 梁逸帆 宋艺 王铀 《材料保护》 CAS CSCD 2024年第3期50-62,69,共14页
随着航空发动机不断向高推重比、高性能方向发展,传统、单一的热障涂层(Thermal barrier coating,TBC)已经不能满足热端部件严苛的服役要求。锆酸镧(La_(2)Zr_(2)O_(7))具有熔点高、高温下结构稳定、低热导率等优点,具有极好的隔热性能... 随着航空发动机不断向高推重比、高性能方向发展,传统、单一的热障涂层(Thermal barrier coating,TBC)已经不能满足热端部件严苛的服役要求。锆酸镧(La_(2)Zr_(2)O_(7))具有熔点高、高温下结构稳定、低热导率等优点,具有极好的隔热性能,有望成为新一代热障涂层候选材料,但在实际应用中仍存在两大关键问题,即热膨胀系数低和断裂韧性差。因此,La_(2)Zr_(2)O_(7)材料在服役过程中会因热失配而造成局部热应力集中,导致涂层过早剥落失效,严重影响涂层的服役寿命。国内外研究表明,对La_(2)Zr_(2)O_(7)材料进行改性可以有效解决上述问题。为此,系统分析了关于La_(2)Zr_(2)O_(7)材料改性的研究工作,将La_(2)Zr_(2)O_(7)材料改性总结为4类:第二相复合、稀土掺杂、纳米化和高熵化。重点介绍了4种不同改性方式对La_(2)Zr_(2)O_(7)材料热导率、热膨胀系数的影响及增韧机理,并对La_(2)Zr_(2)O_(7)材料改性研究工作进行总结和展望,以为La_(2)Zr_(2)O_(7)材料在热障涂层领域的应用提供理论支撑。 展开更多
关键词 La_(2)Zr_(2)O_(7) 热物理性能 断裂韧性 纳米结构 高熵
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超临界CO_(2)对致密碳酸盐岩力学特性影响
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作者 苟波 王琨 +2 位作者 李骁 詹立 刘超 《西南石油大学学报(自然科学版)》 CAS CSCD 北大核心 2024年第2期65-76,共12页
采用超临界CO_(2)破致密碳酸盐岩具有破裂压力低,易形成复杂缝特点,但其作用的力学机理尚未清晰。选用马家沟组致密白云岩样,采用高温高压超临界CO_(2)饱和流体法,研究了岩样在超临界CO_(2)+地层水的流体中浸泡不同时间后的物性、声波... 采用超临界CO_(2)破致密碳酸盐岩具有破裂压力低,易形成复杂缝特点,但其作用的力学机理尚未清晰。选用马家沟组致密白云岩样,采用高温高压超临界CO_(2)饱和流体法,研究了岩样在超临界CO_(2)+地层水的流体中浸泡不同时间后的物性、声波响应、岩石力学特性和破裂形态特征。结果表明,随着浸泡时间增加,化学溶蚀作用引起溶蚀孔径增大,岩样孔隙度、渗透率增加,而声波速度、动态和静态岩石力学参数均下降;当浸泡时间大于1.0 d后,岩样物性参数增大和力学强度降低明显;随着浸泡时间增加,岩样破裂形态由单一低角度剪切缝向高角度剪切缝、共轭缝和剪切、张型复合缝等复杂形态发展;压裂短时间内(小于1.0 d)超临界CO_(2)+地层水形成的弱酸对岩石力学强度劣化程度有限。 展开更多
关键词 致密碳酸盐岩 超临界CO_(2) 前置酸压 力学强度 破裂形态
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基于BMP-2/BMP-7机制探讨生龙接骨胶囊预防老年骨质疏松性胸腰椎骨折术后再发性骨折的作用
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作者 邓平征 周龙殿 +4 位作者 张斌 胡和军 邓雄伟 徐南云 江共涛 《中国当代医药》 CAS 2024年第12期4-8,共5页
目的探讨生龙接骨胶囊对老年骨质疏松性胸腰椎骨折(OTF)术后再发性骨折的作用,并基于骨形态发生蛋白-2/骨形态发生蛋白-7(BMP-2/BMP-7)机制初步分析其作用机制。方法选取2020年1月至2022年10月在南昌市洪都中医院收治的100例行经皮椎体... 目的探讨生龙接骨胶囊对老年骨质疏松性胸腰椎骨折(OTF)术后再发性骨折的作用,并基于骨形态发生蛋白-2/骨形态发生蛋白-7(BMP-2/BMP-7)机制初步分析其作用机制。方法选取2020年1月至2022年10月在南昌市洪都中医院收治的100例行经皮椎体成形术(PVP)的老年OTF患者为研究对象,按随机数字表法分为常规组(50例)和胶囊组(50例)。常规组采用常规的PVP治疗,胶囊组患者在常规组基础上服用生龙接骨胶囊治疗。比较两组患者椎体结构(Cobb角和伤椎椎体前缘高度比)、治疗前后血清BMP-2、BMP-7水平、骨代谢指标[骨特异性碱性磷酸酶(BALP)、Ⅰ型原胶原N端前肽(PⅠNP)、骨钙素(OST)]、骨密度(BMD)、康复情况[Oswestry腰椎功能障碍指数(ODI)]评估、疼痛等级[视觉模拟评分法(VAS)]评分、临床有效率、椎体再骨折发生率和不良反应发生情况。结果治疗后,两组患者Cobb角改善,伤椎椎体前缘高度比优于治疗前,胶囊组均优于常规组,差异有统计学意义(P<0.05);胶囊组的BMP-2、BMP-7表达量高于常规组,差异有统计学意义(P<0.05);患者术后再发性骨折情况均良好,胶囊组愈合速度快于常规组,差异有统计学意义(P<0.05);治疗后,胶囊组的BALP、PⅠNP、OST均高于常规组,差异有统计学意义(P<0.05);两组患者的BMD高于治疗前,且胶囊组高于常规组,ODI评分、VAS评分均低于治疗前,且胶囊组低于常规组,差异有统计学意义(P<0.05);胶囊组的临床总有效率(95.0%)高于常规组(80.0%),胶囊组的再骨折发生率(4%)低于常规组(18%),差异有统计学意义(P<0.05);两组患者均未见明显不良反应。结论生龙接骨胶囊能通过上调患者血清BMP-2、BMP-7水平,改善BMD从而预防老年OTF的术后再发性骨折,其机制可能与生龙接骨胶囊能刺激BMP信号通路,加速成骨细胞分化有关。 展开更多
关键词 骨折 生龙接骨胶囊 骨形态发生蛋白-2 骨形态发生蛋白-7 术后再发性骨折
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超临界CO_(2)脉动压裂-渗流耦合试验系统研制与应用
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作者 刘佳佳 张云龙 +2 位作者 聂子硕 高志扬 许文松 《煤田地质与勘探》 EI CAS CSCD 北大核心 2024年第6期12-20,共9页
【目的】为了有效强化煤层气抽采效果,将脉动压裂与超临界CO_(2)压裂相结合,提出了利用超临界CO_(2)脉动压裂煤(岩)的新思路。【方法】自主研发了超临界CO_(2)脉动压裂-渗流耦合真三轴试验系统,介绍了该试验系统的主要结构、特点和功能... 【目的】为了有效强化煤层气抽采效果,将脉动压裂与超临界CO_(2)压裂相结合,提出了利用超临界CO_(2)脉动压裂煤(岩)的新思路。【方法】自主研发了超临界CO_(2)脉动压裂-渗流耦合真三轴试验系统,介绍了该试验系统的主要结构、特点和功能,然后开展了室内真三轴条件下超临界CO_(2)脉动压裂-渗流试验及超临界CO_(2)脉动压裂-声发射监测试验。该系统结合独立伺服系统与中央数字系统控制三向应力,采用双泵型恒速恒压泵脉动给压,具有高精度、全过程、真三轴、承载高温、高压及高应力的特点。【结果和结论】试验结果表明:超临界CO_(2)脉动压裂-渗流耦合真三轴试验系统可以实现良好的脉动压裂功能。超临界CO_(2)脉动压裂后,煤体渗透率较压裂前呈增大趋势,增大了2~9倍,且煤体渗透率皆呈现良好的指数变化规律。在声发射-超临界CO_(2)脉动压裂时期,煤体产生了新的裂隙通道,该通道由压裂孔中心直接贯穿至煤样表面,且可观测到超临界CO_(2)流体直接从煤中喷出,故超临界CO_(2)脉动压裂具有一定的扩展和连通裂隙的作用,能够有效提高煤层气的抽采效果。研究成果为强化深部低渗煤层增透技术提供了一定的试验支撑。 展开更多
关键词 超临界CO_(2) 脉动压裂 真三轴 渗流特性 声发射
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中深层稠油水平井前置CO_(2)蓄能压裂技术
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作者 杨兆臣 卢迎波 +5 位作者 杨果 黄纯 弋大琳 贾嵩 吴永彬 王桂庆 《岩性油气藏》 CAS CSCD 北大核心 2024年第1期178-184,共7页
利用准噶尔盆地西北缘乌夏地区中深层稠油油藏参数,对水平井前置CO_(2)蓄能压裂技术的开发机理、关键操作参数及开发效果进行了详细研究。研究结果表明:①伴随压裂—焖井—生产等开发阶段的延伸,前置CO_(2)蓄能压裂后的油井逐步显现出... 利用准噶尔盆地西北缘乌夏地区中深层稠油油藏参数,对水平井前置CO_(2)蓄能压裂技术的开发机理、关键操作参数及开发效果进行了详细研究。研究结果表明:①伴随压裂—焖井—生产等开发阶段的延伸,前置CO_(2)蓄能压裂后的油井逐步显现出增能改造、扩散降黏、膨胀补能、释压成泡沫油流等特性,井底流压提高了2~4MPa,CO_(2)扩散至油藏的1/3,原油黏度降至500mPa·s以下,泡沫油流明显;②研究区最优压裂段间距为60m、裂缝半长为90m、裂缝导流能力为10t/m,CO_(2)最佳注入强度为1.5m3/m,注入速度为1.8m3/min,油井焖井时间为30d,油藏采收率提高了2%~3%;③通过与常规压裂生产效果进行对比,前置CO_(2)蓄能压裂技术可使产油量提高5.2t/d,预测CO_(2)换油率达2.45,开发效果显著提升。 展开更多
关键词 中深层稠油 水平井 二氧化碳蓄能压裂 低碳采油 乌夏地区 准噶尔盆地
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基于CT扫描的CO_(2)相变致裂煤裂隙演化特征
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作者 刘高峰 关文博 +3 位作者 张震 李宝林 刘欢 司念 《矿业科学学报》 CSCD 北大核心 2024年第3期342-350,共9页
为进一步揭示CO_(2)相变致裂煤的裂隙改造机理,开展了CO_(2)相变致裂煤体实验,基于CT扫描和三维裂隙重构,分析了CO_(2)相变致裂前后的煤样内部裂隙结构参数,查明了CO_(2)相变致裂煤的三维裂隙结构演化特征。结果表明,致裂后煤样的裂隙... 为进一步揭示CO_(2)相变致裂煤的裂隙改造机理,开展了CO_(2)相变致裂煤体实验,基于CT扫描和三维裂隙重构,分析了CO_(2)相变致裂前后的煤样内部裂隙结构参数,查明了CO_(2)相变致裂煤的三维裂隙结构演化特征。结果表明,致裂后煤样的裂隙总数量减少,裂隙总体积和裂隙总表面积增加;CO_(2)相变致裂产生了裂隙扩张转化效应,在致裂压力的扩张作用下,小尺度裂隙转化为更大尺度的裂隙;长度小于1000μm的裂隙数量减少、裂隙体积和表面积明显减小,长度大于1000μm的裂隙体积和表面积明显增大,且裂隙之间扩张贯通而引起其数量减少;CO_(2)相变致裂大幅度改善了煤体三维裂隙的连通性,有利于气体的运移和产出。此研究为CO_(2)相变致裂效果提供新的分析评价方法,也可为其他非常规天然气储层及其改造的裂隙演化特征研究提供参考和借鉴。 展开更多
关键词 CO_(2)相变致裂 CT扫描 煤储层 三维裂隙演化
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超临界CO_(2)管道止裂韧性预测模型研究
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作者 曹宇光 甄莹 +2 位作者 刘媛媛 张振永 白芳 《石油机械》 北大核心 2024年第7期28-35,共8页
碳中和目标下,超临界态CO_(2)管道输送已成为碳捕集利用与封存(CCUS)技术发展的必然趋势。然而,目前超临界CO_(2)管道止裂控制体系尚未构建,管材止裂韧性难以预测,成为限制其广泛应用的瓶颈问题之一。针对该问题,通过归纳国内外相关文... 碳中和目标下,超临界态CO_(2)管道输送已成为碳捕集利用与封存(CCUS)技术发展的必然趋势。然而,目前超临界CO_(2)管道止裂控制体系尚未构建,管材止裂韧性难以预测,成为限制其广泛应用的瓶颈问题之一。针对该问题,通过归纳国内外相关文献及规范标准,对超临界CO_(2)管道止裂控制研究进展及最新标准体系进行了简要综述;在系统收集已开展CO_(2)管道全尺寸爆破试验信息及数据的基础上,对现有止裂韧性预测模型适用性进行了讨论,由此确定了CO_(2)管道止裂韧性预测模型修正形式,并对不同模型适用范围及预测结果进行了讨论。研究结果表明,建立的修正模型解决了传统止裂预测模型过于激进的问题,同时降低了DNV推荐方法的保守性。建议将修正模型与DNN预测方法相结合,以使管材韧性值处于止裂区域;同时开展高效准确的CO_(2)管道裂纹动态扩展数值模拟。所得结果可为我国CO_(2)管道止裂设计提供指导。 展开更多
关键词 超临界CO_(2) 管道输送 延性断裂 双曲线模型 断裂 韧性 夏比冲击功 止裂控制
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80-3Cr油管钢在CO_(2)驱环境下的性能研究与应用
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作者 时维才 苏航 +3 位作者 周星光 王少龙 姚峰 付安庆 《焊管》 2024年第6期49-53,共5页
针对CO_(2)驱高CO_(2)分压、高H_(2)S分压、低温井筒环境造成N80、P110管柱失效的问题,开展了80-3Cr、N80、P110三种管材的耐CO_(2)腐蚀、抗H_(2)S应力腐蚀开裂、耐低温冷脆对比评价试验。结果表明,不同CO_(2)工况条件下,N80、P110、80-... 针对CO_(2)驱高CO_(2)分压、高H_(2)S分压、低温井筒环境造成N80、P110管柱失效的问题,开展了80-3Cr、N80、P110三种管材的耐CO_(2)腐蚀、抗H_(2)S应力腐蚀开裂、耐低温冷脆对比评价试验。结果表明,不同CO_(2)工况条件下,N80、P110、80-3Cr油管在添加缓蚀剂情况下的腐蚀速率分别为0.0549 mm/a、0.0645 mm/a、0.0333 mm/a;80-3Cr油管的腐蚀速率明显低于N80、P110油管;80-3Cr油管在不同H_(2)S环境下均未出现应力腐蚀开裂,具有较好的抗H_(2)S应力腐蚀性能;在-20℃的低温环境下,N80和P110油管冲击功分别只有80-3Cr油管的62.6%和23.2%;80-3Cr油管在CO_(2)驱油现场应用后,管柱失效率从2019年的20%下降到0,取得显著效果。 展开更多
关键词 80-3Cr油管钢 CO_(2)驱 腐蚀 低温冷脆
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Numerical simulation study on shear resistance of anchorage joints considering tensile-shear fracture criterion of 2G-NPR bolt 被引量:1
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作者 Shulin Ren Zhigang Tao +2 位作者 Manchao He Mengnan Li Qiru Sui 《International Journal of Coal Science & Technology》 EI CAS CSCD 2023年第4期186-202,共17页
2G-NPR bolt (the 2nd generation Negative Poisson’s Ratio bolt) is a new type of bolt with high strength, high toughness and no yield platform. It has signifcant efects on improving the shear strength of jointed rock ... 2G-NPR bolt (the 2nd generation Negative Poisson’s Ratio bolt) is a new type of bolt with high strength, high toughness and no yield platform. It has signifcant efects on improving the shear strength of jointed rock mass and controlling the stability of surrounding rock. To achieve an accurate simulation of bolted joint shear tests, we have studied a numerical simulation method that takes into account the 2G-NPR bolt's tensile–shear fracture criterion. Firstly, the indoor experimental study on the tensile–shear mechanical properties of 2G-NPR bolt is carried out to explore its mechanical properties under diferent tensile–shear angles, and the fracture criterion of 2G-NPR bolt considering the tensile–shear angle is established. Then, a three-dimensional numerical simulation method considering the tensile–shear mechanical constitutive and fracture criterion of 2G-NPR bolt, the elastoplastic mechanical behavior of surrounding rock and the damage and deterioration of grouting body is proposed. The feasibility and accuracy of the method are verifed by comparing with the indoor shear test results of 2G-NPR bolt anchorage joints. Finally, based on the numerical simulation results, the deformation and stress of the bolt, the distribution of the plastic zone of the rock mass, the stress distribution and the damage of the grouting body are analyzed in detail. The research results can provide a good reference value for the practical engineering application and shear mechanical performance analysis of 2G-NPR bolt. 展开更多
关键词 Anchorage joints 2G-NPR bolt Tensile-shear fracture criterion Shear behavior Numerical simulation
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海洋CO_(2)管道输送技术现状与展望 被引量:1
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作者 王子明 李清平 +2 位作者 李姜辉 范振宁 张建 《中国工程科学》 CSCD 北大核心 2024年第2期74-91,共18页
管道输送是经济高效的CO_(2)运输方式,海洋CO_(2)运输是离岸碳捕集、利用与封存(CCUS)产业链的关键环节和规模化开展离岸CCUS工程建设所需的核心技术。本文明晰了我国实施离岸CCUS的优势、典型海洋碳运输情境和海洋CO_(2)运输方式,剖析... 管道输送是经济高效的CO_(2)运输方式,海洋CO_(2)运输是离岸碳捕集、利用与封存(CCUS)产业链的关键环节和规模化开展离岸CCUS工程建设所需的核心技术。本文明晰了我国实施离岸CCUS的优势、典型海洋碳运输情境和海洋CO_(2)运输方式,剖析了国内外海洋CO_(2)管道输送的技术与工程概况;从CO_(2)流体相态及流动安全,沿程腐蚀风险评估、监测及预警,CO_(2)泄漏实时监测技术,高压CO_(2)泄放及对环境的影响等方面梳理了海洋CO_(2)管道输送工艺技术现状;从CO_(2)管道材料断裂行为及止裂措施、高耐蚀及密封材料、碳钢管道长寿命运行的关键腐蚀控制技术、注采井筒的腐蚀风险评估等方面梳理了海洋CO_(2)管道材料技术现状。研究认为,加快发展适应海洋CO_(2)管道输送复杂工况的材料体系、全流程CO_(2)管道的智慧管理与数字孪生技术、海底CO_(2)管道全生命周期运行关键技术、在役海底管道改输评估与保障技术,采取加快推动我国近海碳封存CO_(2)管网规划、拓展和深化跨行业/跨机构合作模式创新、系统建设海陆统筹的标准体系、引导专业化技术服务企业深度参与海底CO_(2)管网建设等举措,促进我国海洋CO_(2)管道输送体系高质量建设。 展开更多
关键词 CO_(2)管道 离岸CCUS 海底管道 管道腐蚀 管道断裂 泄漏监测
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基于CO_(2)水基压裂液的煤体软化及降尘技术应用 被引量:1
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作者 黄辉龙 冯俊文 +2 位作者 邓广哲 李红健 李龙龙 《煤炭技术》 CAS 2024年第1期129-132,共4页
为解决坚硬煤层条件下,常规煤体注水方式效果不好,回采过程中顶煤可放性差、工作面截煤和放煤过程中粉尘大的难题,根据金川煤矿煤层的具体情况,基于煤体压裂软化-润渗除尘理论,利用CO_(2)活性水耦合液、液相与气相耦合液,代替传统注水... 为解决坚硬煤层条件下,常规煤体注水方式效果不好,回采过程中顶煤可放性差、工作面截煤和放煤过程中粉尘大的难题,根据金川煤矿煤层的具体情况,基于煤体压裂软化-润渗除尘理论,利用CO_(2)活性水耦合液、液相与气相耦合液,代替传统注水和注气技术,在金川煤矿开展了煤体软化及降尘技术应用研究。CO_(2)活性水压裂软化润渗技术,能够使煤体中裂隙和孔隙的容积以及结构发生变化,造成煤体的破裂和松动,降低了煤炭强度,达到对硬煤最佳的软化效果。试验表明:煤层CO_(2)水基压裂后,放煤循环速度提高了5.6%,顶煤破碎块度均衡,顶煤平均采出率提高了3.2%;截割浮尘浓度降低45%,工作面能见度提高,工作面转载运输点煤尘降低23%,润渗作用有效降低了煤体产生浮尘的能力。 展开更多
关键词 厚硬煤层 压裂软化 CO_(2)耦合 软化性 润湿性
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Effect of stress sensitivity on displacement efficiency in CO_2 flooding for fractured low permeability reservoirs 被引量:4
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作者 Wang Rui Yue Xiang'an +2 位作者 Zhao Renbao Yan Pingxiang Dave Freeman 《Petroleum Science》 SCIE CAS CSCD 2009年第3期277-283,共7页
Carbon dioxide flooding is an effective means of enhanced oil recovery for low permeability reservoirs. If fractures are present in the reservoir, CO2 may flow along the fractures, resulting in low gas displacement ef... Carbon dioxide flooding is an effective means of enhanced oil recovery for low permeability reservoirs. If fractures are present in the reservoir, CO2 may flow along the fractures, resulting in low gas displacement efficiency. Reservoir pore pressure will fluctuate to some extent during a CO2 flood, causing a change in effective confining pressure. The result is rock deformation and a reduction in permeability with the reduction in fracture permeability, causing increased flow resistance in the fracture space. Simultaneously, gas cross flowing along the fractures is partially restrained. In this work, the effect of stress changes on permeability was studied through a series of flow experiments. The change in the flowrate distribution in a matrix block and contained fracture with an increase in effective pressure were analyzed. The results lead to an implicit comparison which shows that permeability of fractured core decreases sharply with an increase in effective confining pressure. The fracture flowrate ratio declines and the matrix flowrate ratio increases. Fracture flow will partially divert to the matrix block with the increase in effective confining pressure, improving gas displacement efficiency. 展开更多
关键词 Stress sensitivity flowrate distribution MATRIX fracturE co2 flooding displacement efficiency
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Fundamental study and utilization on supercritical CO_(2) fracturing developing unconventional resources:Current status,challenge and future perspectives 被引量:3
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作者 Bing Yang Hai-Zhu Wang +5 位作者 Gen-Sheng Li Bin Wang Liang Chang Gang-Hua Tian Cheng-Ming Zhao Yong Zheng 《Petroleum Science》 SCIE CAS CSCD 2022年第6期2757-2780,共24页
Under the fact that considerable explo ration and production of unconventional re sources and wo rsening global climate,reducing carbon emission and rationally utilizing carbon resources have been drawn increasing att... Under the fact that considerable explo ration and production of unconventional re sources and wo rsening global climate,reducing carbon emission and rationally utilizing carbon resources have been drawn increasing attention.Supercritical CO_(2)(SC-CO_(2)) has been proposed as anhydrous fracturing fluid to develop unconventional reservoirs,since its advantages of reducing water consumption,reservoir contamination etc.Well understanding of SC-CO_(2)fracturing mechanism and key influencing factors will exert significant impact on the application of this technology in the field.In this paper,the fundamental studies on SC-CO_(2)fracturing from the aspects of laboratory experiment and simulation are reviewed.The fracturing experimental setups,fracture monitoring and characterizing methods,unconventional formation categories,numerical simulation approaches,fracturing mechanism and field application etc.,are analyzed.The fundamental study results indicate that compared with conventional hydraulic fracturing,SC-CO_(2)fracturing can reduce fracture initiation pressure and easily induce complex fracture networks with multiple branches.The field test further verifies the application prospect and the possibility of carbon storage.However,due to the limitation of reservoir complexity and attributes of SC-CO_(2),massive challenges will be encountered in SC-CO_(2)fracturing.According to the current research status,the limitations in basic research and field application are summarized,and the future development direction of this technology and relevant suggestions are proposed. 展开更多
关键词 Unconventional resources Supercritical CO_(2)fracturing Experiment and numerical simulation fracture initiation and propagation
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英买2地区多属性约束叠前宽方位裂缝预测
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作者 曾勇坚 高宏亮 +4 位作者 关宝珠 艾明波 蔡泉 李飞 王张恒 《新疆石油地质》 CAS CSCD 北大核心 2024年第4期483-488,共6页
英买2地区位于塔里木盆地塔北隆起英买力低凸起南部的英买2号构造上,受构造运动和岩浆侵入的影响,发育大量定向排列的高角度裂缝,储集层主要为裂缝型储集层。由于英买2地区储集层埋藏深度大且非均质性强,采用相干、曲率、蚂蚁体等叠后... 英买2地区位于塔里木盆地塔北隆起英买力低凸起南部的英买2号构造上,受构造运动和岩浆侵入的影响,发育大量定向排列的高角度裂缝,储集层主要为裂缝型储集层。由于英买2地区储集层埋藏深度大且非均质性强,采用相干、曲率、蚂蚁体等叠后裂缝预测技术预测该地区裂缝型储集层难度大。以英买2地区叠前宽方位偏移距矢量片(OVT)域道集为基础,开展以叠前去噪、各向异性时差校正等手段为主的井控叠前OVT域道集优化处理,获得高质量的叠前宽方位道集,并以能够表征缝洞型储集层的梯度结构张量、振幅曲率和剩余波阻抗为主的叠后多属性为约束开展叠前相控裂缝预测。能够有效预测超深层缝洞型碳酸盐岩储集层的裂缝,为塔里木盆地裂缝型储集层油气勘探开发提供借鉴。 展开更多
关键词 塔里木盆地 英买2地区 裂缝预测 缝洞型储集层 多属性约束 宽方位地震 OVT域
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超临界CO_(2) 萃取页岩油效果评价及影响因素分析
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作者 李邦国 侯家鵾 +3 位作者 雷兆丰 张博 王斌 陈江 《石油钻探技术》 CAS CSCD 北大核心 2024年第4期94-103,共10页
为明确裂缝及压力对超临界CO_(2)萃取页岩油的影响机理,在获取试验用页岩岩样孔径分布、比表面积和孔体积的基础上,进行了超临界CO_(2)岩样萃取试验,采用改进的磁悬浮天平高压吸附仪,实时测定了高温高压下页岩岩样质量的变化;并结合页... 为明确裂缝及压力对超临界CO_(2)萃取页岩油的影响机理,在获取试验用页岩岩样孔径分布、比表面积和孔体积的基础上,进行了超临界CO_(2)岩样萃取试验,采用改进的磁悬浮天平高压吸附仪,实时测定了高温高压下页岩岩样质量的变化;并结合页岩核磁共振T2谱,精确测定了超临界CO_(2)对页岩油的萃取效率,明确了萃取过程中页岩孔隙动用特征及动用孔径下限。试验结果表明,目标储层页岩中介孔(孔径2~50 nm)发育程度最高,占总孔隙体积和总比表面积的69.72%和73.47%;而大孔(孔径>50 nm)发育程度最差,仅占总孔隙体积和总比表面积的4.45%和10.77%。原油主要赋存于孔径1.4~120.0 nm的小孔径孔隙中,CO_(2)对大孔径(>86 nm)孔隙中原油的萃取效果高于小孔径(≤86 nm)孔隙;裂缝能够增大CO_(2)与基质中页岩油的接触面积,加快油气传质速度,提高基质动用深度,降低页岩油渗流阻力和孔隙动用下限。然而,CO_(2)萃取效率除与裂缝数量相关外,还受基质渗透率及裂缝−基质连通特征的影响。CO_(2)动用孔隙孔径下限随注入压力升高而降低,由8 MPa时的6.54 nm减小至18 MPa的3.27 nm。研究成果可为注CO_(2)提高页岩油采收率提供借鉴。 展开更多
关键词 页岩油 裂缝 CO_(2) 注入压力 核磁共振 萃取效率 称重法
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Effect of proppant pumping schedule on the proppant placement for supercritical CO_(2) fracturing 被引量:1
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作者 Yong Zheng Hai-Zhu Wang +4 位作者 Ying-Jie Li Gang-Hua Tian Bing Yang Cheng-Ming Zhao Ming-Sheng Liu 《Petroleum Science》 SCIE CAS CSCD 2022年第2期629-638,共10页
Supercritical CO_(2)fracturing is a potential waterless fracturing technique which shows great merits in eliminating reservoir damage,improving shale gas recovery and storing CO_(2)underground.Deep insight into the pr... Supercritical CO_(2)fracturing is a potential waterless fracturing technique which shows great merits in eliminating reservoir damage,improving shale gas recovery and storing CO_(2)underground.Deep insight into the proppant-transport behavior of CO_(2)is required to better apply this technique in the engineering field.In the present paper,we adopted a coupled Computational Fluid Dynamics and Discrete Element Method(CFD-DEM)approach to simulate the proppant transport in a fracking fracture with multiple perforation tunnels.Previous experiments were first simulated to benchmark the CFD-EDM approach,and then various pumping schedules and injection parameters(injection location,multi-concentration injection order,multi-density injection order and injection temperature)were investigated to determine the placement characteristics of proppant.Results indicate that the swirling vortex below the injection tunnels dominates the proppant diffusion in the fracture.The velocity of fluid flow across the proppant bank surface in multi-concentration injection shows a positive correlation with the proppant concentration.Injecting high-density proppant first can promote the transportation of low-density proppant injected later in the fracture to a certain extent.Decreasing the initial injection temperature of supercritical CO_(2)slurry helps enhance the particle-driving effect of fluid and improve the performance of supercritical CO_(2)in carrying proppant. 展开更多
关键词 Supercritical CO_(2)fracturing Proppant placement CFD-DEM Unconventional natural gas CO_(2)utilization
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